The invention belongs to the technical field of
metal powder preparation, and discloses a method for preparing silver
powder through reduction of hydrazine
hydrate with the adjustable particle size. The preparation method comprises the following steps that a first dispersing agent is dissolved in deionized water, a silver-
ammonia solution and a hydrazine
hydrate solution are sequentially added, stirring reaction is conducted, and nano-silver
seed crystal sol is obtained; uniformly mixing the obtained nano-silver
seed crystal sol with a hydrazine
hydrate solution and a second dispersing agent to obtain a reducing base solution; adding a surface modifier into absolute ethyl
alcohol, and uniformly dissolving to obtain a
surface modification coating solution; preparing a silver-
ammonia solution, adding the prepared silver-
ammonia solution into the reducing base solution, then adding the
surface modification coating solution, and stirring for reaction to obtain silver
powder slurry liquid; and after
solid-liquid separation, a
solid phase is taken, washed and dried, and silver powder is obtained. The preparation method is simple in process, the particle size of the silver powder can be adjusted through the adding amount of the
seed crystal, and the prepared silver powder particles are uniform in
particle size distribution, high in
dispersity and suitable for the fields of conductive
silver paste,
electronic packaging and the like.