The application discloses a kind of frozen forming high
porosity ceramic membrane support and preparation method thereof, it is related to
ceramic membrane technical field,
slurry raw material is placed into
ball mill, ball milling is passed 100 mesh screen, obtain
slurry, again
slurry is introduced into prepared
polytetrafluoroethylene mould, again mould is directly placed into
liquid nitrogen pool and frozen forming, then demolding, obtain wet blank, again wet blank is placed into vacuum environment, vacuum freeze-
drying, obtain dry blank, then dry blank is placed into
kiln, high-temperature
sintering, then natural cooling,
ceramic membrane support is obtained.The application
ceramic membrane support preparation is only 4 process steps, whole process is simple, and
raw material component is simple, it is not necessary to add a large number of binder, pore-forming agent to increase
porosity, 1-5min can be completed forming, greatly reduce forming time, greatly shorten the
sintering cycle of whole support, simultaneously using vacuum freeze-
drying, utilize water sublimation
drying, the position where water is located can form interstice, greatly improve the
porosity of support.