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Microstructure is the very small scale structure of a material, defined as the structure of a prepared surface of material as revealed by an optical microscope above 25× magnification. The microstructure of a material (such as metals, polymers, ceramics or composites) can strongly influence physical properties such as strength, toughness, ductility, hardness, corrosion resistance, high/low temperature behaviour or wear resistance. These properties in turn govern the application of these materials in industrial practice. Microstructure at scales smaller than can be viewed with optical microscopes is often called nanostructure, while the structure in which individual atoms are arranged is known as crystal structure. The nanostructure of biological specimens is referred to as ultrastructure. A microstructure’s influence on the mechanical and physical properties of a material is primarily governed by the different defects present or absent of the structure. These defects can take many forms but the primary ones are the pores. Even if those pores play a very important role in the definition of the characteristics of a material, so does its composition. In fact, for many materials, different phases can exist at the same time. These phases have different properties and if managed correctly, can prevent the fracture of the material.
Fatigue life simulation evaluation method for lightweight aluminum alloy material of new energy automobile
The invention discloses a fatigue life simulation evaluation method for a lightweight aluminum alloy material of a new energy automobile, and relates to the technical field of material life evaluation. A microstructure image is collected, coupling features are extracted through machine learning, and heterogeneous data fusion and enhancement are completed; generating a topological optimization structure based on a GAN, introducing a VPSC model to describe anisotropy according to a stress gradient dynamic grid, and constructing a dynamic finite element model; fusing vehicle driving data, predicting a load by using LSTM, performing VMD decomposition and environment correction, and realizing space-time correlation load spectrum reconstruction; a phase field model is used in a microcosmic mode, cracks are tracked in a macroscopic mode through XFEM, damage parameters are transmitted in a bidirectional coupling mode, and multi-physics field coupling simulation is carried out; fusing simulation and test data by adopting Bayesian reasoning, calculating life probability distribution, and correcting parameters when errors exceed the limit; according to the method, the fatigue life prediction error is finally reduced, the time consumption of single simulation is reduced, full-life-cycle evaluation and visual early warning are realized, an efficient scheme is provided for lightweight design, and industrial technology upgrading is promoted.
Owner:ANHUI TECHN COLLEGE OF MECHANICAL & ELECTRICAL ENG
Curved polyaniline modified 3D printing polyurethane material and application thereof
The invention belongs to the technical field of polymer preparation, and particularly relates to a curved-surface polyaniline modified 3D printing polyurethane material and application thereof. According to the preparation method, an ice crystal hard template method and a polyether glycol soft template method are combined, so that the microstructure of polyaniline is adjusted, and the curved polyaniline with regular morphology is prepared. The curved-surface arc-shaped structure has a large specific surface area, can form more contact sites with resin when being directly melt-blended with the resin, is beneficial to construction of a conductive path, and is not easy to agglomerate due to the curved-surface structure. The polyaniline with the arc-shaped structure is of a three-dimensional space structure and is directly blended with the resin to form a randomly arranged conductive network structure, so that the composite material is not easy to break when being impacted, and can be better embedded between the resin to form a stress transfer channel, and a complex three-dimensional network structure is constructed; the mechanical property and the antistatic capability of the product are improved.
Owner:SUZHOU GANGRUITONG NANO MATERIALS TECH CO LTD
Flexible magnetic tactile sensing device based on microstructure elastic layer, three-dimensional force measuring device and measuring method
PendingCN120927180ASynthetic resin layered productsElectrical equipmentCondensed matter physicsMaterials science
The invention discloses a flexible magnetic tactile sensing device based on a microstructure elastic layer, a three-dimensional force measuring device and a measuring method.The flexible magnetic tactile sensing device comprises a flexible magnetic film, the microstructure elastic layer, a Hall sensor, a PCB and a bottom shell, the Hall sensor is installed on the PCB, and the flexible magnetic film, the microstructure elastic layer, the PCB and the bottom shell are sequentially stacked from top to bottom; the microstructure elastic layer is of a non-planar structure, when the flexible magnetic film deforms due to stress, deformation of the flexible magnetic film is transmitted to the microstructure elastic layer, the change of the three-axis magnetic field intensity is measured through the Hall sensor and uploaded to a PC terminal for data processing, and three-dimensional force measurement is achieved. Three-dimensional force measurement can be achieved, the flexible magnetic film can generate local deformation in the normal direction when normal force is applied, the flexible magnetic film can generate tangential displacement when tangential force is applied, and application scenes suitable for different microstructure elastic layers are provided according to quantitative analysis results.
Owner:SOUTHEAST UNIV
Double cold rolled non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
A double cold rolled non-oriented electrical steel sheet having a composition including, expressed in percentage by weight: 0.0001%≤Carbon≤0.007%, 0.15%≤Manganese≤0.3%, 3.2%≤Silicon≤3.8%, 0.8%≤Aluminum≤1.1%, Phosphorus≤0.15%, Sulfur≤0.006%, Nitrogen≤0.09%, and can contain various optional elements. The remainder composition being iron and unavoidable impurities caused by processing, the microstructure is made of ferrite and has in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, less than 30% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000 A / m (J50) from 1.66 T to 1.69 T.
Owner:ARCELORMITTAL SA
Earth and rockfill dam material seepage deformation inspection system and method
The invention discloses an earth and rockfill dam material seepage deformation inspection system and method, and relates to the technical field of earth and rockfill dam engineering.The method comprises the steps that a sample of an earth and rockfill dam material is prepared and arranged in a test cavity of a permeameter; maintaining a steady-state seepage field in the sample; in the maintaining process of the steady-state seepage field, acoustic response signals and thermal response signals excited in the sample due to the seepage effect are synchronously collected through a distributed sensing system arranged around the sample; analyzing the acquired acoustic response signal and thermal response signal, and identifying and positioning an acoustic abnormal area with abnormal sound energy release and a thermal abnormal area with abnormal thermal change; and after the early warning signal is generated, the spatial and temporal distribution characteristics of the acoustic abnormal region and the thermal abnormal region are used as input, a parameter distribution field representing the damage evolution of the microstructure in the sample is calculated through a coupled physical inversion algorithm, and the permeability stability of the sample is evaluated based on the parameter distribution field.
Owner:LIANYUNGANG WATER CONSERVANCY PLANNING & DESIGN INST CO LTD
Double cold rolled non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
A double cold rolled non-oriented electrical steel sheet having a composition including of the following elements, expressed in percentage by weight: 0.0001%≤Carbon≤0.007%, 0.1%≤Manganese≤0.3%, 3.1%≤Silicon≤3.8%, 0.6%≤Aluminum≤0.8%, Phosphorus≤0.15%, Sulfur≤0.006%, Nitrogen≤0.09%, and can contain various optional elements. The remainder composition is iron and unavoidable impurities caused by processing. The microstructure ferrite and has in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, of 40 to 50% when calculated in accordance with Bertotti method and simultaneously having a magnetic polarization at 5000 A / m (J50) from 1.66T to 1.7T.
Owner:ARCELORMITTAL SA
Additive manufacturing lens surface optimization method based on real-time feedback control
The invention relates to the technical field of additive manufacturing, and discloses an additive manufacturing lens surface optimization method based on real-time feedback control. The method comprises the following steps: firstly, acquiring eye biometric data and personalized visual demand parameters of a wearer, establishing a personalized optical model of eyeballs according to the eye biometric data and the personalized visual demand parameters, and deducing a retina defocusing amount distribution map; and determining spatial arrangement and geometric morphology parameters of the distributed out-of-focus microstructure layer on the lens according to the atlas. In the additive manufacturing process, the optical material is deposited and solidified layer by layer, and the three-dimensional shape information of the surface of the optical material is obtained in real time after deposition of each layer. And comparing and analyzing the morphology information with a theoretical model to generate a morphology deviation result. And then, a correction instruction of the printing parameters is calculated by using the correction model, and the printing parameters of the additive manufacturing equipment are adjusted in real time, so that real-time compensation and optimization of the morphology deviation are realized, and finally, a high-precision lens product meeting personalized optical design requirements is manufactured.
Owner:南通诺瞳奕目医疗科技有限公司 +1
Method for detecting surface cracks of steel rail
The invention relates to a method for detecting surface cracks of a steel rail, which comprises the following steps of: controlling the environmental temperature difference change of the steel rail to enable thermal response to generate a hysteresis phenomenon, inducing slight asynchronous thermal fluctuation with discontinuous and asymmetric thermal diffusion in a local area of a material surface layer, and exposing a potential crack boundary; non-contact low-intensity laser thermal disturbance multi-angle scanning is used for executing a disturbance penetration test, non-structural thermal anomalies are removed, and a real crack area is determined; carrying out attenuation curve recording on the thermal response after multiple rounds of disturbance excitation, and reversely deducing the integrity degree of the microstructure below the crack according to the disturbance settlement time so as to judge the structural fatigue grade; environmental steady state comparison is carried out on the same detection area, through comparison of temperature and humidity, wind speed and radiation environment parameter changes before and after disturbance, if the crack area still continuously shows thermal response abnormity under a constant environment condition, it is confirmed that the thermal characteristic is caused by a structural crack, and otherwise, misjudgment caused by external accidental interference is eliminated.
Owner:ZHEJIANG YUNZONG INFORMATION TECHNOLOGY CO LTD
Optical diffusion plate microstructure defect detection method, electronic equipment and storage medium
ActiveCN121595563AImage analysisOptically investigating flaws/contaminationReference imageEngineering
The invention discloses an optical diffusion plate microstructure defect detection method, electronic equipment and a storage medium. The method comprises the following steps: acquiring images of the same diffusion plate area under at least two different illumination angles and performing elastic registration so as to eliminate image dislocation caused by plate movement; decoupling and separating physical defect features stably existing under all illumination and shadow interference features changing along with illumination from the registered image; carrying out enhancement and dynamic up-sampling processing on the physical defect features, and generating a suspected defect candidate region set with a low confidence threshold; for each candidate region, reconstructing a virtual reference image when the region has no defect through a generative model by utilizing the peripheral texture of the candidate region, and judging authenticity and outputting a confidence coefficient by comparing residual errors; and determining a final alarm result according to whether the confidence exceeds an alarm threshold. According to the invention, artifacts and real physical defects caused by mechanical micro-vibration and micro-structure reflection can be effectively distinguished, and the false alarm rate is obviously reduced.
Owner:SHENZHEN YUHUI OPTICAL TECH CO LTD
Online test analysis method for physical properties of electronic component material
The invention relates to the technical field of electronic component testing for investigating or analyzing internal microstructures and physical properties of materials by utilizing an electrical means, and discloses an online testing and analyzing method for physical properties of electronic component materials, which comprises the following steps of: constructing a composite excitation signal formed by linearly superposing a main carrier voltage and a perturbation wave voltage; applying the signal to a to-be-tested electronic component and acquiring response current; and extracting an intermodulation current amplitude at an intermodulation frequency point in the frequency spectrum of which the linear response interval is excluded, calculating a nonlinear response coefficient of the material in combination with the excitation amplitude, and comparing the nonlinear response coefficient with a preset degradation threshold so as to judge whether the nonlinear response coefficient is qualified or not. By extracting intermodulation components which cannot be generated by linear contact resistance, physical isolation of external contact noise in a frequency domain is realized, and the problem that contact resistance fluctuation and material intrinsic aging cannot be distinguished in a traditional linear impedance test is solved.
Owner:SICHUAN SHENGYI ELECTRICAL EQUIPMENT CO LTD
Welding deformation prediction system based on simulation analysis
The invention discloses a welding deformation prediction system based on simulation analysis, and relates to the technical field of welding deformation prediction.The welding deformation prediction system comprises the steps that a micro-area unit grid is constructed by obtaining a geometric model of a to-be-welded structure, material heterogeneous distribution and welding path information; based on the grid and material characteristics, establishing a local nonlinear thermal-mechanical coupling simulation model; inputting heat source parameters, calculating an instantaneous temperature field, and constructing a stress evolution function in combination with path change; further deducing initial strain distribution, and generating a local deformation estimation map; error inversion is executed by comparing with historical experimental data, heat source and material parameters are corrected, and a simulation model is updated; and finally, outputting a welding deformation prediction map, and identifying a deformation sensitive region in the microstructure. The method has the high-precision prediction capability and the self-adaptive correction characteristic, and is suitable for deformation control and process optimization of the micro-scale welding structure.
Owner:CHANGCHUN INST OF TECH
Laser cladding layer based on copper-magnesium-titanium-zirconium gradient design and preparation method thereof
PendingCN120945362AIncreasing energy efficiencyMetallic material coating processesThermal dilatationSurface engineering
The invention relates to the technical field of metal surface engineering, and discloses a laser cladding layer based on copper-magnesium-titanium-zirconium gradient design and a preparation method thereof.The preparation method comprises gradient structure design, a microstructure strengthening mechanism, a laser cladding process and thermal field control. By constructing a copper-magnesium-titanium component gradient transition structure and matching the thermal expansion coefficient difference between a matrix and a coating in real time, interface thermal stress accumulation can be dynamically inhibited, the crack defect caused by thermal expansion mismatch of a traditional cladding layer is avoided, ordered diffusion of elements at the interface is promoted through gradual change of gradient components, and the thermal conductivity of the cladding layer is improved. The metallurgical bonding reliability of the coating and a base body is improved, meanwhile, a stable coating is formed, the long-term service stability under the extreme working condition is guaranteed, a microstructure strengthening mechanism regulation and control means is adopted, the coating has a stable and effective protective barrier in a corrosive medium environment, and the problem of performance degradation caused by structure defects of a traditional cladding layer is solved.
Owner:ANHUI UNIVERSITY OF ARCHITECTURE
Multi-dimensional light pressure regulation and control method and device based on metasurface microstructure array
The invention relates to the technical field of optical metasurface and light field regulation and control, in particular to a light pressure multi-dimensional regulation and control method and device based on a metasurface microstructure array. The method comprises the following steps: designing and preparing a metasurface microstructure array, wherein the microstructure array is composed of a plurality of sub-wavelength scale three-dimensional microstructure units arranged on a dielectric substrate; surface plasmon resonance is excited by adjusting structural parameters of the three-dimensional microstructure units and adjusting working parameters of a light source acting on the microstructure array, and near-field localization and enhancement are achieved. And calculating, regulating and controlling the light pressure borne by the metasurface microstructure array based on the Maxwell stress tensor. The method can keep a remarkable light pressure enhancing effect in a wide spectrum range of 380-1300 nm, and is suitable for various material systems such as silver, gold and the like. The method can be applied to the fields of optical tweezers systems, optical control devices, precision measurement and the like, and has the advantages of flexible design, simplicity and convenience in preparation, high regulation and control precision and the like.
Owner:TIANJIN UNIV
460 mpa-grade marine engineering steel having excellent fracture resistance and manufacturing method therefor
A 460 MPa-grade marine engineering steel having excellent fracture resistance and a manufacturing method therefor, said steel comprising: C: 0.05%-0.10%; Si: 0.15%-0.40%; Mn: 1.40%-2.00%; P≤0.008%; S≤0.002%; Cu: 0.15%-0.45%; Ni: 0.50%-1.00%; Cr: 0.15%-0.40%; Nb: 0.015%-0.05%; Ti: 0.007%-0.02%; Alt: 0.015%-0.055%; O≤0.001%; N≤0.005%; and the balance being Fe and unavoidable impurities, wherein Pcm≤0.24%. By means of optimization of raw material composition screening and proportioning, a preparation process, microstructure strength and toughness matching, etc., a 460 MPa-grade marine engineering steel having excellent fracture resistance and a maximum thickness of 100 mm is obtained.
Owner:ANGANG STEEL CO LTD
High belite iron aluminate cement clinker and preparation method thereof
The invention discloses a high belite iron aluminate cement clinker, which is prepared from the following raw materials in parts by weight: 39 to 73 parts of carbide slag, 8 to 37 parts of low-grade bauxite, 10 to 16 parts of ardealite, 1 to 31 parts of fly ash and 3 to 9 parts of steel slag. According to the cement clinker, the resource utilization rate of industrial solid waste in cement preparation can be remarkably increased, and dependence on natural raw materials and high-grade raw materials is reduced; impurities in various solid wastes can be used as in-situ mineralizing agents and activating agents, and on the basis of realizing high-added-value resource utilization of various industrial solid wastes and low-grade bauxite, efficient synthesis of target minerals at a relatively low temperature is promoted; and gradient temperature control calcination and gradient cooling processes are further combined, so that sufficient crystallization and development of a target mineral phase can be effectively promoted, a clinker microstructure is optimized, excellent early strength and continuously increased later strength of the cement are ensured, and the common problems of strength shrinkage and the like of the traditional solid waste-based cement can be effectively avoided.
Owner:YICHENG ANDA SPECIAL CEMENT CO LTD +1
Multi-dimensional stealth submarine bionic heterogeneous protective shell and preparation method thereof
The invention discloses a multi-dimensional stealth submarine bionic heterogeneous protective shell and a preparation method thereof, and relates to the technical field of ship and ocean engineering. The submarine bionic heterogeneous protective shell is composed of a sandwich structure and a modified carbon nanotube film; the sandwich structure comprises a bionic Priative multi-stage rotating core layer, a bionic Diamond multi-stage rotating core layer, a bionic octagonal body spiral core layer, a bionic rhombic dodecahedron spiral core layer, a micro-perforated plate and a sound absorption lower plate. According to the design, the Bouligand structure and the acoustic structure principle of the giant bone tongue fish scale are fused, the unique configuration of inter-layer rotation and spiral rising in the microstructure of the giant bone tongue fish scale is used for reference, four bionic structures are innovatively constructed, deformation is effectively restrained, the stability of the overall structure is improved, and through force-sound coupling regulation and control, the mechanical property of the giant bone tongue fish scale is greatly improved. And an innovative solution is provided for achieving the mechanical bearing and sound stealth integrated function of the submarine shell.
Owner:JILIN UNIVERSITY
Lap welding method for thin aluminum row
PendingCN120901448APolishing machinesWelding/soldering/cutting articlesPower batteryTemperature control
The invention relates to the technical field of copper-aluminum composite welding, in particular to a thin aluminum bar lap welding method. The method comprises the following steps: firstly, carrying out microstructure regulation and control on a welding surface by adopting a mechanical directional polishing technology, effectively removing a surface oxide layer and forming a uniform rough surface; secondly, accurate management of heat input is achieved through a gradient temperature control strategy, and heat damage to the thin-wall material is avoided; and meanwhile, mutual diffusion of copper atoms and aluminum atoms is promoted by combining a metallurgical transition layer technology, and stable metallurgical bonding is formed. In terms of structural design, a unique positioning system ensures the assembly precision, and the process stability is remarkably improved in cooperation with an optimized welding process. According to the method, the welding quality of the thin aluminum row is improved in a breakthrough mode, meanwhile, the good industrial production adaptability is achieved, and a reliable solution is provided for the connection technology in the fields of power batteries, energy storage equipment and the like.
Owner:GUANGZHOU SUNNYWAY METAL PROD CO LTD
Surface treatment process of hydraulic rod and coating monitoring system
The invention discloses a surface treatment process of a hydraulic rod and a coating monitoring system, relates to the technical field of electroplating, and aims to solve the problems that various complementary sensing technologies cannot be integrated, information such as thickness, uniformity and microstructure cannot be synchronously acquired in a lossless, in-situ and real-time manner, and closed-loop control cannot be formed based on the information in the background technology. According to the scheme, the method comprises the steps that PR electrolytic degreasing is conducted, a workpiece serves as an anode, an oil film is torn through the oxygen evolution effect, an extremely-thin oxidation film possibly existing on the surface of the workpiece is dissolved, base metal is completely activated, and an optimal combination basis is provided for a follow-up coating; and washing with hot water, namely removing residual alkaline degreasing fluid and emulsified oil stains by using hot water with the temperature higher than 60 DEG C in a stirring and spraying manner. According to the method, multi-dimensional information such as the thickness, the uniformity and the microstructure can be synchronously obtained in a lossless, in-situ and real-time mode in the surface treatment process, closed-loop control is formed based on the information, and it is ensured that plating growth is always located on the optimal track.
Owner:LONGGONG FUJIAN HYDRAULIC PRESSURE CO LTD
Preparation method of etching-resistant and wear-resistant Y2O3-AlxOy composite coating
The invention relates to a preparation method of an etching-resistant and wear-resistant Y2O3-AlxOy composite coating. The preparation method comprises the following steps: carrying out ultrasonic cleaning on a corrosion-resistant matrix; performing plasma bombardment cleaning activation on the surface of the corrosion-resistant matrix; a Y2O3 coating and an AlxOy coating are alternately deposited on a corrosion-resistant base body in a double-target magnetron sputtering mode to form the Y2O3-AlxOy composite coating, the sputtering power of a Y target is larger than that of an Al target, and the ratio of x to y in the AlxOy coating is larger than 1. According to the method, the amorphous AlxOy coating dominated by the metal state is introduced into the Y2O3 coating, growth of Y2O3 columnar crystals is continuously broken, crystal grains are refined, formation of intergranular easy-to-etch point locations is inhibited, and an yttrium aluminum oxide composite strengthening phase is formed at an interface, so that plasma etching resistance is improved; the thickness of a single-layer coating in the composite coating is very thin; under the action of growth stress, the structure of the coating presents a wave-shaped microstructure and a soft and hard alternate mechanical structure, and the soft and hard alternate mechanical structure is beneficial to inhibiting generation of transverse cracks, guiding friction crack level expansion, prolonging the friction life of the coating and reducing the wear rate.
Owner:SOUTH CHINA UNIV OF TECH +1
Flexible piezoresistive sensor and preparation method and application thereof
PendingCN121558215AFluid pressure measurement using ohmic-resistance variationForce measurementSand-paperElectronic conductivity
The invention discloses a flexible piezoresistive sensor and a preparation method and application thereof, the flexible piezoresistive sensor comprises an upper layer flexible conductive member, the upper layer flexible conductive member comprises an upper layer flexible substrate and an upper layer conductive layer, one surface of the upper layer flexible substrate is provided with a microstructure formed by sand paper reverse molding, and the upper layer conductive layer is embedded in the surface of the microstructure; the lower-layer flexible conductive member comprises a lower-layer flexible substrate, a lower-layer conductive layer and an elastic conductive layer; the lower-layer flexible substrate is provided with an arc-shaped stripe array microstructure; the elastic conductive layer includes a polymer matrix and a conductive filler dispersed therein. Through the double-gradient design of the gradient conductivity and the gradient structure, the core contradiction that a traditional flexible piezoresistive sensor is difficult to consider high sensitivity and wide linear range at the same time is successfully solved by utilizing the deep coupling and synergistic effect of the conductivity gradient and the structure gradient, and synchronous improvement of the sensitivity and the linear range is realized.
Owner:HUNAN NORMAL UNIVERSITY
Antibacterial ceramic glaze sintering process optimization and intelligent temperature control method and system
The invention provides an antibacterial ceramic glaze sintering process optimization and intelligent temperature control method and system. According to the method, the molecular vibration characteristics of the antibacterial agent at different temperatures are dynamically obtained, and a thermal decomposition dynamic fingerprint database is constructed according to the attenuation law of the molecular vibration characteristics; meanwhile, a three-dimensional temperature field of the glaze layer is reconstructed based on a coupling relation between sound wave propagation parameters and glaze thermal expansion. And carrying out transfer learning on the fingerprint database and historical process data, predicting a glaze thermal stability attenuation parameter, and calculating a temperature gradient and molecular chain fracture compensation coefficient. And fusing the temperature field and the attenuation parameter, and dynamically regulating and controlling the sintering temperature curve and preserving heat by combining the compensation coefficient. The adjusted parameters generate closed-loop feedback by verifying the matching degree of the glaze microstructure and the antibacterial indexes, the compensation coefficient is corrected, and it is ensured that the antibacterial performance of the glaze is stabilized within the process allowance. The temperature control precision and the antibacterial performance stability of antibacterial ceramic glaze sintering are improved.
Owner:ZHEJIANG ENDERUI IND & TRADE CO LTD
Wafer bonding method
PendingCN121269622ADecorative surface effectsDrying solid materials without heatVacuum pressureLiquid water
The invention discloses a wafer bonding method, which comprises the following steps of: 1, providing a first wafer and a second wafer, the surface of the first wafer being provided with a microstructure with a high aspect ratio; step 2, cleaning the first wafer and the second wafer; step 3, performing vacuum drying treatment on the first wafer and the second wafer, wherein the vacuum pressure is controlled to be 0.1-10 Torr in the vacuum drying treatment process; step 4, carrying out pre-bonding on the first wafer and the second wafer to form a bonding body; and step 5, carrying out annealing treatment on the bonding body. Aiming at the problem of residual water in the pre-cleaning process in the bonding process of the micro-structure wafer with a high aspect ratio, the wafer is placed in a controllable vacuum environment, phase change boiling of liquid water under the condition of no heat input is realized, and the problem of high-temperature heat damage caused by an existing heating and baking method is effectively avoided.
Owner:SHANGHAI IND U TECH RES INST
Multi-scale performance evaluation and optimization method and device for well cementation cement stone
PendingCN121026842AWeighing by removing componentMaterial thermal coefficient of expansionThermal dilatationFluorescence
The invention discloses a multi-scale performance evaluation and optimization method and device for well cementation cement stone, and relates to the technical field of oil exploitation, the well cementation cement stone is subjected to nanoindentation test and scanning electron microscope microstructure test, and a mechanical property-microstructure test result is obtained; performing electronic computer tomography and mercury injection test on the well cementation cement stone, and constructing a pore network three-dimensional model; performing triaxial mechanical property test, thermogravimetric analysis and thermal expansion test on the well cementation cement stone to obtain a thermal-mechanical coupling test result; performing X-ray diffraction and X-ray fluorescence spectrum analysis on the well cementation cement stone to obtain mineral phase information and element information of the cement stone; according to the method, a mechanical property-microstructure test result, topological parameters, a thermal-mechanical coupling test result, cement stone mineral phase information and element information are fused, an optimal design scheme for target well conditions is generated, multi-dimensional performance testing and characterization are achieved, and an accurate basis is provided for well cementation cement stone optimal design and quality control.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)
Shield segment heterogeneous modeling crack and limit simulation method
The invention discloses a shield segment heterogeneous modeling crack and limit simulation method. The method comprises the following steps: constructing an aggregate three-dimensional model database; generating a heterogeneous aggregate accumulation model; establishing a concrete shield segment three-dimensional model; defining a model material constitutive relation and a damage criterion; setting an equivalent field staged loading working condition and a boundary condition; grid division and nonlinear static simulation solution are carried out; and constructing a crack response monitoring and output module, and executing judgment of a structure limit state. High-precision construction and multi-stage loading simulation of a shield segment model are realized by reconstructing a concrete microstructure and steel bar arrangement information and combining a field loading force value and a boundary condition; and a nonlinear material constitutive and damage evolution criterion is introduced, the whole-process response of the crack is captured, a limit state criterion is set, and automatic identification and damage form judgment of the bending resistance limit load are completed. According to the method, a technical path capable of being popularized is provided for shield segment structure performance evaluation, ultimate bearing prediction and a crack control strategy.
Owner:CCCC (SHENZHEN) ENG BUREAU CO LTD +1
Bionic anti-drag protective film based on surface micro-nano structure and preparation method of bionic anti-drag protective film
ActiveCN120941788ALiquid surface applicatorsSynthetic resin layered productsPolymer scienceNano structuring
The invention discloses a bionic anti-drag protective film based on a surface micro-nano structure and a preparation method of the bionic anti-drag protective film, and relates to the technical field of anti-drag film preparation. According to the preparation method, the high-strength nitrogen-containing thermoplastic polyurethane film layer with the flame retardant property is prepared, one layer is coated with the hyperbranched polyurethane coating, the drag reduction functional layer with the microstructure is formed through embossing and photo-thermal dual curing, and the hyperbranched polyurethane coating can form a high-density cross-linked network during curing, so that the drag reduction performance is improved; according to the present invention, the hyperbranched polyurethane coating material has characteristics of good mechanical property and good weatherability, the hyperbranched structure can assist in dispersion of shrinkage stress and maintenance of coating surface flatness during heating, and the hyperbranched polyurethane coating material further contains nitrogen rings so as to provide the coating material with certain fire resistance.
Owner:FEILINKE NEW MATERIALS (NANTONG) CO LTD
Ultraviolet aging resistant anti-drag film and preparation process thereof
ActiveCN120963181APolyureas/polyurethane adhesivesSynthetic resin layered productsPolymer scienceAcrylic resin
The invention relates to the technical field of anti-drag films, and particularly discloses an ultraviolet aging resistant anti-drag film and a preparation process thereof.A hindered amine light stabilizer HALs and a silane coupling agent KH-560 are introduced into substrate TPU resin, the strength, heat resistance and aging resistance of the material are enhanced, then an adhesive layer is formed on a substrate film, and the anti-drag film is prepared. A disulfide bond in the adhesive layer has a reversible fracture-self-repairing function, the fatigue resistance of the material is enhanced, the long-term service life of the material is prolonged, the surface layer is acrylic resin formed through copolymerization, the structure comprises a flexible alkyl chain and a siloxane chain segment, a microstructure is formed through hot rolling, the aerodynamic performance is optimized, and the purpose of reducing frictional resistance is achieved.
Owner:FEILINKE NEW MATERIALS (NANTONG) CO LTD +1
Silica gel integrated optical film with 3D light splitting function and manufacturing method thereof
The invention relates to the field of optical display and material engineering, in particular to a silica gel integrated optical film with a 3D light splitting function and a manufacturing method of the silica gel integrated optical film. A silica gel integrated optical film with a 3D light splitting function comprises a transparent optical base material and a microstructure layer, and the microstructure layer is combined on the surface of the transparent optical base material in an integrated forming mode. And the microstructure layer is an anhydrous silica gel-resin composite material obtained by combining organic silica gel with low refractive index and resin with high refractive index through an anhydrous chemical reaction system. The optical film obtained in the invention has excellent interface bonding stability and long-term reliability, the overall thickness of the optical film is small, the optical loss is reduced, the light transmittance is higher, and the overall transmittance can reach 93% or above. And the manufacturing process integration degree and the mold repeated utilization rate are high, the industrial batch production requirement can be met, and the excellent industrial application prospect is achieved.
Owner:深圳市谱维智能科技有限公司
Sulfate-erosion-resistant preparation method of solid waste concrete
The invention discloses an anti-sulfate-attack preparation method of solid waste concrete, and relates to the technical field of building materials and civil engineering, the anti-sulfate-attack solid waste concrete is prepared from the following materials in parts by weight: 100 parts of cement, 30-50 parts of composite solid waste cementing material, fly ash, steel slag micro powder and coal gangue according to a given mass ratio, 60-80 parts of modified recycled aggregate; 0.05-0.1 wt% of sodium molybdate as an erosion inhibitor. According to the invention, solid waste activation-interface reconstruction-ion competition-structure self-healing is taken as a core, synchronous spanning of solid waste concrete in the dimensions of sulfate erosion resistance, resource consumption, construction convenience and the like is realized through multi-process collaboration, and the gelation potential of solid wastes such as fly ash and steel slag is accurately excited through microwave targeted activation, so that the construction efficiency is improved. And a dense microstructure is reconstructed by combining a nano-SiO2 induced crystallization technology, so that excellent mechanical properties are still ensured when the solid waste mixing amount exceeds 70%.
Owner:XINJIANG NORTH CONSTR GRP CO LTD
Preparation method of recrystallized silicon carbide-silicon carbonitride ceramic membrane
The invention belongs to the technical field of nanofiltration, and provides a preparation method of a recrystallized silicon carbide-silicon carbonitride ceramic membrane. The preparation method comprises the following steps: applying a polysilazane solution to a porous substrate for the first time, and then performing first pyrolysis to obtain a pyrolysis material; and applying a polysilazane solution on the pyrolysis material for the second time, and then carrying out second pyrolysis to obtain the recrystallized silicon carbide-silicon carbonitride ceramic membrane. According to the invention, a solution containing propargyl polysilazane or organic polysilazane Durazane 1500 quick-drying resin is used as a precursor to prepare the ceramic membrane, and the ceramic membrane has the advantages of high ceramic yield, excellent high-temperature stability, high retention rate and controllable microstructure, and is suitable for separation and protection application in extreme environments.
Owner:SHENYANG STARLIGHT NEW MATERIAL CO LTD
Visual characterization method, device and equipment for deformation rule of rock microstructure
PendingCN121170129ACharacter and pattern recognitionBiological modelsRock microstructureFeature extraction
The invention provides a visual characterization method, device and equipment for a deformation rule of a rock microstructure, and relates to the technical field of oil-gas exploration. The method comprises the following steps: acquiring scanning grey-scale map data of an internal structure of a rock under different load conditions; establishing a rock three-dimensional digital core model under different load conditions according to the scanned grey-scale map data and the pre-trained neural network; performing pore structure feature extraction processing according to the rock three-dimensional digital core model to obtain rock pore structure feature parameters, and representing a dynamic deformation rule of the rock micro-pore structure along with effective stress loading according to the rock pore structure feature parameters; performing fracture morphological feature extraction processing according to the rock three-dimensional digital core model to obtain a rock fracture morphological feature parameter system, and representing a rock internal fracture morphological deformation evolution rule according to the rock fracture morphological feature parameter system. According to the method provided by the invention, the real rock micro-pore structure is accurately reflected.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)