The invention relates to a preparation method of a nano
silver halide emulsion, which comprises the following steps: S1, fully dissolving deionized water,
sodium bromide, a nucleating aid, a stabilizer and
gelatin in a container with disc type stirring, and uniformly mixing to prepare a primary glue solution; uniformly mixing
silver nitrate with deionized water to prepare a
silver nitrate solution; uniformly mixing
sodium bromide,
potassium iodide and deionized water to prepare a
halogen solution; s2, at a certain temperature, injecting a prepared
silver nitrate solution and a
halogen solution into the primary glue solution at the same time to obtain a mother solution containing nano
silver halide; and S3, desalting the
mother liquor containing the nano
silver halide, supplementing glue, and sensitizing to obtain the nano silver
halide emulsion. The nucleating aid and the stabilizer are added into the
gelatin aqueous solution, the prepared nano silver
halide particles are uniform, stable in storage and free of aggregation, and the
emulsion can be desalted at normal temperature, is low in
energy consumption and high in production efficiency, and is beneficial to
continuous production.