3377 results about "Triazine" patented technology

Provided herein are compounds of Formula (I), or a pharmaceutically acceptable form thereof, and pharmaceutical compositions comprising the same. Also provided herein methods of modulating the activity of cellular targets by administering to a subject a compound of Formula (I), or a pharmaceutically acceptable form thereof. Further provided herein are methods of treating cancer, fibrotic diseases, and inflammatory diseases by administering to a subject a compound of or a pharmaceutically acceptable form thereof.

The invention discloses an OCA optical adhesive and a preparation method thereof, and relates to the technical field of adhesives, and the OCA optical adhesive is prepared from the following raw materials in parts by weight: 35-45 parts of acrylate-terminated hyperbranched organosilicon modified polyurethane, 2-4 parts of allyl succinimido carbonate, 1-3 parts of hexafluorobisphenol A diacrylate, 1-3 parts of 1, 2, 4-trimethyl-1, 3-pentanediol monoisobutyrate, 1-3 parts of 1, 3-pentanediol monoisobutyrate, 1-3 parts of 1, 3-pentanediol monoisobutyrate, 1-3 parts of 1, 3-pentanediol The invention relates to a photocurable adhesive, which is prepared from the following components in parts by weight: 20 to 30 parts of a diluent, 0.6 to 1.2 parts of a photoinitiator, 0.5 to 1 part of an antioxidant and 0.5 to 1 part of a de-foaming agent. The photocurable adhesive is prepared from the following components in parts by weight: 1 to 5 parts of 1, 3-bis (oxiranyl methyl)-5-(2-propenyl)-1, 3, 5-triazine-2, 4, 6 (1H, 3H, 5H)-triketone, 3 to 5 parts of 2, 2 '-bis (trifluoromethyl) diaminodiphenyl, 6 to 8 parts of other polymerizable monomers, 20 to 30 parts of the diluent, 0.6 to 1.2 parts of the photoinitiator, 0.5 to 1 part of the antioxidant and 0.5 to 1 part of the de-foaming agent. The OCA optical adhesive is good in bonding performance, sufficient in weather resistance and environmental protection performance and good in oil resistance.

The invention relates to the technical field of drilling fluids, and discloses a lignite-based modified filtrate reducer for a drilling fluid and a preparation method of the lignite-based modified filtrate reducer. The lignite-based modified filtrate reducer for the drilling fluid is obtained by stirring and mixing the lignite grafted copolymer, the hydroxy propyl cellulose and the graphene oxide, drying and crushing. The steric effect generated by an oxazine ring, a pyridine ring, a triazine ring, a benzene ring and a pyrrole ring grafted into the lignite improves the temperature resistance and salt resistance of the filtrate reducer; the dispersing capacity of clay particles in a drilling fluid system is improved through sulfonic acid hydrated groups, and high-temperature coalescence of drilling fluid clay due to the high-temperature effect is avoided; a sulfonic acid anion group and a quaternary ammonium salt cation group are introduced into the filtrate reducer at the same time, so that the filtrate reducer can form a salt internal bond under the action of electrostatic force, and the salt resistance of the filtrate reducer is improved; the nano silicon dioxide increases the rigidity of the filtrate reducer, so that the filtrate reducer is not easy to curl under the conditions of high temperature and high salt.

The invention relates to the technical field of organic photoelectric materials, in particular to a triazine compound, an OLED with the compound and an organic light-emitting device with the compound. According to the triazine compound disclosed by the invention, a triazine structure is taken as a core, and aryl and alkyl are combined with a fluorenyl group to form side chain matching, so that the compound has excellent luminous efficiency and relatively good thermal stability; meanwhile, when the triazine compound provided by the invention acts on a device, the organic light-emitting device can effectively have lower driving voltage and maintain the stability of the voltage, the light-emitting efficiency is improved, the service life is obviously prolonged, and the triazine compound has a very good application prospect.

The invention relates to a flame-retardant inorganic quick-setting material and a preparation method thereof, and the flame-retardant inorganic quick-setting material is prepared from the following raw materials: sulphoaluminate cement, aluminum-magnesium hydrotalcite, phosphorus slag powder, waste PBO fiber, an accelerator, a water reducer, a functional auxiliary agent, and 3, 3 '-diamino-4, 4'-difluorodiphenyl sulfone. The functional auxiliary agent comprises structural units introduced by the following monomers: 3-[N, N-dimethyl-[2-(2-methylpropyl-2-enoyloxy) ethyl] ammonium] propane-1-sulfonic acid inner salt, diphenyl (4-vinyl phenyl) phosphine oxide, 1, 3-bis (oxirane methyl)-5-(2-allyl)-1, 3, 5-triazine-2, 4, 6 (1H, 3H, 5H)-triketone, 10-(4-vinyl phenyl)-10H-phenoxazine and itaconic acid. The material is high in strength, remarkable in rapid hardening and flame-retardant effect, and safe and environment-friendly to use.

The invention discloses a waterproof anticorrosive coating and a preparation method and application thereof, and relates to the technical field of coatings, and the waterproof anticorrosive coating is prepared from the following raw materials in parts by weight: 30-40 parts of carboxyl-terminated hyperbranched polyester resin, 20-30 parts of carboxyl-terminated functional polyamide, 10-15 parts of hyperbranched polyurethane containing epoxy groups, 15-20 parts of filler, 1-3 parts of (3, 6-diamino acridine-9-yl) boric acid, 1-3 parts of 1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5- the component A is prepared from the following components in parts by weight: 3-5 parts of 2, 3, 5-triglycidyl-S-triazinetrione, 1-2 parts of a coupling agent, 0.8-1.2 parts of a flatting agent and 0.6-1.3 parts of a defoaming agent; the carboxyl-terminated functional polyamide comprises a structural unit introduced by the following monomers: N-(4H-1, 2, 4-triazole-4-yl) diphenylamine-4, 4 '-dicarboxylic acid, and 3, 3'-diamino-4, 4 '-difluorodiphenyl sulfone. The coating is good in waterproof and anti-corrosion performance, high in adhesive force with a base material, sufficient in solvent resistance and aging resistance and long in service life.

The invention discloses a halogen-free flame-retardant TPU (thermoplastic polyurethane) cable material and a preparation method thereof, belongs to the technical field of TPU processing, and aims to solve the technical problem that the wear resistance and flame retardance of a TPU cable material in the prior art need to be further improved. The TPU cable material is prepared from the following raw material components in parts by weight: 80 to 100 parts of polyurethane elastomer, 1 to 2 parts of antioxidant, 1 to 3 parts of stabilizer, 10 to 15 parts of plasticizer, 10 to 20 parts of filler and 5 to 10 parts of flame-retardant glass powder. The TPU cable material is obtained by blending, melting and extruding the polyurethane elastomer, the flame-retardant glass powder and auxiliary materials; during combustion, flame-retardant groups in the polyurethane elastomer and the flame-retardant glass powder are decomposed to promote carbonization of triazine groups in the polyurethane elastomer to obtain a flame-retardant layer, and the TPU cable material is flame-retardant, wear-resistant, stretch-resistant, high-temperature-resistant and more environment-friendly through crosslinking of organic chain segments and synergistic cooperation of functional groups.

The invention relates to the technical field of thickening agents, and discloses a preparation method of a high-temperature-resistant thickening agent for fracturing. According to the preparation method disclosed by the invention, acrylamide, sulfobetaine modified acrylamide and pyrrolidone modified naphthyl melamine are polymerized, so that the thickening agent for high-temperature-resistant fracturing is obtained. A triazine ring structure and naphthyl have high stability, the rigidity of a polyacrylamide molecular chain and the hydrophobic association effect between molecules are enhanced, the high temperature resistance and the salt resistance are improved, and due to the conjugation effect formed by two benzene rings in naphthyl, the thermal stability is further enhanced; by introducing vinyl pyrrolidone, hydrolysis of amido in polyacrylamide can be inhibited, and the temperature resistance and salt resistance of the thickening agent are improved; under a high-salt condition, due to weakening and shielding of mutual attraction of salt ions to anionic and cationic groups in the sulfobetaine, polyacrylamide molecules are more stretched, macroscopically, the viscosity is increased or reduced slightly, and the temperature resistance and salt resistance are improved.

The invention discloses an intelligent continuous pretreatment process for herbicide pesticide wastewater, relates to the technical field of pesticide wastewater pretreatment, and aims to solve the problem of poor removal effect of pesticide residues in wastewater. According to the method, Fenton oxidation, photocatalysis and other processes are accurately selected for different pollutants such as chlorinated organic compounds and triazines, the degradation pertinence is greatly improved, the pollutant removal rate is remarkably increased, all links are seamlessly connected, a pretreatment-deep purification closed loop is formed, the adaptability to complex pesticide wastewater is improved by 40% compared with a single process, and the method is suitable for industrial production. By combining the design of sludge combined treatment, gravity flow sludge discharge and the like, the energy consumption and the operation and maintenance cost are remarkably saved, a multi-stage monitoring and parameter dynamic adjustment mechanism is adopted, the reaction conditions can be timely corrected, the blind feeding of chemicals is reduced, the treatment effect is ensured, the waste of consumables is reduced, and the economic benefit is increased. Compared with the traditional process, the medicament consumption is reduced by more than 30%.

The invention discloses a UV photocureable coating as well as a preparation method and application thereof in automobiles, and relates to the technical field of coatings. When the UV photocureable coating is prepared, 4-aminophenylboronic acid is dehydrated to prepare aminated boron oxygen six-ring; carrying out a reaction on the aminated boroxane and diallyl chlorophosphate to prepare functionalized boroxane; the preparation method comprises the following steps: sequentially reacting graphene oxide with 3-chloropropyltriethoxysilane and 1, 3-diallyl-1, 3, 5-triazine-2, 4, 6-triketone, so as to obtain modified graphene; the preparation method comprises the following steps: reacting epoxy resin with 2-butenal thiosemicarbazone to prepare modified epoxy resin; and uniformly mixing the modified epoxy resin, the epoxy acrylate resin, the modified graphene, the functionalized boroxane, the 1, 6-hexanediol diacrylate and the 1-hydroxycyclohexyl phenyl ketone, so as to obtain the UV photocureable coating. The UV photocureable coating prepared by the invention has excellent flame retardant, self-repairing and mechanical properties.

The invention relates to the technical field of fabrics, and discloses a preparation method of a high-elastic anti-wrinkle blended fabric, which comprises the following steps: adding sodium carbonate, an organosilicon quaternary ammonium salt triazine finishing agent and a cotton / spandex blended fabric into water, soaking, then soaking and rolling twice, washing, and then pre-drying and baking to obtain the high-elastic anti-wrinkle blended fabric. The finishing agent contains cyanuric chloride groups, active chlorine atoms of the cyanuric chloride groups can react with hydroxyl groups of the cotton fabric, so that the finishing agent is connected to the surface of the blended fabric through stable chemical bonds, meanwhile, the finishing agent contains a large number of amido bonds, and the amido bonds and carbamate groups of spandex fabric form hydrogen bond interaction, so that the finishing agent can be used for finishing the cotton fabric. The finishing agent can be firmly attached to the surface of the blended fabric and has good washing resistance, the finishing agent is not prone to falling off after multiple times of washing, and the fabric still has high wrinkle recovery angle, moisture regain and good hand feeling and keeps good wrinkle resistance, hydrophilic performance and soft and elastic hand feeling.

The invention provides a DOPO-HQ-based flame retardant, a preparation method and application thereof, a flame-retardant anti-dripping PET composite material and preparation thereof, and belongs to the technical field of flame retardants. The DOPO-HQ-based flame retardant provided by the invention contains an efficient phosphorus-based flame retardant DOPO structure, so that the composite material can be endowed with efficient flame-retardant self-extinguishing performance; besides, the DOPO-HQ-based flame retardant contains a triazine structure, is high in thermal stability and has excellent high-temperature carbonization capacity, so that a large number of carbon layers are generated in the combustion process of the composite material and cover the surface of a base material, and the effects of molten drop resistance and smoke suppression are achieved. The thermal performance of the flame-retardant PET composite material prepared from the DOPO-HQ-based flame retardant is similar to that of pure PET, and the flame-retardant PET composite material has the characteristics of high flame-retardant efficiency, no halogen, no molten drop, low smoke release amount and the like under the condition of a small addition amount (2-8wt%) (the current commercially available flame-retardant anti-molten drop addition amount is greater than or equal to 15wt%).

The invention discloses a triazine biphenyl compound, a composition, a cured product as well as a preparation method and application of the triazine biphenyl compound, the composition and the cured product. The compound is phenolic resin with a triazine biphenyl structure obtained through condensation polymerization of p-cyanobiphenol; the phenolic resin respectively reacts with an epichlorohydrin compound and an acyl chloride compound to obtain epoxy resin and active ester with a triazine biphenyl structure, and the epoxy resin and the active ester can be self-cured or cured under the action of an imidazole accelerator; in the preparation process, triazine ring (containing nitrogen) is introduced as a node, trifunctional epoxy resin with a rigid aromatic structure as an arm and an active ester curing agent (the same skeleton) are prepared into a thermosetting cross-linked network by adopting a non-polar cross-linking scheme, and a three-dimensional network intrinsic microporous structure is formed through in-situ cross-linking regulation and control of a rigid long-arm branched unit. Further, the bottlenecks of low dielectric property, high temperature resistance, flame retardance and the like are broken through, and the cured material has the characteristics of excellent flame retardance, high temperature resistance and low dielectric property.

The invention discloses sodium alginate hydrogel for extracting pesticide and veterinary drug COFs and application of the sodium alginate hydrogel, and belongs to the field of detection. According to the invention, seven COFs are designed and synthesized, including grafting of different functional groups, different charged properties and different conjugated structures, and then corresponding seven COFs-sodium alginate hydrogel (CACPs) are prepared, and the COFs-sodium alginate hydrogel (CACPs) is used as an extraction material of dSPE to be applied to detection of common pesticide and veterinary drugs. The adsorption capacity of the CACPs on pesticide and veterinary drugs is coordinated and determined by the porous structure properties (specific surface area and pore size) of the CACPs and the inherent structure (conjugate structure size and grafting group) of the loaded COFs. The CACPs prepared from the COFs with large conjugated structures and grafted hydroxyl groups are most beneficial to adsorption of carbamate pesticides; for triazole and triazine pesticides and sulfonamide antibiotics, the CACPs with large specific surface area and medium pore diameter has the best extraction effect; for beta-receptor agonists, the CACPs with a large specific surface area have the best extraction effect.

The invention relates to the technical field of acrylic resin, and discloses green, environment-friendly and high-temperature-resistant acrylic resin for printing ink and a preparation method of the acrylic resin. The acrylic resin for the green, environment-friendly and high-temperature-resistant ink is prepared from the following components in parts by weight: 100 parts of vinyl monomer, 3 to 8 parts of triazinyl styrene monomer, 0.7 to 0.8 part of initiator and 0.5 to 3 parts of zinc salt, a styrene hard monomer structure and a triazine ring are introduced into an acrylic resin molecular chain, so that the pencil hardness, the mechanical property and the high temperature resistance of a paint film are improved. The triazinyl styrene monomer contains an o-hydroxyl Schiff base triazine structure, and has a strong coordination chelation effect with zinc ions, so that the zinc ions can be adsorbed in an acrylic resin molecular chain and are not easy to wash and remove, and a paint film is endowed with excellent antibacterial performance. The obtained acrylic resin has good practical application in the aspect of high-temperature-resistant and antibacterial ink.

The invention discloses a synergistic compound light stabilizer for an automobile coating and a preparation method of the synergistic compound light stabilizer, and belongs to the technical field of coating additives. The light stabilizer comprises the following components in percentage by mass: 30-50% of a hindered amine light stabilizer, 20-40% of an ultraviolet light absorber, 5-15% of surface modified nano cerium dioxide, 5-10% of a hyperbranched polyester anti-migration aid and the balance of a solvent, wherein the ultraviolet light absorber is a mixture of benzotriazole and triazine in a mass ratio of (1: 1)-(1: 3); the particle size of the nano cerium dioxide is 10-50nm, and the surface of the nano cerium dioxide is coated with a silane coupling agent; the preparation method comprises the following steps: modifying the surface of nano cerium dioxide, shearing and dispersing multiple components at a high speed, and adjusting and filtering a solvent; the weather resistance of the automobile coating is remarkably improved and the service life of the automobile coating is remarkably prolonged through the synergistic effect of a plurality of light stabilizing components and the combination of the photocatalytic degradation capability of the nano cerium dioxide and the anti-migration characteristic of the hyperbranched polyester.

The present disclosure provides a method of treating a fatty liver disease (e.g., non-alcoholic steatohepatitis (NASH)) in a human subject (e.g., an adult human subject) in need of such treatment (e.g., NASH / improving liver fibrosis) with 2-(3,5-dichloro-4-((5-isopropyl-6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)-3,5-dioxo-2,3,4,5-tetrahydro-1,2,4-triazine-6-carbonitrile (resmetirom) or a pharmaceutically acceptable salt thereof. The present disclosure also provides a method of improving liver fibrosis in a human subject (e.g., an adult human subject) in need of such treatment (e.g., NASH / improving liver fibrosis) with 2-(3,5-dichloro-4-((5-isopropyl-6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)-3,5-dioxo-2,3,4,5-tetrahydro-1,2,4-triazine-6-carbonitrile (resmetirom) or a pharmaceutically acceptable salt thereof.

The invention discloses a synthesis method of a non-silicon defoaming agent and application of the non-silicon defoaming agent in the field of scandium extraction in hydrometallurgy. The defoaming agent is synthesized by a component A, a component B and a component C through a two-step reaction, the synthesis method comprises the following specific synthesis steps: 1) carrying out esterification reaction on an amino acid substance A and a fatty alcohol substance B to generate an amino ester substance D; and 2) carrying out substitution reaction on the amino ester substance D and a triazine compound C to obtain the non-silicon defoaming agent. The defoaming agent disclosed by the invention is wide in application range, can be applied to links such as a laterite-nickel ore hydrometallurgy front-end scandium extraction method and an MHP hydrometallurgy scandium impurity removal process, is added as an auxiliary agent in the extraction process, and is used for reducing the surface tension of liquid, preventing the formation and enrichment of a third-phase substance and reducing the occurrence of an emulsification phenomenon; the process stability and the output quality are improved, and the method has important industrial application value.

The invention relates to the technical field of preparation of organic photoelectric materials, in particular to an electron transport material, an OLED with the electron transport material and an organic light-emitting device with the electron transport material. According to the electron transport material disclosed by the invention, triazinyl is taken as a framework, phenyl and cyano-substituted biphenyl is taken as a specific substituent group, methyl, adamantyl, phenyl and pyridyl are limited to be matched, and the electron transport material is used as a material for forming an electron transport layer to manufacture an organic electroluminescent device, so that the evaporation process of the device can be smoothly carried out; and the light-emitting efficiency of the organic light-emitting device is effectively improved, and the application prospect is very good.

The invention relates to an anti-yellowing automobile composite film and a preparation method thereof, and belongs to the technical field of high polymer materials. The yellow-resistant automobile composite film is prepared from the following components in parts by weight: 60 to 70 parts of PVC (Polyvinyl Chloride) master batch, 10 to 20 parts of TPU (Thermoplastic Polyurethane) master batch, 1 to 2 parts of plasticizer, 0.5 to 0.8 part of flatting agent, 0.1 to 2 parts of yellowing-resistant modifier and 0.1 to 2 parts of modified flame retardant, sym-triazine cyanuric chloride and a benzotriazole intermediate in the anti-yellowing modifier absorb ultraviolet rays and reduce yellowing of the ultraviolet rays on the composite material, and maleimide groups, maleic anhydride and isocyanurate rings for increasing the crosslinking density cooperate with one another, so that the heat resistance of the material is improved, and the yellowing is reduced; phosphorus and nitrogen main chains of phosphonitrilic chloride trimer in the modified flame retardant have a conjugation effect, so that a protective film is formed, oxygen is isolated, and the phosphonitrilic chloride trimer and nitrogen are synergistically flame-retardant; the anti-yellowing automobile composite film prepared by the invention not only has excellent ultraviolet absorption performance, heat resistance and anti-yellowing effects, but also has a good flame retardant effect.

The invention relates to a preparation method and application of a porous material for preparing methanol through carbon dioxide adsorption and conversion. When the material is prepared, firstly, 4, 4 '4' '-(1, 3, 5-triazine-2, 4, 6-trimethylene) triphenylamine and 1, 2-acenaphthequinone are treated in a mixed solvent containing dioxane / acetonitrile / 6M acetic acid, and AT-COF is obtained; further synthesizing by adopting an impregnation method to obtain IrRu-COF; and finally, uniformly mixing the active gamma-aluminum oxide and the IrRu-COF material to form a carrier dispersion liquid, and then carrying out PEI loading, vacuum impregnation, washing and drying to obtain the PEI functionalized gamma-Al2O3 / COF composite catalyst. The technical closed loop from low-concentration CO2 capture to solar driven conversion is realized, the process flow is simple, and the energy consumption is low.

The invention discloses a chlorine-resistant and acid-resistant composite nanofiltration membrane and a preparation method thereof, and belongs to the technical field of membrane separation. A polyhydric alcohol or / phenol compound monomer containing no less than two hydroxyl groups is subjected to interfacial polymerization with cyanuric chloride, so that a relatively loose network structure can be formed, and selective separation of dye and salt is realized. As a hydrochloric acid (HCl) byproduct can be generated in the reaction process, an alkaline compound is added as an acid-binding agent to neutralize HCl and promote the interfacial polymerization reaction, the formed composite nanofiltration membrane structure does not contain amino groups and polyamide bonds sensitive to active chlorine, the reaction sites of the active chlorine are reduced, and the chlorine-resistant stability of the membrane is good. Meanwhile, the polymer film contains a triazine ring structure, and a formed ether bond has good chemical stability, so that the acid-resistant stability of the film is good. The prepared composite nanofiltration membrane has good nanofiltration separation performance, shows good chlorine-resistant and acid-resistant stability, and can be used for separation of dyes / salts.

The invention relates to the technical field of dispersing agents for ceramics, and discloses a preparation method of a dispersing agent for ceramics, and the novel dispersing agent for ceramics is prepared by taking methoxypolyethylene glycol, bromoacetyl bromide, 4-hydroxyphthalic anhydride, 2, 4, 6-diethanolamine amino-1, 3, 5-s-triazine and the like as raw materials. The polyether polyol contains a plurality of carboxyl groups, has strong interaction with the surface of ceramic powder such as aluminum oxide, has a star-shaped multi-arm polyether molecular chain, can well coat the aluminum oxide powder, can effectively inhibit the growth of crystal nucleus particle size of the aluminum oxide powder, reduces the particle size of the aluminum oxide, and avoids agglomeration and sedimentation of the aluminum oxide; the modified aluminum oxide ceramic powder has good activation degree in solvents such as water, ethanol, dichloromethane or N, N-dimethylformamide and the like, is lower in settling volume and shows excellent dispersing performance.

The invention relates to the field of wear-resistant fabrics, and discloses a high-strength wear-resistant fabric and a preparation method thereof.The high-strength wear-resistant fabric comprises a surface coating and a base cloth layer, the surface coating and the base cloth layer are formed by coating and drying modified waterborne polyurethane emulsion, and the modified waterborne polyurethane emulsion comprises isophorone diisocyanate, ethylene glycol terephthalate, 2, 3, 4-trimethyl-1, 3-pentanediol monoisobutyrate, polyisobutylene glycol monoisobutyrate, according to the present invention, 2, 2-dimethylolpropionic acid, a modified additive, a flame retardant modifier, 1, 4-butanediol, trimethylolpropane and the like are adopted to prepare the modified additive, dopamine is subjected to in-situ auto-polymerization on the surface of a titanium dioxide nanotube, nano-silica is grown on the surface in situ, and modification is performed through a polysiloxane solution to prepare the modified titanium dioxide nanotube flame retardant; the polysiloxane solution is prepared by carrying out a reaction on methyl triethoxysilane and dihydroxyl-terminated polydimethylsiloxane; the flame-retardant modifier is prepared by reacting 2-chloro-4, 6-diamino-1, 3, 5-triazine, 5-hydroxymethylfurfural and phosphorous acid, so that the fabric is endowed with good mechanical properties and wear resistance, and the fabric has a hydrophobic surface and is excellent in flame retardance and durability.

The invention discloses a skin-friendly antibacterial spinning yarn and a preparation method thereof, and relates to the field of spinning yarns. When the skin-friendly antibacterial spinning yarn is prepared, 3-amino-1, 2, 4-triazine and vinyl phosphonyl chloride are subjected to a reaction, and a phosphorus-nitrogen flame-retardant monomer is obtained; activating bamboo nano-cellulose with ammonium ceric nitrate, grafting a phosphorus-nitrogen flame-retardant monomer, and performing electrostatic spinning to obtain modified bamboo nano-cellulose coated fibers; dipping polyester filament yarns in dopamine hydrochloride and sodium hypochlorite in sequence to obtain modified polyester core yarns; the modified bamboo nano-cellulose wrapping fiber and the modified polyester core yarn are twisted through a ring spinning frame and then react with 3, 3 ', 4, 4'-benzophenone tetracarboxylic dianhydride, and the skin-friendly antibacterial spinning yarn is obtained. The skin-friendly antibacterial spinning yarn prepared by the method has excellent skin-friendly antibacterial property, flame retardance, aging resistance and mechanical property.

The invention discloses an efficient wet desulfurization synergist and a preparation method thereof, and relates to the technical field of flue gas desulfurization. The efficient wet desulphurization synergist comprises the following raw materials in parts by weight: 10-20 parts of sodium formate, 5-10 parts of citric acid, 20-30 parts of binary acid, 5-6 parts of a surfactant, 15-20 parts of magnesium salt, 12-18 parts of sodium salt and 2-5 parts of a pH buffer agent. The preparation method comprises the following steps: reacting cyanuric chloride with lauryl amine to generate a monosubstituted compound; then reacting with L-asparaginic acid to generate a disubstituted compound; reacting with diethylenetriamine to generate a bis-triazine ring compound; and finally, reacting with sodium 2-chloroethanesulfonate to generate the surfactant. The high-efficiency wet desulphurization synergist prepared by the invention has a desulphurization effect.

The present application relates to a various novel crystalline forms of 2- [3,5-dichloro -4-(5-isopropyl-6-oxo-1,6-dihydropyridazin-3-yloxy) phenyl]-3,5- dioxo- 2,3,4,5-tetrahydro [1,2,4] triazine-6-carbonitrile represented by the following structural formula-1, which is referred to as Resmetirom. The present application also relates to process for the preparation of various novel crystalline polymorphic forms of compound of formula-1.

The invention discloses an antibacterial and deodorant blended fabric, a preparation method thereof and application of the antibacterial and deodorant blended fabric in underwear, and relates to the technical field of fabrics. When the antibacterial and deodorant blended fabric is prepared, firstly, indolyl polyester is subjected to melt spinning to be prepared into fibers; the preparation method comprises the following steps: reacting fibers, indole and indole-6-formaldehyde, reacting with 4-(aminomethyl)-2, 6-di-tert-butylphenol, and reducing to obtain modified polyester fibers; secondly, the pretreated bamboo fibers react with carbon disulfide and potassium hydroxide; the preparation method comprises the following steps: oxidizing a modified bamboo fiber precursor obtained by reacting the modified bamboo fiber with 1-(2-propenyl)-1, 3, 5-triazine-2, 4, 6 (1H, 3H, 5H)-triketone to obtain a modified bamboo fiber, and oxidizing the modified bamboo fiber precursor to obtain the modified bamboo fiber; the modified polyester fibers and the modified bamboo fibers are blended and woven to obtain fabric, and then the fabric is finished through a finishing agent to obtain the antibacterial and deodorant blended fabric. The antibacterial and deodorant blended fabric prepared by the invention has good antistatic, antibacterial and durable properties.

The invention relates to a K / O co-doped and cyano-grafted graphite phase carbon nitride material as well as a preparation method and application thereof. The material comprises three defect types, namely a C-O-C bond formed by a C-N = C bond in an oxygen substituted triazine skeleton, potassium ions existing between layers and cyano groups generated by protonation of amino groups at the edge. According to the material disclosed by the invention, K ions are doped into the g-C3N4 layer to form K-N bridge connection between layers, the material can be used as an electron channel to effectively accelerate electron migration, cyano groups at the edge have relatively strong electron-withdrawing capability and can be used as sites for adsorbing hydrogen ions, and introduced oxygen can be used as active sites for producing H2O2. The three components cooperate with each other to effectively promote transmission of photo-induced electrons and separation of photo-induced electron hole pairs, so that the photocatalytic effect is remarkably improved, and the photocatalyst is an efficient photocatalyst with excellent performance.

The invention belongs to the field of organic electroluminescence, and discloses an electron transport layer material and a preparation method and application thereof. The structure of the material of the electron transport layer is as shown in a chemical formula I: # imgabs0 #. The compound of the material of the electron transport layer provided by the invention is composed of 9-alkyl-9-phenylfluorenyl, a triazine group and cyano-substituted aryl or heteroaryl, and the groups have high electron affinity to form an efficient electron transport channel; the organic light-emitting material also has good thermal stability, and as an electron transport layer material of an organic electroluminescent device, the organic light-emitting material has the characteristics of low driving voltage, high luminous efficiency and long service life.