208 results about "Triketone" patented technology

The present invention relates to the field of pesticide herbicides, and discloses a herbicide composition and a herbicide containing the herbicide composition, the herbicide composition comprises a component A and a component B, the component A is a triketone compound shown as formula (I), and the component B is at least one selected from the group consisting of triazine herbicides, hydroxybenzonitrile herbicides, triazolinone herbicides, diphenyl ether herbicides, pyridinecarboxylic acid herbicides, phenoxycarboxylic acid herbicides, benzoic acid herbicides, pyridine herbicides, chloroacetamide herbicides, sulfonylurea herbicides, triazolopyrimidine herbicides, bentazone, mesotrione and topramezone. The herbicide composition can broaden the herbicidal spectrum and can improve the controleffect and retard the occurrence of weed drug resistance and anti-drug property.

The invention relates to a phosphor-nitrogen additive type flame retardant 3-(3-DOPO-2-hydroxyl-1-propyl)-triazine triketone (TGIC-DOPO), and belongs to the technical field of preparing flame-retardant epoxy resin materials by adding specific flame-retardant components in common epoxy resin. The cured epoxy resin is prepared by carrying out melt blending on a flame retardant TGIC-DOPO and a bisphenol A diglycidyl ether type resin at a certain temperature, adding an organic solvent to prepare a flame-retardant epoxy resin, adding a curing agent into the flame-retardant epoxy resin, volatizing the organic solvent at a certain temperature and performing a curing reaction of epoxy resin. The epoxy resin disclosed by the invention can be used as a flame-retardant binding material in the field of electronic appliances.

The invention relates to a process for synthesizing triketone herbicide cyclic sulcotrione. The method comprises the following steps: (1) synthesizing 2-chloro-6-methylsulfonyl methylbenzene; (2) synthesizing 2-chloro-3-acetyl-6-methylsulfonyl methylbenzene; (3) synthesizing 2-chloro-3-methyl-4-methylsulfonyl benzoic acid; (4) synthesizing methyl 2-chloro-3-methyl-4-methylsulfonyl benzoate; (5) synthesizing methyl 2-chloro-3-bromomethyl-4-methylsulfonyl benzoate; (6) synthesizing 2-chloro-3-(2,2,2-trifluoroethyoxy)methyl-4-methylsulfonyl benzoic acid; (7) synthesizing 2-chloro-3-(2,2,2-trifluoroethyoxy)methyl-4-methylsulfonyl benzoic acid 3-oxo-1-cyclohexene ester; and (8) synthesizing cyclic sulcotrione. The process disclosed by the invention has the beneficial effects that the reaction steps are reduced, the reaction time is shortened, and the yield of intermediates is improved; the reaction conditions are mild and safe; and the cost is reduced.

A composition comprising a stable anhydrous mixture of an oxidizing agent and an active halogen agent wherein the oxidizing agent is potassium hydrogen peroxymonosulfate and the active halogen agent is an alkali metal salt of dichloro-s-triazinetrione, halogenated dimethylhydantoin, or mixtures thereof, and a method of treating water with such compositions are disclosed.

The invention belongs to the technical field of chemical product synthesis, and relates to a micro-reaction system and method for synthesizing herbicide clethodim. The system is formed by sequentiallyconnecting a micro-channel reactor I, a micro-channel reactor II and a collector in series. The synthesis method comprises the following steps of: by taking an ethanol solution of 5-[2-(ethanethiol)propyl]- 2-propionyl-1, 3-cyclohexanedione (referred to as refined triketone) and chloroallyloxyamine (referred to as chloroamine) as raw materials, respectively and continuously conveying the raw materials into the micro-channel reactor I through a metering pump to realize strong mixing and reaction; and continuing to mix and react the reacted materials in the micro-channel reactor II, controlling the temperature of the system through a heat exchanger, enabling the reaction product to enter the collector, and carrying out acid washing separation to obtain the product clethodim. According to the system and the method, low-energy-consumption, safe and continuous production of clethodim can be realized, the conversion rate of refined triketone is higher than 99% under the condition that themolar ratio of chloramine to refined triketone is 1.20, and the yield of the product clethodim is higher than 95%.

The invention discloses a synthesis method and application of a trialkynyl monomer 1,3,5-tripropargyl-1,3,5-triazine-2,4,6-triketone. The synthesis method comprises: isocyanuric acid and propargyl bromide as raw materials are utilized to synthesize the trialkynyl monomer in the presence of a phase transfer catalyst; and poly 1,3,5-tripropargyl-1,3,5-triazine-2,4,6-triketone is obtained after 1,3,5-tripropargyl-1,3,5-triazine-2,4,6-triketone is cured at high temperature. The synthesis method has the beneficial effects of high safety, low raw material cost and mild reaction conditions, is simple in operation and easy for scale production.