The invention discloses a mesoporous-microporous SBA-15 / HY
molecular sieve and a preparation method thereof.The method comprises the steps that S1, a
nonionic surfactant, inorganic acid and water are mixed to be uniform, a
silicon source is added into the mixture, a
hydrolysis reaction is conducted under the
ultrasonic emulsification condition, and a
solid hydrolysate and
mother liquor are obtained through filtering; s2, uniformly mixing the
mother liquor, a
nonionic surfactant, inorganic acid and water, adding a
silicon source into the mixture, carrying out
hydrolysis reaction under an
ultrasonic emulsification condition, and filtering to obtain a
solid hydrolysate and
mother liquor; s3, repeating the step S2 for 5-20 times, combining all obtained
solid hydrolyzates, and performing hydrothermal
crystallization on the solid hydrolyzates by using mother liquor to obtain a crystallized product; and S4, dissolving the crystallized product in a
hydrochloric acid solution, stirring, adding an HY
molecular sieve, continuously stirring, filtering,
drying, and
roasting to obtain the mesoporous-microporous SBA-15 / HY
molecular sieve. According to the method, the molecular
sieve synthesis efficiency is improved, and the synthesis cost and
pollution are reduced.