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527 results about "Nitrilotriacetic acid" patented technology

Nitrilotriacetic acid (NTA) is the aminopolycarboxylic acid with the formula N(CH₂CO₂H)₃. It is a colourless solid that is used as a chelating agent, which forms coordination compounds with metal ions (chelates) such as Ca²⁺, Co²⁺ , Cu²⁺, and Fe³⁺.

Neutral blockage removing agent composition used for oilfield mechanical recovery well and preparation method thereof

The invention relates to a neutral blockage removing agent composition used for a mechanical recovery well in an oilfield. The neutral blockage removing agent composition is prepared from the following components in parts by weight: 16-20 parts of polyepoxysuccinic acid amine, 7-12 parts of hydroxyethylidene dipllosphate sodium, 21-25 parts of divinyl pentaacetic acid amine, 20-25 parts of hydroxyl ammonium acetate, 12-16 parts of activated attapulgite, 21-25 parts of ammonium persulfate, 9-12 parts ofdicyclohexyl sulfobutanedioate sodium, 7-9 parts of butyl lactate, 0.2-0.3 part of vanadium pentoxide, 5-8 parts of straight chain sodium dodecylbenzenesulfonate, 10-14 parts of nitrilotriacetic acid sodium salt, 4-7 parts of urotropin and 0.1-0.3 part of glycerin fatty acid ester. The neutral blockage removing agent composition is suitable for scale removal and blockage removal of an oil pumping unit well and a screw pump well, can effectively control the reaction speed of the blockage removing agent and the scale of the oil pumping unit well and the scaled screw pump well, and prevent the falling-off of big scale residues to result in the secondary blockage of the mechanical recovery well and an oil recovery pump thereof, has high blockage removal speed, is neutral and is free of corrosion; the waste liquid for blockage removal does not need to be discharged onto the ground to be subjected to sewage treatment, the blockage removal time does not exceed 24 hours, and the effect of safe and corrosion-free blockage removal is achieved.
Owner:GANSU HEIMA PETROCHEM ENG

Deep treatment method for industrial wastewater through natural pyrite catalyzed H2O2 oxidation

The invention relates to a deep treatment method for industrial wastewater through natural pyrite catalyzed H2O2 oxidation. The deep treatment method specifically comprises the following steps: pretreating natural pyrite, adding wastewater into a reactor, adjusting the pH value to be 8-10, adding the pretreated natural pyrite, adding nitrilotriacetic acid, fast stirring, adding a hydrogen peroxide solution, after reaction under stirring, adding a FeCl3 solution to control the mass ratio of pyrite and Fe (III) to be 10:1, adding hydrogen peroxide, continuing the reaction, and standing for precipitation, wherein residual mineral can be recycled; introducing air into supernatant separated through precipitation for secondary oxidation while keeping dissolved oxygen in the water to be above 3ppm, after sufficient aeration, adding polyacrylamide for coagulation treatment, and after standing for precipitation, discharging effluent; carrying out water quality analysis on a treated water sample to assess the treatment effect. By a simple way and various synergistic effects, the deep treatment method provided by the invention changes the generation way of Fenton reaction, significantly increases the reaction reactivity, expands the applicable pH range of the wastewater, improves the utilization efficiency of H2O2, and reduces the cost of technology, thus being an economical and efficient wastewater deep treatment technology.
Owner:TONGJI UNIV

Ultralow-molecular weight intercalation inhibitor and preparation method thereof

The invention relates to an ultralow-molecular weight intercalation inhibitor and a preparation method thereof. The ultralow-molecular weight intercalation inhibitor contains any one or more of amino triethylamine, ethylenediamine tetraethylammonium and diethylenetriamine pentaethylamine and is prepared from the component and clear water in a ratio of 0.5-3%; the amino triethylamine is synthesized from nitrilotriacetic acid; the ethylenediamine tetraethylammonium is synthesized from ethylenediamine tetraacetic acid; and the diethylenetriamine pentaethylamine is synthesized from diethylenetriamine pentaacetic acid; and the preparation method comprises the following steps: adding the raw materials into absolute ethyl alcohol; adding concentrated sulfuric acid for reacting; adding an organic solvent and introducing ammonia water; and stirring and distilling to obtain the product. According to the invention, the inhibition performance of a drilling fluid system can be remarkably improved, the temperature resistance exceeds 240 DEG C, the needs of ultra-deep well drilling are completely met, and the problem of unstable well wall caused by shale hydration and dispersion is effectively reduced; and moreover, the synthesis technology is simple and environment-friendly, the yield is relatively high, the production cost is low, and the ultralow-molecular weight intercalation inhibitor is suitable for industrial production.
Owner:SOUTHWEST PETROLEUM UNIV

Low-foam water-based diamond wire cutting liquid

InactiveCN107011981AReduce stabilityReduce controllabilityLubricant compositionWater basedWire cutting
The invention provides low-foam water-based diamond wire cutting liquid which comprises the following components in percentage by weight: 3-15 percent of low-foam polyether with a molecular weight of 1500-2000, 2-10 percent of polyether modified polysiloxane with a silicone oil molecular weight of 220-20000 and a polyether molecular weight of 500-2000, 0.5-7 percent of an emulsifying agent, 0.5-5 percent of a PH regulating agent, 0.5-5 percent of a complexing agent, 0.2-1.5 percent of an extrusion agent and 70-95 percent of water, wherein the emulsifying agent uses one or more of isodecanol polyoxyethylene ether, iso-tridecanol polyoxyethylene ether, isooctyl alcohol polyoxyethylene ether, glyceryl monostearate, sorbitan polyethylene laurate and sorbitan stearate; the PH regulating agent is organic amine; the complexing agent is one of or a mixture of more of sodium gluconate, potassium gluconate, sodium nitrilotriacetate, sodium citrate, potassium citrate and sodium potassium tartrate; the extrusion agent preferably selects one or several of sodium carbonate, sodium silicate and sodium sulfate. The low-foam water-based diamond wire cutting liquid provided by the invention can realize a lubricating effect, the abrasion resistance, the cooling performance and the like required to be met in the cutting process.
Owner:ZHENJIANG RENDE NEW ENERGY TECH

Bismuth base hydrogen storage material and preparation method thereof

The invention relates to a bismuth base (bismuth selenide, bismuth telluride) hydrogen storage material and a preparation method thereof, relating to low temperature liquid phase synthesis of bismuth base material and the application thereof on hydrogen storage, lithium storage and electrode material. The invention is characterized in that water is taken as solvent, bismuth salts such as bismuth nitrate, bismuth chloride and the like as a bismuth source, and water-soluble tellurium (selenium) acid salts (such as sodium tellurite, selenium substituted sodium sulfate, sodium selenite) or tellurium (selenium) acids (such as orthotelluric acid, tellurous acid and selenous acid) as a tellurium source (selenium) source; proper coordination agents (such as nitrilotriacetic acid, hexamethylene diamine tetraacethyl and the like) and reducing agents (such as vitamin C, sodium borohydride and the like) are added for liquid phase reaction synthesis at the low temperature of 60-80 DEG C. The bismuth selenide crystal grains prepared by the invention take on flower shapes with the sphere diameter of 1-6mum, and the bismuth telluride crystal grains take on sheet shapes with nanometer diameter; the hydrogen storage performance reaches over 100mAh.g. The method has the advantages of cheap raw material, simple technique, convenient operation, easy mass production, etc.
Owner:中国科学院上海硅酸盐研究所苏州研究院

Method for detecting salmonella and staphylococcus aureus in food simultaneously

The invention discloses a method for detecting salmonella and staphylococcus aureus in food simultaneously. The method includes the following steps: 1), diluting a to-be-tested food sample according to GB4789 to obtain sample homogenate of 1:10, adding 50-65wt% of nitrilotriacetic acid solution into the sample homogenate according to the volume ratio of the sample homogenate to the nitrilotriacetic acid solution being (5-7):1, vibrating the mixture, adding phosphate buffer solution or 0.05% tween-20 contained phosphate buffer solution, performing centrifugal layering, and discarding an upper layer; 2), mixing a sample obtained after processing of the step 1) with immunomagnetic beads, vibrating the mixture, subjecting the mixture to standing and layering on a magnetic frame, discarding an upper layer, and washing a lower layer of the sample, wherein the immunomagnetic beads are obtained by modifying salmonella and staphylococcus aureus antibodies, which are labeled by magnetic bead coupled biotin, by streptavidin; 3), adding the phosphate buffer solution to the washed sample, vibrating the mixture, applying the mixture to an LB plate, and performing cultivation and observation. The method is simple and convenient to operate, accurate, efficient and low in cost, two target bacteria are enriched, and detection time can be shorten from 72h to 25h.
Owner:HENAN BUSINESS SCI RES INST

Method for preparing Ni@C or Co@C core-shell nanoparticles

The invention relates to a method for preparing Ni@C or Co@C core-shell nanoparticles. The method comprises the steps: (1) adding nickel chloride or cobalt chloride into an isopropanol aqueous solution, adding nitrilotriacetic acid, and stirring for 1 hour at room temperature, so as to obtain a mixed solution; (2) transferring the mixed solution to a reactor, placing the reactor into an air-blasting drying oven, carrying out heat preservation for 6 hours at the temperature of 180 DEG C, cooling, then, separating a product, cleaning and drying in vacuum, so as to obtain a precursor; (3) putting the precursor into a tubular furnace, heating to the temperature of 500-600 DEG C at the heating rate of 2 DEG C / min, and carrying out heat preservation for 2 hours, thereby obtaining a black product, namely the Ni@C or Co@C core-shell nanoparticles. The method has the advantages that the method is simple in process, low in energy consumption, low in cost and free from environmental pollution, and the in-situ synthesis of the Ni@C or Co@C core-shell nanoparticles is realized; the prepared core-shell nanoparticles have porous structures and are larger in specific surface area and narrower in pore size distribution, thereby being a promising catalyst or energy storage material.
Owner:NANKAI UNIV

Organic solderability preservative (OSP) on surface of printed circuit board and presoaking stoste and method for manufacturing OSP

The invention discloses an organic solderability preservative (OSP) on the surface of a printed circuit board and a presoaking stoste and a presoaking method for manufacturing the OSP. The presoaking stoste for manufacturing the OSP on the surface of the printed circuit board comprises the following components of: 1 to 30 g / L of benzotriazole, 1 to 10 g / L of N-(2-ethoxy)quadrol-N,N',N'-nitrilotriacetic-acid, 5 to 30 g / L of alkaline stabilizer, 1 to 10 g / L of pH buffering agent and 200 to 300 g / L organic solvent. The presoaking method for manufacturing the OSP on the surface of the printed circuit board comprises the following steps of: preparing a presoaking bath solution, adjusting the pH value and forming a nano thin film. The OSP on the surface of the printed circuit board is prepared by presoaking by the presoaking method for manufacturing the OSP on the surface of the printed circuit board, and then forming an OSP film. The presoaking stoste for manufacturing the OSP on the surface of the printed circuit board is high in stability and long in service life; the presoaking method for manufacturing the OSP on the surface of the printed circuit board is simple in process, and the conditions are easy to control; the obtained OSP has high adhesive force and high temperature resistance, and is uniform and compact, so that the solderability of the finished printed circuit board is improved.
Owner:深圳市华傲创表面技术有限公司

High-phosphorus chemical nickel-plating solution

The invention discloses a high-phosphorous chemical nickel-plating solution which comprises a cylinder opening solution and a supplement solution. The cylinder opening solution contains nickel sulfate, sodium hypophosphite, citric acid, lactic acid, sodium acetate, succinic acid, potassium iodate, potassium iodide, nitrilotriacetic acid, cerous sulfate, copper sulfate, benzotriazole, benzimidazole with the concentration being 2-10 mg / L, 5-25 mL / L of OP-10 with the concentration being 5-25 mL / L and the balance pure water. The nickel-plating solution has the advantages that cost is low, the excellent plating ability is achieved, the cylinder opening solution is stable, glossiness is achieved, the magnetism level requirement is met, and the service life reaches 11.0 MTO; during the service life, the average sedimentation rate is 12-14 [mu]m / h, the phosphorus content of a plating layer is 10%-14%, the time for neutral salt spraying is longer than or equal to 96 h (the thickness of the plating layer is 18-25 [mu]m), and the time for a purification resistant nitric-acid test is longer than or equal to 8 min (the thickness of the plating layer is 18-25 [mu]m); the magnetism level is lower than or equals to 200 gamma (specifically, 1 gamma is equal to 1 nT, and in general, remanence in the aerospace field takes gamma as a unit), the western country standard is met, and the magnetism is required to meet the NMB magnetism level; and the plating solution is free of lead and cadmium, conforms to the RoHS command and is an environment-friendly high-phosphorous chemical nickel-plating solution.
Owner:贵阳华科电镀有限公司
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