This invention discloses a high-permeability
cobalt-
bismuth-
nickel micro / nano soft magnetic material and its preparation method. The micro / nano soft magnetic material exhibits high permeability at ultra-high frequencies. The material is
micrometer-scale and chain-like. In this invention, different amounts of
cobalt,
nickel, and
bismuth salts, along with an alkali, are uniformly mixed in a reducing solution environment. A certain amount of complexing agent and surfactant are then added to orderly complex the ions through interaction, modifying the surface of the CoBiNi micro / nano particles. The liquid mixture is gradually heated to 150°C. o C-250 o C,
hydrothermal reaction for 8-24 hours. This invention has the advantages of simple operation and low cost. The prepared micro-nano soft magnetic materials maintain high permeability in the ultra-
high frequency and super-
high frequency bands (1GHz-18GHz). After measurement by a vector network analyzer (VNA), the prepared CoBiNi micro-nano particles still maintain a permeability of over 3.00 at ultra-high frequencies of 16.04GHz-16.86GHz, and can reach a maximum of 4.27, which is dedicated to meeting the high permeability requirements of 5G communication materials at specific frequencies.