22374 results about "Mixed solution" patented technology

A kit and for flushing a medical device a method of preparing the kit is disclosed. The kit includes a container containing a mixed solution a unit dose of a pharmacologically effective amount of an antimicrobial agent and a second agent. The mixed solution has been mixed in a carrier solution and lyophilized. The second agent is an anticoagulant, an antithrombotic agent or a chelating agent. The kit and method are useful for maintaining the patency of indwelling medical devices such as catheters and for preventing infections caused by bacterial growth in catheters.

The invention discloses a method for extracting krill oil with high phosphatide content from Antarctic krills. The method comprises the following steps: (1) drying fresh Antarctic krills to obtain dry Antarctic krills; (2) performing extraction to dry Antarctic krills for 3 times with organic solvent; (3) mixing the extracting solutions, evaporating the mixed extracting solution to obtain Antarctic krill oil with the phosphatide content of 30-35%; then introducing nitrogen or carbon dioxide to remove the residual organic solvent; and adding polar organic solvent in the Antarctic krill oil, mixing evenly, standing to ensure that the mixed solution performs natural layering; and evaporating the lower solution to obtain the Antarctic krill oil with high phosphatide content, and then introducing nitrogen or carbon dioxide to remove the residual polar organic solvent so as to obtain a product. The extraction technology is performed at a low temperature, thus the red color of krill oil can be maintained and the beneficial ingredients in the product can not be damaged. The invention has high extraction efficiency and good phosphatide accumulation effect. Therefore, the Antarctic krill oil with high phosphatide content can be obtained and other byproducts can also be obtained.

The invention discloses a super-hydrophilic and underwater-super-oleophobic oil-water separation mesh membrane, and a preparation method and an application thereof. According to the method, fabric mesh with a specification of 100-300 meshes is subjected to ultrasonic cleaning, and is air-dried under normal temperature; a hydrophilic polymer water-sensitive agent and a cross-linking agent are dissolved in water according to a ratio of 1:9-9:1; the mixture is well mixed by magnetic stirring, such that a solution with a concentration of 1-99% is prepared; nano-sol is prepared with a sol-gel method; the solution and the nano-sol are prepared into a mixed solution with a concentration of 1-99%, and the solution is well dispersed through ultrasonic dispersion; the mesh is soaked in the mixed solution and is vertically lifted, or the mesh is directly sprayed by using a high-pressure spraying gun; and the mesh is bake-dried, such that the super-hydrophilic and underwater-super-oleophobic oil-water separation mesh membrane is obtained. Contact angles of the super-hydrophilic and underwater-super-oleophobic oil-water separation mesh membrane with water and oil in air are both 0 DEG, and the membrane is super-hydrophilic. Under water, the contact angle of the membrane with oil drops is larger than 150 DEG, and the membrane has an oil drop low adhesion characteristic. The mesh membrane provided by the invention can be used in oil-water mixture separation and oil-containing sewage processing.

A method of forming an impurity-introduced layer is disclosed. The method includes at least a step of forming a resist pattern on a principal face of a solid substrate such as a silicon substrate (S27); a step of introducing impurity into the solid substrate through plasma-doping in ion mode (S23), a step of removing a resist (S28), a step of cleaning metal contamination and particles attached to a surface of the solid substrate (S25a); a step of anneal (S26). The step of removing a resist (S28) irradiates the resist with oxygen-plasma or brings mixed solution of sulfuric acid and hydrogen peroxide water, or mixed solution of NH₄OH, H₂O₂ and H₂O into contact with the resist. The step of cleaning (S25a) brings mixed solution of sulfuric acid and hydrogen peroxide water, or mixed solution of NH₄OH, H₂O₂ and H₂O into contact with the principal face of the solid substrate. The step of removing a resist (S28) and the step of cleaning (S25a) can be conducted simultaneously by bringing mixed solution of sulfuric acid and hydrogen peroxide water, or mixed solution of NH₄OH, H₂O₂ and H₂O into contact with the principal face of the solid substrate.

The invention discloses a method for extracting tungsten, titanium and vanadium from a waste SCR (selective catalytic reduction) catalyst, which comprises the following steps: crushing the waste SCR catalyst, adding a strongly alkaline solution, and reacting; filtering, separating, then adding strong acid into the sodium tungstate and sodium vanadate mixed solution, and reacting to obtain tungstic acid and a sodium salt and vanadic acid mixed solution; regulating the pH value of the sodium salt and vanadic acid mixed solution until precipitate is separated out, thus obtaining ammonium vanadate; then adding sulfuric acid into the tungsten-and-vanadium-removed SCR catalyst, and reacting to obtain a titanyl sulfate solution and solids such as aluminum slag and the like; then adding water into the titanyl sulfate solution, and hydrolyzing to obtain titanic acid and a waste acid solution; and finally, respectively calcining the obtained ammonium vanadate, tungstic acid and titanic acid to obtain vanadium pentoxide, tungsten trioxide and titanium dioxide. According to the invention, tungsten, titanium and vanadium can be extracted from the SCR catalyst through the reaction with strong alkali and strong acid at a low temperature, the equipment requirement is low, the energy consumption is low, some products having added values can be coproduced, and no secondary pollution is generated, thereby facilitating popularization and application.

The invention discloses a method for preparing nickel cobalt aluminum serving as a cathodic material of a lithium ion battery, which comprises the following steps of: mixing nickel salt solution and cobalt salt solution uniformly, adding complexing agent solution, precipitant solution and the mixed solution into a reaction kettle with base solution in a parallel flow mode to perform precipitation reaction, performing solid-liquid separation after the reaction is performed fully, and washing; adding the washed solid material into the reaction kettle, dripping aluminum salt solution and the precipitant solution slowly to perform secondary precipitation reaction, so that an aluminum element is precipitated on the surface of the solid material gradually, stirring continuously in the integral process, performing solid-liquid separation after the reaction is finished, and washing and drying the solid material to a precursor of the cathodic material of the lithium ion battery; and mixing the precursor and a lithium source, performing two-section sintering under the condition of introducing oxygen, and crushing the calcined material which is subjected to the two-section sintering and performing subsequent processing to obtain the nickel cobalt aluminum serving as the cathodic material of the lithium ion battery. The method has the advantages of low requirement on equipment, high automation degree, environment friendliness, few wastes, high quality of products and the like and is easy to operate.

The invention discloses a graphene-supported cobaltosic oxide nano composite material and a preparation method thereof. The graphene-supported cobaltosic oxide nano composite material consists of graphene and cobaltosic oxide, wherein the cobaltosic oxide is loaded on graphene nano sheets; the content of the graphene nano sheets is 2 to 95 weight percent, and the thickness of the graphene nano sheets is 0.3 to 50 nanometers; and the particle size of the cobaltosic oxide is 1 to 200 nanometers and the cobaltosic oxide is ball-shaped or flaky. The preparation method comprises: firstly, mixing solution of graphene oxide, a bivalent cobalt salt and a polymer surfactant; and secondly, mixing the solution obtained by the first step with alkaline solution added with an oxidant, stirring the mixed solution or stirring the mixed solution by ultrasonic waves for 0.2 to 5 hours, transferring the mixed solution to a high-temperature reaction kettle, annealing the reaction product at 100 to 250 DEG C for 3 to 30 hours to obtain a product and washing and drying the product to obtain the graphene-supported cobaltosic oxide nano composite material. The size of the cobaltosic oxide is controllable. The reduction of the graphene oxide and the generation of the cobaltosic oxide are accomplished at the same time.

The invention discloses preparation of a multilayer composite membrane for a secondary battery by using an electrostatic spinning coating technology combined with a pore-forming technology, a manufacturing method of the multilayer composite membrane and the secondary battery prepared by using the membrane. The method is characterized by comprising the following steps of: (1) dissolving a high-molecular organic matter into a solvent to form a high-molecular solution; (2) adding a small-molecular organic matter and/or an inorganic nanometer material into the high-molecular solution to ensure that the small-molecular organic matter is dissolved into the high-molecular solution; dispersing an inorganic nanometer material into the high-molecular solution to form an organic/inorganic mixed solution; (3) uniformly coating the formed organic/inorganic mixed solution on at least one side of a film matrix by using the electrostatic spinning coating technology to form a composite film, and drying the composite film; and (4) extracting the small-molecular organic matter from the dried composite film to continuously dry and form the multilayer composite membrane for the secondary battery. By using the method, an inorganic complex of inorganic membranes is realized quickly and conveniently, the ionic conductivity of the lithium ion battery membrane can be improved, and the heat stability and the security of the battery are guaranteed; and the method has the advantages of being simple in operation and convenient for industrialization.

The invention discloses an oxidized grapheme/polyaniline super capacitor composite electrode material and the preparation method and the application thereof. The preparation method comprise the following steps: firstly, adding oxidized graphite to water for ultrasonic dispersion so as to form an oxidized grapheme solution with uniformly dispersed single pieces; at room temperature, dropping aniline to the obtained oxidized grapheme solution for continuous ultrasonic dispersion to from a mixed solution; at a low temperature condition, adding hydrogen peroxide, ferric trichloride and a hydrochloric acid solution dropwise to the mixed solution, and stirring the solution for polymerization; and after the reaction is finished, centrifugating, washing and roasting the obtained mixed solution in vacuum to obtain the oxidized grapheme/polyaniline super capacitor composite electrode material which is used as the electrode material of an electricity storage system of a super capacitor and a battery. The oxidized grapheme/polyaniline super capacitor composite electrode material with good electrochemistry performance is obtained by the method, and the specific capacity of the oxidized grapheme and the polyaniline is greatly improved. In addition, the addition of the oxidized grapheme improves the charge and discharge service life of the polyaniline.

The invention provides a preparation method of ultraviolet-proof antistatic graphene coating textile fabric. The method is characterized by comprising the following steps: adding a graphene solution to a water-soluble polyurethane solution after shaking and dispersing so as to obtain a mixed solution; fully stirring the mixed solution; putting a graphene screening agent solution into a padder immersion tank; processing textile base fabric under room temperature through implementing a two-dipping and two-rolling procedure; padding the graphene screening agent on a textile, putting kinds of textiles on which the graphene screening agent is padded into a high-temperature oven for drying, wherein the temperature of the high-temperature oven is 75-95 DEG C; the high-temperature fixation time lasts for 5-30 minutes, so as to prepare the ultraviolet-proof antistatic graphene coating textile fabric. The method is simple in process, and easy to operate, and the yield is high; the produced textile fabric has the excellent function of preventing ultraviolet rays and static electricity.

The invention discloses a method for removing hydrogen sulfide in a gas phase through oxidization under a high gravity field, which comprises the steps of: enabling a desulfurizing agent to be in a countercurrent or cross current contact with a hydrogen sulfide containing gas in a desulfurizing high gravity machine; and then adding the desulfurizing agent rich in sulphur in a sulphur sedimentation agent and then enabling the desulfurizing agent added with the sulphur sedimentation agent to be in a countercurrent or cross current contact with air in a regeneration high gravity machine, whereinthe desulfurizing agent is a mixed solution consisting of complex iron, aqueous alkali, a sulphur modifying agent and a defoaming agent, and in the mixed solution, the concentration of iron ions is 0.1-10g/L, pH is 8.0-9.2, the concentration of the sulphur modifying agent is 10-200ppm, and the concentration of the defoaming agent is 5-50ppm. The high gravity machine is used for replacing the traditional low-transfer-efficiency reactor, and a high gravity rotary packed bed reactor is adopted during hydrogen sulfide oxidization and catalyst regeneration, thus process transfer efficiency is greatly strengthened, and time of oxidization desulfurization and regeneration of a desulfurizing agent is shortened; in addition, the sedimentation agent is adopted in a sulphur sedimentation stage and acts together with the sulphr modifying agent, thus the sulphur sedimentation time is also greatly shortened.

The invention discloses a high-efficiency graphene/silver phosphate composite visible light photocatalyst and a preparation method thereof, belonging to the technical field of composite materials and environmental management photocatalysis. The preparation method comprises the following steps: dissolving graphene oxide in water, and carrying out ultrasonic treatment to obtain a graphene oxide dispersed liquid; dissolving silver nitrate in deionized water, gradually and dropwisely adding into the graphene oxide dispersed liquid while stirring to obtain a mixed solution, uniformly stirring, and aging; dropwisely adding a prepared disodium hydrogen phosphate or sodium dihydrogen phosphate solution into the graphene oxide-silver nitrate mixed solution, continuing stirring, transferring into a hydrothermal reaction kettle, carrying out hydrothermal reaction, and cooling to room temperature; and washing the reaction product, and carrying out vacuum drying to obtain the visible light photocatalyst. The invention has the advantages of wide material sources and simple preparation process; and the obtained composite material has the advantages of controllable structure and regular pattern, and has high-efficiency degradation effect on organic dyes rhodamine B and methylene blue with certain concentration under the visible light irradiation.

The invention relates to a method of synthesizing nickel cobalt oxide electrode material using a hydrothermal method and an application thereof. The method comprises dissolving CoCl2.6H2O, NiCl2.6H2O and CO(NH2)2 into an appropriate amount of deionized water, wherein the mole ratio of CoCl2.6H2O to NiCl2.6H2O is 1 : 2; uniformly stirring the mixed solution by using a magnetic stirrer, transferring the solution into an autoclave, heating the solution to 100 DEG C and keeping the temperature constant for 10 hours; cooling the solution to room temperature, filtering, washing and drying reactants, and then annealing the reactants for 2 hours in an air atmosphere of 250 DEG C. The method is simple to operate and environmental-friendly. The prepared nickel cobalt oxide nanowire is a spinel-type cubic phase and porous, has high purity and relatively high specific surface area, and can be used as electrode materials for super capacitors, with specific capacitance thereof being 722 F/g.

The embodiment of the invention discloses a preparation method of an ozone oxidation catalyst loaded with polymetallic oxide. The method comprises the following steps that an ozone oxidation catalyst carrier is pretreated, wherein the pretreatment method comprises the steps that the ozone oxidation catalyst carrier is soaked through an acid solution after being washed through water, and then the soaked carrier is washed to be neutral and dried; immersion treatment is conducted on the pretreated ozone oxidation catalyst carrier at least once, and then calcination is conducted; the immersion treatment comprises the steps that the pretreated ozone oxidation catalyst carrier is immersed in an immersion solution to be immersed for 6-48 h at the temperature ranging from 20 DEG C to 100 DEG C, and then drying treatment is conducted, wherein the immersion solution is a mixed solution of nitrate, sulfate and acetate or chloride of three metal elements of manganese, nickel, iron, cerium, cobalt and copper, and the concentration of each metal element in the immersion solution ranges from 0.01 mol/L to 1.00 mol/L. By means of the preparation method of the ozone oxidation catalyst loaded with the polymetallic oxide, the removal rate of chemical oxygen demand (COD) in sewage can be significantly increased.

The invention provides preparation and application of a nitrogen doped graphene fuel cell catalyst, wherein a preparation method of the nitrogen doped graphene fuel cell catalyst is characterized by comprising the following steps: dispersing graphene oxide into a solvent, and carrying out ultrasonic treatment, thereby obtaining a graphene solution; dispersing at least one of non-noble metal salt as well as hydrate thereof and nitrogenous small organic molecules into the solvent, thereby obtaining a mixed solution; dropping the graphene oxide solution into the mixed solution, drying the solvent by distillation, thereby obtaining a nitrogen doped graphene precursor, warming to 600-1000 DEG C under the protection by inert gases, keeping the temperature for 1-4 hours, and cooling naturally, thereby obtaining the doped graphene catalyst. The nitrogen doped graphene preparation process provided by the invention is simple; required raw materials are low in cost, high in yield, can achieve industrial production easily, have very high oxygen reduction catalytic activity, can be applied to the fields of fuel cells, metal-air cells as well as microorganism fuel cells and the like.

The invention discloses an efficiency oil and water separation composition fiber film and a preparation method thereof, and belongs to the field of functional nanometer fiber materials. Hydrophobic polymers such as polyurethane, polystyrene and polymethyl methacrylate or polycaprolactone are used as the main raw materials of the fiber film, the main raw materials are dissolved in an organic solvent to form a polymer solution, hydrophobic nanometer particles are added into the polymer solution in the preparation process, after the mixture is evenly mixed, electro-spinning is conducted on the mixed solution by means of the electrostatic spinning method, and then a fiber film material which is formed by micro-nanometer composite structures and is in the shape of non-woven fabric is obtained. The electro-spun fiber film of the micro-nanometer structure has super-hydrophobic/super-oleophylic property in the air and excellent oil adsorption performance, and the contact angle to oil is nearly zero. The efficient oil and water separation composite fiber film is simple in preparation method, low in energy consumption, high in efficiency, high in oil and water separation speed, and capable of being widely used in the fields such as oily water efficient purification.

The present invention discloses a method for preparing low density silica aerogel under normal pressure. The method comprises: mixing tetraethoxysilane, water and ethanol according to a volume ratio of 1:0.5-19:1-29, adding an acid to adjust the pH value to 3-4, carrying out catalysis hydrolysis, adding an alkali to adjust the pH value to 6-6.5, carrying out catalysis gelating for 8-10 min to obtain a wet gel, aging the wet gel for 6-36 h at a room temperature, adding n-hexane to carry out solvent replacement for 6-36 h, immersing in a trimethylchlorosilane and n-hexane mixed solution to carry out hydrophobic modification for 12-15 h, adopting a n-hexane washing solution to remove the modification solution, placing into a muffle furnace to heat to a temperature of 30-250 DEG C, drying, and finally cooling to a room temperature to obtain the silica aerogel. Test results show that the density of the SiO2 aerogel is 50-80 kg/m<3> and is significantly lower than the density of the SiO2 aerogel prepared under the normal pressure dry condition in most of the public reports.

The invention discloses poly dopamine-modified reduced graphene oxide and a preparation method and application thereof, the polydopamine-modified reduced graphene oxide includes reduced graphene oxide and poly dopamine, and the poly dopamine is attached to the surface of the reduced graphene oxide in physical adsorption manner. The preparation method comprises the following steps: according to the mass ratio of (1-4): (1-4), weighing graphene oxide and dopamine hydrochloride, adding the graphene oxide and the dopamine hydrochloride into solvent to completely dissolve to prepare a mixed solution; adjusting the pH value of the mixed solution to 8.5-9, and reacting for 12h-24h at the temperature of 55 to 65 DEG C to obtain the poly dopamine-modified reduced graphene oxide. The preparation method is friendly to the environment, low in reduction temperature, in no need of adding a stabilizer, and simple in process, realizes the reduction and stabilization in one step, and is suitable for mass production. The invention also provides the application of the poly dopamine-modified reduced graphene oxide.

The invention discloses gel electrolyte, which comprises a polymer matrix material, a non-aqueous solvent and an inorganic filler in a mass ratio of 1:5:0.1-1:20:1 and also comprises electrolyte containing 0.5 to 2.0 mol/L of electrolyte lithium salt. The invention also discloses a preparation method of the gel electrolyte. The preparation method comprises the following steps of: mixing the polymer matrix material, the non-aqueous solvent, the inorganic filler and the electrolyte containing the electrolyte lithium salt in an inert atmosphere, and stirring the mixed solution till dissolving at the temperature of between 40 and 90 DEG C. The invention also discloses an anode and a lithium sulfur battery prepared by using the gel electrolyte. The gel electrolyte provided by the invention has high ionic conductivity, and can avoid the dissolution of the sulfur anode and the reactants; the lithium sulfur battery containing the gel electrolyte has good cycle performance; and the method is simple, does not need a large amount of extracting agent, is safe and environment-friendly, and is favorable for large-scale industrialized production.

A recovery method for copper indium gallium selenide. The method includes firstly using a mixed solution of hydrochloric acid and hydrogen peroxide to dissolve the metal powder containing CIGS. After selenium is separated using hydrazine, copper is replaced by indium metal. Finally, indium and gallium are separated by a supported liquid membrane (SLM) combined with a dispersed stripping solution. The acid used in all the steps of the method is hydrochloric acid, so the copper indium gallium selenium can be separated one by one without the conversion of the solution during the operation, effectively reducing the process time and cost.

The invention relates to a method for preparing a length-controlled silicon nanowire array with a smooth surface, and belongs to the technology of the preparation of nanometer materials. The method comprises the following steps of: firstly, performing wet chemical cleaning on a silicon wafer; secondly, depositing a silver nanometer granular layer on the surface of the silicon wafer in mixed solution containing hydrofluoric acid and silver nitrate by an electroless chemical deposition method; thirdly, performing chemical etching by mixed solution containing the hydrofluoric acid and hydrogen peroxide; and finally, removing silver nanometer granules by using nitric acid to obtain the silicon nanowire array. In the method, length-controlled silicon nanowires with the smooth surfaces are prepared by regulating the concentration and etching time of the hydrogen peroxide serving as an oxidant simply in a chemical etch system, so the technical problem of preparing the silicon nanowires with fewer surface defects in metal-assisted chemical etching is solved.

The invention discloses a novel polymer-based composite and a preparation method of the composite material as well as a method for deep fluorine removal of a water body, belonging to the fields of drinking water and industrial wastewater treatment, and environment function materials. The substrate of the composite is styrene-divinylbenzene copolymerized spheres, and nanometre zirconia hydrate particles are uniformly distributed in the holes of the spheres. The method for deep fluorine removal of the water body comprises the following steps of: (a) filtering fluorine-containing wastewater, and adjusting the pH of a filtrate to 3.0-8.0; (b) passing the filtrate through an adsorption tower in which a novel polymer-based composite material is filled; and (c) stopping adsorption in the case that the concentration of fluorine ions in effluent achieves a leakage point, performing adsorption regeneration on the novel polymer-based composite material in the adsorption tower by virtue of a NaOH-NaCl mixed solution, and then standing for recycling after regeneration. According to the invention, the pre-concentration effect of a polymer substrate and the selective fluorine removal performance of nanometre zirconia hydrate are organically combined, thus the adsorption capacity and the selectivity of the material on fluorine ions are effectively improved.

The invention discloses a preparation method of a lithium-ion secondary battery diaphragm with a crosslinking composite layer. The method comprises the following steps of: performing surface treatment on the polyolefin microporous membrane by using solution of strong oxidant to hydroxylate the surface of the membrane; preparing graft solution containing a grafting monomer, an initiator and a solvent; putting the surface-hydroxylated polyolefin microporous membrane into the graft solution and heating the solution in a water bath; in a protective atmosphere of nitrogen, performing graft polymerization on the surface of microporous membrane; preparing a mixed solution of absolute ethanol and water in a ratio of 9:1; and putting the grafted polyolefin microporous membrane and nano inorganic particles into the mixed solution to allow the nano inorganic particles to react with the polymer grafted on the surface of the diaphragm to form a crosslinked structure. The surface of the polyole finmicroporous membrane is modified or hydroxylated by using solution of strong oxidant. The crosslinked layer bonded to the surface of the diaphragm by chemical bonds can act for a long time, so the surface modification is lasting.

The invention provides a preparation method of an antibacterial nanofiber membrane. The method comprises the procedures of preparation of a nanofiber membrane, preparation of germicide solutions and modification of the nanofiber membrane by the germicide solutions. The method is characterized in that the antibacterial nanofiber membrane is prepared by soaking the nanofiber membrane in the germicide solutions of different concentrations; the nanofiber membrane is formed by being subjected to a polymerization reaction in an organic monomer or a solution of the organic monomer and an inorganic germicide, or is formed by being directly soaked in a polymer solution or a germicide solution of a polymer and an inorganic mixed solution. The preparation method comprises the following steps: step (1), preparing the germicide solutions; step (2), preparing a polymer electrostatic spinning solution and preparing the nanofiber membrane; step (3), modifying the nanofiber membrane by the germicide solutions; an obtained hierarchical-pore nanofiber cross-linked-structure thin film of a core-shell structure is an antibacterial nanofiber membrane finished product.

The invention discloses a preparation method of multi-taste Maotai-flavor white spirit. Eleven flavor types of white spirits are taken as seasoning liquors, the preparation method is characterized by comprising the following steps of: finishing and soaking grains; cooking, gelatinizing and mixing with Luzhou-flavor white spirit fermented grains and Maotai-flavor white spirit fermented grains; spreading out and airing, stirring distiller's yeast, adding Maotai-flavor ending liquor, Luzhou-flavor yellow wine, Maotai-flavor fermented grains and Maotai-flavor yeast, and accumulating and fermenting; fermenting in a cellar, and spraying mixed solution of the Maotai-flavor ending liquor and the Luzhou-flavor yellow wine on the surface of each distilled grain layer; making sand and adding the Luzhou-flavor white spirit fermented grains, cooking and gelatinizing, then adding the Maotai-flavor ending liquor, the Luzhou-flavor yellow wine, the Maotai-flavor fermented grains and the Maotai-flavoryeast, accumulating and fermenting, and storing in the cellar and spraying the mixed solution of the Maotai-flavor ending liquor and the Luzhou-flavor yellow wine on each distilled grain layer; steaming by using a rice steamer to obtain unblended wine in rounds of 1, 2, 3, 4, 5, 6 and 7, and the wine in the seven rounds are combined according to taste and-flavor characteristics, so as to obtain combined Maotai-flavor unblended wine; and then blending the combined unblended wine with flavoring liquor, thus obtaining the multi-taste Maotai-flavor white spirit. The preparation method disclosed by the invention has the advantages of enriching-flavor of Maotai-flavor white spirit, meeting market demand and promoting development of the Maotai-flavor white spirit.

The invention is a mixed solution to wireless resources management and its implementing method, i.e. a solution to manage wireless resources (such as frequency, time gap, code channel, wireless transmission power, etc) and its implementing method, which synthetically uses related techniques of wireless resources management (namely power control, channel allocation, control technique, calling admittance control, self-adapting link, etc) in mobile communication system, according to transmission requirements of various services and estimated result of wireless channel, periodically updating system parameters by a wireless resources management and control device to allocate the wireless resources in the mobile communication system, thus more flexibly and reasonably using the wireless resources and assuring requirements for transmission quality of service (QoS) and increasing system capacity.

The invention discloses an underwater super-oleophobic oil-water separation mesh membrane and a preparation method thereof. The oil-water separation mesh membrane is prepared by coating a micron-thickness chitosan-based polymer coating layer on the mesh wire of a fabric mesh with 100-400 meshes. The oil-water separation mesh membrane is provided with micrometer-scale meshes and the chitosan-based polymer coating layer is provided with protruding structures with a nanoscale width. The preparation method of the oil-water separation mesh membrane comprises the following steps of: (1) cleaning and drying the fabric mesh; (2) dissolving a chitosan-based polymer in acid solution and stirring evenly to obtain mixed solution; (3) immersing the cleaned and dried fabric mesh in the mixed solution, taking out and drying the fabric mesh; and (4) immersing the fabric mesh obtained by the step (3) in alkaline solution, taking out and drying the fabric mesh to obtain the oil-water separation mesh membrane. The oil-water separation mesh membrane provided by the invention has the advantages of large water flux, high oil-water separation speed and good oil-water separation effect, is applicable to treatment of sewage with high oil content, and has good separation effect on normal hexane, petroleum ether, dichloroethane, benzene, animal and vegetable oils and the like.

The invention relates to a multifunctional rare earth metal-organic framework of which the chemical formula is {[Ln(FDA)1.5(DMF)].DMF}n, wherein Ln is Eu or Tb, the FDA is furyl-2,5-dicarboxylic acid, and the DMF is N,N-dimethylformamide; and the rare earth metal framework structure has an Eu<3+>/Tb<3+> ion in a coordination environment, and forms a three-dimensional framework structure containing one-dimensional honeycomb channels. The preparation method comprises the following steps: by using europium nitrate hexahydrate or terbium nitrate hexahydrate as a metal salt, H2FDA as a ligand and DMF as a solvent, stirring the mixed solution, baking, separating and washing the solid to obtain the multifunctional rare earth metal-organic framework. The multifunctional rare earth metal-organic framework provided by the invention has an fluorescent identification function on cancerigenic organic solvents, such as methylbenzene, benzene and acetone, has excellent selective adsorptivity for gas and high acting force with H2, contains high adsorptive enthalpy, and thus, is a multifunctional novel-structure microporous MOF (metal-organic framework) material.

The invention provides a preparation method of a superhydrophobic coating. The preparation method comprises the steps of 1, mixing 50-80 parts of hydrophobic nanoparticle dispersing liquid with the mass percentage of 2-15%, 20-50 parts of polystyrene nanoparticle dispersing liquid with the mass percentage of 1-10% and 0-30 parts of solvent according to the volume part ratio, and ultrasonically dispersing the mixture to obtain a mixed solution; 2, forming the mixed solution on the surface of a substrate and in a microstructure in the substrate; 3, drying the substrate obtained in the step 2, then, raising the temperature to 160-230 DEG C, baking to melt polystyrene nanoparticles, and taking out for naturally airing. The invention also relates to a superhydrophobic paint and the superhydrophobic coating.

The invention provides a microfluidic device and a method for preparing microgel by using the microfluidic device. The method comprises the steps of (1) taking a solution containing live cells or bioactive molecules, a photocuring agent and a hydrogel prepolymer as an internal phase, taking a mixed solution containing oil and an surfactant as an intermediate phase, and taking a polyvinyl alcohol aqueous solution as an external phase; (2) respectively conveying the internal phase, the intermediate phase and the external phase into a corresponding microchannel of the microfluidic device through a micro pump or a micro injector to form a monodispersed water-in-oil-in-water double emulsion; (3) enabling the monodispersed water-in-oil-in-water double emulsion in the step (2) to pass through an output channel of the microfluidic device, and collecting the monodispersed water-in-oil-in-water double emulsion in the step (2) into a collection vessel filled with an aqueous solution, thus obtaining the microgel immobilizing with the live cells or the bioactive molecules. The preparation of the microgel immobilizing with cells by a one-step method is realized, the obtained microgel is controllable in size, and narrow in size distribution, and meanwhile the survival rate of cells is maintained.