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1423 results about "Nickel salt" patented technology

Composition, method of making, and treatment of wood with an injectable wood preservative slurry having biocidal particles

A method of preserving wood includes injecting into the wood an effective amount of a aqueous wood-injectable biocidal slurry, said a wood-injectable biocidal slurry containing dispersants and sub-micron biocidal particles selected from at least one of the following classes: 1) a plurality of particles containing at least 25% by weight of a solid phase of sparingly soluble salts selected from copper salts, nickel salts, tin salts, and/or zinc salts; 2) a plurality of particles containing at least 25% by weight of a solid phase of sparingly soluble metal hydroxides selected from copper hydroxide, nickel hydroxide, tin hydroxide, and/or zinc hydroxide; 3) a plurality of particles containing at least 25% by weight of a solid phase comprising a substantially-insoluble organic biocide selected from triazoles, chlorothalonil, iodo-propynyl butyl carbamate, copper-8-quinolate, fipronil, imidacloprid, bifenthrin, carbaryl, strobulurins, and indoxacarb; 4) a plurality of particles containing on the outer surface thereof a substantially-insoluble organic biocide; 5) a plurality of particles containing a solid phase of a biocidal, partially or fully glassified composition comprising at least one of Zn, B, Cu, and P. The particles may advantageously contain metallic copper, a leachability barrier, pigments, dyes, or other adjuvants disposed on the outer surface thereof.
Owner:OSMOSE

Method for preparing nickel cobalt aluminum serving as cathodic material of lithium ion battery

The invention discloses a method for preparing nickel cobalt aluminum serving as a cathodic material of a lithium ion battery, which comprises the following steps of: mixing nickel salt solution and cobalt salt solution uniformly, adding complexing agent solution, precipitant solution and the mixed solution into a reaction kettle with base solution in a parallel flow mode to perform precipitation reaction, performing solid-liquid separation after the reaction is performed fully, and washing; adding the washed solid material into the reaction kettle, dripping aluminum salt solution and the precipitant solution slowly to perform secondary precipitation reaction, so that an aluminum element is precipitated on the surface of the solid material gradually, stirring continuously in the integral process, performing solid-liquid separation after the reaction is finished, and washing and drying the solid material to a precursor of the cathodic material of the lithium ion battery; and mixing the precursor and a lithium source, performing two-section sintering under the condition of introducing oxygen, and crushing the calcined material which is subjected to the two-section sintering and performing subsequent processing to obtain the nickel cobalt aluminum serving as the cathodic material of the lithium ion battery. The method has the advantages of low requirement on equipment, high automation degree, environment friendliness, few wastes, high quality of products and the like and is easy to operate.
Owner:HUNAN CHANGYUAN LICO CO LTD

Rare-earth doping modified lithium ion battery ternary positive electrode material and preparation method thereof

The invention relates to a rare-earth doping modified lithium ion battery ternary positive electrode material and a preparation method of the rare-earth doping modified lithium ion battery ternary positive electrode material. The chemical general formula of the material is as follows: LiNiaCo<1-a-b>MnbRxO2/M, wherein a is more than 0 and less than 1, b is more than 0 and less than 1, (1-a-b) is more than 0 and less than 1, x is more than 0.005 and less than 0.1, R is one or more of rare-earth lanthanum, cerium, praseodymium and samarium, and M is a composite cladding layer of oxide of aluminum, titanium or magnesium and carbon. The soluble metal nickel salt, cobalt salt, manganese salt and rare-earth compound are mixed to prepare a mixed salt solution, the mixed salt solution is reacted with a mixed alkaline solution prepared by mixing NaOH and ammonium hydroxide, after the reaction solution is filtered, washed and dried, the obtained product is uniformly mixed with lithium salt powder to be ball milled, then the mixture is calcined at the high temperature and coated with the composite cladding layer of the aluminum, titanium or magnesium oxide and carbon, and finally the calcined mixture is calcined at a constant temperature to obtain the rare-earth doping modified lithium ion battery ternary positive electrode material. After doping the rare earth, the metal oxide and carbon composite cladding layer, which are cheap and easy to obtain, are adopted, so that the cycling performance and the rate performance can be improved, and the charging-discharging efficiency of the material also can be improved.
Owner:ZHEJIANG MEIDARUI NEW MATERIAL TECH CO LTD

Modified lithium ion battery ternary positive electrode material and preparation method thereof

The invention relates to a modified lithium ion battery ternary positive electrode material and a preparation method of the modified lithium ion battery ternary positive electrode material. The chemical generation formula of the material is as follows: LiNiaCo<1-a-b>MnbBxO2/TiO2, wherein a is more than 0 and less than 1, b is more than 0 and less than 1, (1-a-b) is more than 0 and less than 1, x is more than 0.005 and less than 0.1, and the TiO2 is a cladding layer. The soluble nickel salt, cobalt salt and manganese salt are prepared into a mixed salt solution, the mixed salt solution is reacted with a mixed alkaline solution prepared by mixing the NaOH and ammonium hydroxide, after being filtered, washed and dried, the reaction product is mixed with a boronic compound and roasted for 4h to 12h at the temperature of 300 to 800 DEG C under an air atmosphere, then the roasted product is ball milled with the lithium salt to be uniformly mixed together, the mixture is coated with titanium dioxide after being calcined at the high temperature to obtain the modified lithium ion battery ternary positive electrode material. The prepared boron doping modified ternary positive electrode material is high in specific capacity and good in cycling performance.
Owner:ZHEJIANG MEIDARUI NEW MATERIAL TECH CO LTD

Preparation method of high density nickel cobalt lithium manganate positive electrode material

The invention discloses a preparation method of a high density nickel cobalt lithium manganate positive electrode material, LiNixCoyMnzO2. The preparation method comprises the following steps: firstly, mixing a nickel salt solution, a cobalt salt solution and a manganese salt solution according to a certain mol ratio, adding the mixed solution, a complexing agent solution and a precipitant solution together to a stirring reaction kettle with a base solution, fully reacting, carrying out solid-liquid separation, and washing and drying to obtain a globular nickel cobalt manganese oxyhydroxide precursor; calcining the precursor at the temperature of 350-900 DEG C for 2-20 hours to obtain a globular nickel cobalt manganese oxide precursor, and smashing the globular nickel cobalt manganese oxide precursor at high speed to obtain a mono-crystalline nickel cobalt manganese oxide precursor; mixing a lithium source and the mono-crystalline precursor according to a certain mol ratio, calcining at the temperature of 700-980 DEG C for 2-20 hours, and smashing and classing to obtain the mono-crystalline nickel cobalt lithium manganate positive electrode material. The preparation method provided by the invention has the advantages that the compacted density of the prepared nickel cobalt lithium manganate material is large, the specific capacity is high, the rate property and consistency are good, the preparation method is simple, and the preparation process is easy to control and operate.
Owner:HUNAN SOUNDDON NEW ENERGY

Method for preparing lithium-enriched lithium manganese oxide solid solution cathode material

ActiveCN102544475AFlexible adjustment ratioHomogeneous coprecipitationCell electrodesOXALIC ACID DIHYDRATENickel salt
The invention relates to a method for preparing a lithium-enriched lithium manganese oxide solid solution cathode material. The method comprises the following steps of: adding a mixed aqueous solution of nickel salt, cobalt salt and manganese salt into an oxalic acid or oxalate aqueous solution by an oxalate coprecipitation high-temperature solid state method, and stirring and reacting to generate nickel, cobalt and manganese oxalate coprecipitation; performing solid and liquid separation, washing and drying to obtain a nickel, cobalt and manganese oxalate precursor; and mixing and grinding the precursor and lithium salt, drying, baking at high temperature in an air atmosphere, and thus obtaining the lithium-enriched lithium manganese oxide solid solution cathode material. During preparation of the precursor, the proportion of the nickel salt, the cobalt salt and the manganese salt is adjusted, so that the constituents of the lithium-enriched lithium manganese oxide solid solution cathode material can be adjusted flexibly. The preparation method is suitable for large-scale, economic, stable and reliable production of the lithium-enriched lithium manganese oxide solid solution cathode material, has obvious advantages, and is high in practical value.
Owner:HUBEI WANRUN NEW ENERGY TECH DEV

Preparing method of lithium ionic cell 5V anode material spherical LiNi*Mn*O*

The invention relates to a preparation method of 5V level anode material of a lithium ion battery, namely, ball LiNi0.5Mn1.5O4, and pertains to the energy material and novel material preparation technology field. The method includes the steps that: a liquid mixture of manganese salt and nickel salt which is prepared according to a molar ration of 3:1, reacts with dissoluble carbonate or bicarbonate water solution and ammonia or ethylene diamine water solution to obtain ball MnCO3-NiCO3, processes of centrifugal separation, washing and drying are carried out, ball Mn2O3-Ni2O3 powder is obtained by heat treatment at 400 DEG C to 600 DEG C, the ball Mn2O3-Ni2O3 powder is mixed with lithium salt compound, ball LiNi0.5Mn1.5O4 is obtained by heat treatment at 700 DEG C to 900 DEG C. The LiNi0.5Mn1.5O4 anode material obtained by the method has high purity and relatively high specific capacity; the product grain is a ball shape, with high tap density which can reach 2.2 to 2.5 g question mark cm <-3>; the ball grain can provide a beneficial condition to the further carrying out of surface coating and to the improvement of the cycle stability of the material, and has great practical value in the field of high energy density and high power lithium ion battery.
Owner:TSINGHUA UNIV

High-activity amorphous silica-alumina, hydrocracking catalyst supported by amorphous silica-alumina, and preparation methods thereof

The invention discloses a high-activity amorphous silica-alumina, a hydrocracking catalyst supported by amorphous silica-alumina, and preparation methods thereof. The preparation method of the amorphous silica-alumina supporter comprises the following steps: preparing a silicon source-aluminum source mixed water solution, mixing the mixed water solution with a precipitant solution, carrying out cocurrent flow coprecipitation to obtain a precipitated slurry, transferring the slurry into a closed vessel, aging, molding, and roasting. The invention also provides a preparation method of a hydrocracking catalyst by using the amorphous silica-alumina as the supporter. The preparation method of the hydrocracking catalyst is as follows: in the preparation method of the amorphous silica-alumina supporter, a nickel salt or nickel salt and metal aid M salt is/are added into the silicon source-aluminum source mixed water solution in the step (1), and the rest steps are the same as those in the preparation method of the amorphous silica-alumina supporter. The coprecipitation process is adopted in the preparation process, and the silicon source and aluminum source finally exist in the catalyst in the form of the amorphous silica-alumina, but the catalyst has much higher activity than the common amorphous silica-alumina catalyst.
Owner:SYNFUELS CHINA TECH CO LTD

Preparation method of magnetic-alloy-loaded porous carbon sphere composite wave-absorbing material

The invention relates to a preparation method of a magnetic-alloy-loaded porous carbon sphere composite wave-absorbing material. The method comprises the following steps: 1) preparing a precursor solution containing two or more magnetic metal ion salts; 2) stirring the porous carbon spheres in the precursor solution for impregnation; 3) filtering out the porous carbon spheres, washing and drying; 4) calcining the dried porous carbon spheres in an inert atmosphere; and 5) cooling to room temperature in an inert atmosphere to obtain the magnetic-alloy-loaded porous carbon sphere composite wave-absorbing material. The iron salt/cobalt salt, iron salt/nickel salt and cobalt salt/nickel salt mixed precursor solution are introduced to the inside of the ducts of the carbon spheres by using the high specific area and strong adsorptivity of the porous carbon spheres through the capillary actions and are combined with the hydrophilic oxygen-containing functional group; and finally, the drying and sintering treatment in the inert atmosphere are performed to obtain the iron-cobalt/iron-nickel/cobalt-nickel-alloy-loaded porous carbon sphere composite material. The whole preparation process is simple in technique and convenient to operate, and has low requirements for the production equipment.
Owner:XI'AN INST OF OPTICS & FINE MECHANICS - CHINESE ACAD OF SCI

Modified nickel-cobalt lithium aluminate positive electrode material and preparation method thereof

The invention relates to a modified nickel-cobalt lithium aluminate positive electrode material and a preparation method of the material. The chemical general formula of the material is LiNi(1-a-b)CoaAlbO2/TiO2, wherein a is greater than 0.1 and less than 0.3; b is greater than 0.01 and less than 0.2; 1-a-b is greater than 0 and less than 1; the TiO2 layer is a coating layer; the preparation method of the material comprises the following steps: preparing soluble metal nickel salt, cobalt salt and aluminium salt into a mixed salt solution, preparing the mixed salt solution, NaOH and ammonia water into a mixed alkali solution for reacting, filtering, washing, drying and then roasting the mixed alkali solution for 5-10 hours at the temperature of 400-600 DEG C in the oxygen atmosphere, then carrying out ball milling and uniformly mixing with lithium salt, roasting the mixed alkali solution for 6-16 hours at the high temperature of 800-1000 DEG C in the oxygen atmosphere, coating the mixed alkali solution by titanium dioxide to prepare the modified nickel-cobalt lithium aluminate positive electrode material. The prepared modified ternary positive electrode material of the lithium ion battery is good in electrochemical performance; the dry coating process is free of waste liquid and high-temperature sintering, so that the energy consumption and the cost are reduced.
Owner:ZHEJIANG MEIDARUI NEW MATERIAL TECH CO LTD

Nickel oxide nano rod array material, method for preparing same and application thereof

The invention discloses a nickel oxide nano rod array material, a method for preparing the same and application thereof, and belongs to the technical field of inorganic advanced nano materials. The nickel oxide nano rods are vertically and orderly grown on the nickel foam substrate, and the nickel oxide nano rods are 100 to 800 nanometers long and 5 to 30 nanometers wide. The preparation method comprises the following steps of: putting the nickel foam substrate in concentrated hydrochloric acid, deionized water and ethanol for ultrasonic cleaning respectively; dissolving soluble nickel salt and urea in deionized water to obtain clear solution; obliquely putting the nickel foam substrate in a reaction kettle, and moving the clear solution to the reaction kettle for hydrothermal reaction, and after reaction, using the cooling water to cool the reaction kettle to the room temperature; taking the nickel foam substrate out of the reaction kettle, and cleaning the nickel foam substrate withwater and ethanol; and drying the product in an oven, and calcining the dried product. The one-piece product has a very big capacitance value which can be well kept even under high current density and is high in cycle performance, so that the product is a super capacitor material with a great application prospect.
Owner:BEIJING UNIV OF CHEM TECH

Preparation method of lithium-ion battery positive electrode material spherical nickel-cobalt-lithium aluminate

ActiveCN103296263AGuaranteed spherificationHigh tap densityCell electrodesNickel saltReaction temperature
The invention discloses a preparation method of lithium-ion battery positive electrode material spherical nickel-cobalt-lithium aluminate. The preparation method comprises the following steps of: firstly dissolving aluminum salt in deionized water, and preparing AlOOH aluminum sol by adding HNO3 or ammonium hydroxide and nitric acid; preparing nickel salt and cobalt salt into uniform aqueous solution according to a certain ratio; enabling the mixed salt solution to be collectively reacted with the aluminum sol and a mixed alkali solution, adjusting the pH value to be 9 to 12, controlling the reaction temperature, carrying out the solid-liquid separation after 20 to 30h of the reaction, and washing, filtering and drying the reaction product to obtain spherical nickel-cobalt-aluminum hydroxide precursor powder; then mixing the spherical nickel-cobalt-aluminum hydroxide precursor powder with lithium, sintering the mixture, and pulverizing and grading sintered material to obtain the lithium-ion battery positive electrode material spherical nickel-cobalt-lithium aluminate. The prepared spherical nickel-cobalt-lithium aluminate particles are controllable in shape and granularity, high in compacting density, high in specific discharge capacity, good in cycling stability and low in cost.
Owner:山东天骄新能源有限公司
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