9202results about How to "Uniform particle size" patented technology

A sintered polycrystalline diamond material (PCD) of extremely fine grain size is manufactured by sintering a diamond powder with pre-blended catalyst metal under high pressure/high temperature (HP/HT) processing. The PCD material has an average sintered diamond grain structure of less than 1.0 μm.

The invention relates to a synthesis method of fine grain ZSM-5 zeolite molecular sieve with high silicon aluminium ratio, which comprises using a surface active agent, charging it into acidified aluminium salt solution, then slowly dropping alkaline solution formed from sodium silicate, template agent and seed crystal into aluminium saline solution, the overall composition of the obtained reaction mixture being Na2O:Al2O3:SiO2:H2O=1.5-4.0:1:20-280:500-2000 by mol ratio, then subjecting the reaction mixture to thermal crystallization through the conventional method.

The present invention provides a nano-micellar preparation containing vinca alkaloids antitumor agent for intravenous injection, which cincludes a therapeutically effective amount of vinca alkaloids antitumor agent (vinblastine, vincristine, vindesine and vinorelbine), a phosphatide derivatized with polyethylene glycol, together with pharmaceutically acceptable adjuvants. The preparation is prepared by encapsulating the medicament with a nano-micelle to obtain the nano-micellar preparation containing vinca alkaloids antitumor agent for injection. The vinca alkaloids antitumor agent and the phosphatide derivatized with polyethylene glycol form a nano-micelle with a highly uniform particle size. In the micelle, the hydrophobic core of encapsulated medicament is surrounded by polyethylene glycol molecules to form a hydrophilic protective layer, so that the medicament is prevented from contacting with the enzymes and other protein molecules in blood and being recognized and phagocytozed by reticuloendothelial system in body, and the circulation time in vivo of the micelle is prolonged.

The present invention provides a method for forming an electrode of a flat panel display device using ink for ink jet printing and an ink jet printer. The ink for ink jet printing is prepared by a method comprising the first step of contacting the vapor of a metal with the vapor of the first solvent, according to the vapor phase-evaporation technique, to thus give a dispersion of metal ultrafine particles; the second step of adding a low molecular weight polar solvent as the second solvent to the dispersion prepared in the first step to thus precipitate the metal ultrafine particles and removing the first solvent; and the third step of adding the third solvent to the precipitates thus prepared to carry out the solvent substitution and to give a dispersion of independently dispersed metal ultrafine particles, and prepared by adding a dispersant in or during the foregoing first and/or third steps, and the ink for ink jet printing consists of a dispersion excellent in ink characteristic properties. In the dispersion, metal ultrafine particles having a particle size of not more than 100 nm are independently and uniformly dispersed. The electrodes of FPD devices are formed using this ink for ink jet printing.

The invention discloses a material for rapid three dimensional printing forming and a preparation method thereof. The material comprises a modifying powder material A and bonding agent B, wherein preparation method of the modifying powder material A comprises the following steps: adding powder material and a first solvent into a ball mill or grinding mill, and milling to obtain a pretreated powder material; adding surfactant, lubricant and organic resin into a second solvent in sequence, and stirring and dispersing for 2-3 hours to obtain modifying solution; mixing the pretreated powder material and the modifying solution, adding into the grinding mill, mixing and milling at normal temperature, drying, grinding, and pulverizing to obtain the modifying powder material A. When in use, one weight part of the modifying powder material A and 0.01-0.07 weight parts of the bonding agent B are blended. The material provided by the invention is used as the raw material for a rapid three dimensional printing forming machine, and can be used for effective rapid forming on different types of three dimensional printing machines.

The invention relates to a polymer nanomicrosphere product with uniform and controllable size and a preparation method thereof. The preparation method comprises the following steps: preparing polymerizable olefine monomers, an initiator, assistants and the like into an oil phase, and preparing water, a stabilizer, an emulsifier and the like into a water phase; and mixing the oil phase and water phase into an O/W pre-emulsion, quickly passing the pre-emulsion through a uniform-pore-size microporous membrane under pressure to form a uniform-particle-size O/W emulsion, and polymerizing and curing emulsion droplets in the emulsion into the uniform-particle-size polymer nanomicrospheres. The average particle size of the microspheres can be controlled within the range of tens of nanometers to 50 micrometers, and the particle size distribution coefficient C.V. is smaller than 20%. The method has the advantages of simple steps, favorable batch repetitiveness, uniform and controllable particle size, no need of subsequent screening and the like, is easy to control, can easily implement large-scale production, and therefore, has the characteristics of fewer emissions and low preparation cost.

Disclosed herein is a method for manufacturing metal sulfide nanocrystals using a thiol compound as a sulfur precursor. The method comprises reacting the thiol compound and a metal precursor in a solvent to grow metal sulfide crystals to the nanometer-scale level. Further disclosed is a method for manufacturing metal sulfide nanocrystals with a core-shell structure by reacting a metal precursor and a thiol compound in a solvent to grow a metal sulfide layer on the surface of a core. The metal sulfide nanocrystals prepared by these methods can have a uniform particle size at the nanometer-scale level, selective and desired crystal structures, and various shapes.

The invention provides a method for preparing nanosilver powder in batches, belonging to the field of nano-material preparation. Nanosilver particles are synthetized in two steps, at first, a low-concentration reducing agent solution is slowly added into a solution mixed with silver salt, a protective agent, and a pH conditioning agent drop by drop, and then a high-concentration reducing agent solution is rapidly added drop by drop to obtain a nanosilver mixed solution; impurities in the nanosilver mixed solution are removed through a membrane separation device to obtain a nanosilver dispersion liquid; and at the end, absolute ethyl alcohol and a high-molecular dispersant are added into the nanosilver dispersion liquid, and spray drying is carried out by a spray drying device to obtain nanosilver powder in a certain particle size. The particle size of the prepared nanosilver powder is controllable, the batches are stable, the problems of non-uniform particle size during the synthesis of nanosilver, nanosilver separation, and agglomeration and acaking during powder preparation are solved, the preparation process and the operation are simple, and industrial and batches production is realized.

The invention provides a method for extracting carbon quantum dots from activated carbon, which comprises the following steps of: adding dry activated carbon powder to salpeter solution and stirring for backflow; performing reduced pressure distillation for evaporating suspension obtained by backflow to dryness; dispersing obtained black solids in water, and neutralizing obtained solution with sodium hydroxide; and finally, centrifugating neutralized black suspension for removing precipitation, separating supernatant fluid by using an ultrafiltration centrifugal tube or an ultrafiltration membrane, collecting filtrate, and drying the filtrate to obtain carbon quantum dots. The method uses cheap and available activated carbon as carbon sources, and can obtain a large number of carbon quantum dots by simple chemical oxidation process and simple subsequent processes of evaporation, saturation, centrifugation and ultrafiltration. The carbon quantum dots are graphite structure nanocrystals with the grain diameter of 3 to 5 nm, the surfaces of which have a large amount of hydroxide radicals. The carbon quantum dots have good fluorescence and electrochemiluminescence.

A method of forming a component from a gamma prime precipitation-strengthened nickel-base superalloy. The method entails formulating the superalloy to have a sufficiently high carbon content and forging the superalloy at sufficiently high local strain rates so that, following a supersolvus heat treatment, the component is characterized by a fine and substantially uniform grain size distribution, preferably finer than ASTM 7 and more preferably in a range of about ASTM 8 to 10.

The invention relates to a method for preparing nano iron phosphate, belonging to the technical field of the preparation of lithium ion battery cathode materials. The method is characterized by comprising the following steps: inputting an alkaline aqueous solution and a mixed solution formed by one of phosphoric acid or a soluble phosphate solution, one of a water-soluble ferrous salt solution and an oxidant or a ferric salt solution and a water-soluble dispersing agent into a rotating packed bed layer by a metering pump at a certain feeding speed; regulating the rotating speed of the rotating packed bed and controlling the pH value of the reaction system by an alkaline solution; discharging nano iron phosphate particles generated by reaction crystallization from a discharge hole of the rotating packed bed along with the mixed solution; and filtering, washing and drying the nano iron phosphate particles to obtain nano iron phosphate (FePO4.2H2O) powder. The method is simple and has easy operation and high efficiency, and the prepared iron phosphate reaches the nano grade, has uniform particle size and narrow distribution range and is suitable for industrialized production. The nano iron phosphate is a good precursor material for preparing lithium iron phosphate which is used as a cathode material of high-power type lithium ion batteries.

The invention belongs to the technical field of materials and discloses a flexible low-smoke halogen-free flame-retardant wire and cable material and a preparation method thereof. The wire and cable material is prepared by using the following raw materials in parts by weight: 100 parts of ethylene-vinyl acetate copolymer, 1 to 70 parts of polyethylene, 30 to 100 parts of flame retardant, 5 to 20 parts of smoke suppressor, 0.1 to 5 parts of coupling agent, 1 to 20 parts of plasticizer, 0.1 to 10 parts of crosslinking agent, 3 to 15 parts of lubricant and 0.1 to 1 part of antioxidant. The wire and cable material disclosed by the invention is a thermoplastic sulfurized elastomer material, can be used for preparing insulating layers and sheath layers of wires and cables, and has the characteristics that no halogen is contained, the flame-retardant effect is good, the smoking amount is low, the surfaces of the insulating layers and sheath layers are smooth and do not stick with one another, the flexibility is good, the mechanical strength is high, the wear resistance is good, the processing fluidity is good, the process is simple and the material can be recycled.

The invention discloses a preparation method and application in the luminescent element thereof of CuInS2-ZnS/ZnSe/ZnS semiconductor quantum dots with a core-shell structure, belonging to the technical field of the preparation method of the semiconductor quantum dot. The method comprises the following steps: dissolving the precursors of copper source, zinc source, indium source and sulfur source in nonpolar mixed solvent to perform nucleation and growth under a certain temperature and obtain a CuInS2-ZnS alloy core-ZCIS, then adding zinc source and selenium source alternately in the solution to perform epitaxial growth of ZnSe on the core, then perform epitaxial growth of ZnS to prepare the CuInS2-ZnS/ZnSe/ZnS quantum dots, finally adding polar solvent in the solution, settling, centrifuging, cleaning, and perform vacuum drying to obtain solid quantum dot powder. The prepared quantum dots are 2-8nm and have uniform particle size, controllable emission wavelength and high yield. The quantum dots are used as luminescent material to prepare red, yellow and green quantum dot luminescent elements and the luminescent elements have excellent luminescent property.

The invention relates to a method for preparing spherical aluminum-doped nickel lithium carbonate for a lithium ion battery positive electrode material by combining liquid phase oxidation and crystallization controlling. Through controlling of the preparation technique, firstly synthesizing a spherical hydroxyl oxygenized nickel cobalt aluminum precursor with high density, and then calcining at the temperature of 500-800 DEG C for 10-24 hours in a flow oxygen gas atmosphere after mixing the precursor with a lithium source, thus acquire the spherical aluminum-doped nickel lithium carbonate with high density. The synthesized aluminum-doped nickel lithium carbonate is in a single spherical shape, has good stacking density, and can be used for improving the volume ratio capacity of a battery.The aluminum-doped nickel lithium carbonate prepared by the method in the invention has the advantages of high specific capacity and good loop stability. The method provided by the invention has the advantages of simple technique, low cost, less pollution, good product performance and suitability for industrialized production.

The invention relates to the field of silicon wafer wire-electrode cutting and discloses a method for recycling carborundum and cutting polyethyleneglycol in waste mortar by silicon wafer wire-electrode cutting. In monocrystalline silicon piece processing technique, a viscosity reduction agent is firstly added before waste mortar linear cutting, and then a suspending liquid part and a solid particles part are obtained by the solid-liquid separation; The suspending liquid part is added with a filter aid, then filter pressing with a plate frame, micro porous filtration, hyper filtration with hollow fiber and ion exchange are carried out sequentially, and finally, the suspending liquid is distillated in vacuum and polyethyleneglycol is recycled. Alkali reaction cleaning, water scrubber washing, centrifugalization, acid reaction cleaning, the second water scrubber washing, the second centrifugalization, the second acid reaction cleaning, drying and drying classification are carried out on the solid particles in sequence, and finally, recyclable silicon carbide particles are obtained.