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7019 results about "Acrylamide" patented technology

Acrylamide (or acrylic amide) is an organic compound with the chemical formula CH₂=CHC(O)NH₂. It is a white odorless solid, soluble in water and several organic solvents. It is produced industrially as a precursor to polyacrylamides, which find many uses as water-soluble thickeners and flocculation agents. It is highly toxic, likely to be carcinogenic, and partly for that reason it is mainly handled as an aqueous solution.

Cyclic structure betaine and double-tailed hydrophobic association polymer fracturing thickening agent and preparation method thereof

The invention relates to a ring structure betaine and double-tailed hydrophobic association polymer fracturing thickening agent and a preparation method thereof. The thickening agent is formed by copolymerization of four monomers, namely acrylamide, 2-allyl methylamino sodium ethanesulfonate, methyl diallyl sulfoethyl betaine and hydrophobic monomer double-tailed long-chain alkyl methyl allyl ammonium chloride. The preparation method comprises the following steps: firstly adding distilled water, then sequentially adding acrylamide, 2-allyl methylamino sodium ethanesulfonate, methyl diallyl sulfoethyl betaine and a hydrophobic monomer double-tailed long-chain alkyl methyl allyl ammonium chloride, adjusting the total concentration, introducing N2 to remove oxygen, adding an initiator, and reacting to prepare an AM / AMES / MDASBA / DCnMAAC quadripolymer, namely the polymer fracturing thickening agent. The thickening agent provided by the invention has good water solubility, and shows good salt resistance in mixed brine with the mineralization degree of greater than or equal to 30000 mg / L. The prepared linear solution and gel formed after crosslinking have high viscosity retention capacity at the temperature of 150 DEG C and the shearing rate of 170 s <-1 >, and the actual construction requirement for fracturing yield increase with the on-site mineralization degree larger than or equal to 30000 mg / L is met.
Owner:HEBEI PETROLEUM VOCATIONAL & TECH UNIV

A fireproof magnesium oxide plate

A fireproof magnesium oxide board is prepared by mixing the following raw materials, the raw material names and weight parts are as follows: 80-100 parts of magnesium oxide; 20-30 parts of anhydrous magnesium chloride; 10-20 parts of modified expanded vermiculite foaming agent; 20-30 parts of aluminum silicate fiber; 5-10 parts of sawdust; 10-15 parts of fly ash; 8-12 parts of glass magnesium board crushed powder; 1.5-5 parts of non-woven fabric; 10-20 parts of water; wherein the modified expanded vermiculite is prepared by the following steps: (1) Vermiculite is incompletely expanded and calcined; (2) acrylic acid monomer, sodium hydroxide, acrylamide monomer, initiator potassium persulfate, crosslinking aid pentaerythritol polyglycidyl ether, incompletely expanded vermiculite, and water are taken, stirred evenly and ultrasonically dispersed to obtain a first reaction solution, which is placed in a reactor for reaction to obtain a gel material; (3) the gel material is preliminarily crushed and dried, and then further crushed in a ball mill to obtain a fire-resistant expanded vermiculite with water absorption performance.
Owner:SHIJIAZHUANG YICHEN FIRE INSULATION MATERIAL CO LTD

Negative electrode binder, negative electrode plate and secondary battery

The invention provides a negative electrode binder, a negative plate and a secondary battery in order to solve the problems of low peeling strength and low cycle life of a coating of an existing negative electrode binder. The negative electrode binder comprises a copolymer, and the copolymer comprises an acrylate unit, a vinyl aromatic unit, an acrylamide unit, an acrylate-polyol unit and a crosslinking unit. According to the negative electrode binder provided by the invention, the negative electrode active material layer has relatively high binding power, low pole piece rebound and relatively small full-charge rebound, so that the long cycle life of the battery is ensured.
Owner:SHENZHEN HAODYNE TECH CO LTD

Foam base fluid, preparation method and preparation method of temperature-resistant and salt-resistant CO2 foam oil displacement system

The invention discloses a foam base fluid, a preparation method and a preparation method of a temperature-resistant and salt-resistant CO2 foam flooding system.The foam base fluid comprises a foaming agent, a foam stabilizer and water, the foaming agent is a betaine type surfactant, and the foam stabilizer is a biological polysaccharide polymer. A temperature-resistant and salt-resistant foam base solution and a biological polysaccharide reinforced CO2 foam oil displacement system are obtained by introducing a biological polysaccharide polymer as a foam stabilizer and combining with a betaine type surfactant, so that the problem that the viscosity of polyacrylamide as a traditional foam stabilizer is reduced and even fails in a high-temperature and high-salt environment is effectively solved; the stability of CO2 foam can be obviously improved. Meanwhile, the biological polysaccharide polymer has the characteristics of environmental friendliness and degradability, and can effectively reduce the negative influence on the environment. In addition, due to rich resources and low price of the biological polysaccharide, the system is competitive in cost, and the economic benefit of the oil field can be further improved.
Owner:SICHUAN UNIV

Wear-resistant and high-temperature-resistant synchronous belt and preparation method thereof

The invention discloses a wear-resistant and high-temperature-resistant synchronous belt and a preparation method thereof. The wear-resistant and high-temperature-resistant synchronous belt comprises a synchronous belt framework and a synchronous belt rubber sheet, the synchronous belt rubber sheet is prepared from the following raw materials: a fluorosilicone thermoplastic polyurethane elastomer containing a benzene ring structure, an amino-containing hyperbranched liquid crystal polymer, methyl vinyl phenyl silicone rubber, epoxidized natural rubber, molybdenum sulfide nanosheets, reinforced fibers, bis (1-vinyl imidazole-2-) ketone, 2-acrylamido-2-methylpropanesulfonic acid, 4, 4 '-difluoro-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1, 3, 4-trimethyl-1 The high-temperature-resistant rubber is prepared from 2, 6-hydroxy-2-cyanobenzothiazole, bis (3-aminophenyl) 3, 5-bis (trifluoromethyl) phenylphosphine oxide, a catalyst, a coupling agent, a vulcanizing agent, an anti-aging agent, a scorch retarder and a lubricating agent. The synchronous belt is good in mechanical property, sufficient in high-temperature resistance and cold resistance, good in wear resistance and excellent in aging resistance and flame retardance.
Owner:NINGBO FULONG SYNCHRONOUS BELT

Preparation method of temperature-resistant and salt-resistant fracturing fluid

The invention relates to the technical field of fracturing fluids, and discloses a preparation method of a temperature-resistant and salt-resistant fracturing fluid, which comprises the following steps: carrying out polymerization reaction on acrylamide, acrylic acid and an acrylamide sulfonic acid monomer to obtain a polymer thickening agent, and compounding the polymer thickening agent with a cross-linking agent, a clay stabilizer and the like to obtain the temperature-resistant and salt-resistant fracturing fluid. The polymer thickening agent contains long-chain alkyl, a physical cross-linked spatial network structure can be formed through a hydrophobic association effect, the hydrodynamic volume is increased, a good tackifying effect is achieved, and after high-speed shearing, the long-chain alkyl can be cross-linked again to form a spatial network structure, so that a solution still keeps very high apparent viscosity, and the viscosity of the solution is improved. Good anti-shearing performance is realized. The acrylamide sulfonic acid monomer contains a sulfonate group and is used as a temperature-resistant and salt-resistant monomer, so that the polymer thickening agent has good temperature resistance and salt resistance, and the fracturing fluid still keeps relatively high apparent viscosity after being subjected to high-temperature heat treatment and in formation water with high salinity.
Owner:SHAAN XI ACTIVE SUN RISE PETROCHEMICAL CO LTD

Self-crosslinking temperature-resistant salt-resistant emulsion type fracturing fluid thickening agent and preparation method thereof

The invention discloses a self-crosslinking temperature-resistant salt-resistant emulsion type fracturing fluid thickening agent and a preparation method thereof, and belongs to the technical field of oilfield chemistry. The raw materials adopted by the invention comprise 30 to 50 parts of an oily solvent, 15 to 25 parts of deionized water, 10 to 20 parts of acrylamide, 5 to 10 parts of acrylic acid, 2 to 4 parts of 2-acrylamido-2-methylpropanesulfonic acid, 0.05 to 0.2 part of a crosslinking monomer, 0.5 to 1 part of a quaternary ammonium salt type hydrophobic association monomer, 4 to 8 parts of an emulsifier and 1 to 2 parts of a phase inversion agent. The self-crosslinking emulsion is formed through water phase-oil phase mixing, high-speed emulsification, low-temperature initiation polymerization and phase inversion treatment. Based on physical-chemical double-crosslinking temperature control cooperation, a salt-resistant-hydrophobic double-shielding mechanism and an integrated design without an exogenous crosslinking agent, the contradiction between the temperature-resistant and salt-resistant performance of a traditional thickening agent and the process complexity is broken through, and a technical support is provided for efficient development of high-temperature and high-salt oil and gas reservoirs.
Owner:JILIN INST OF CHEM TECH +1

Three-dimensional network polymer gel electrolyte, positive plate and solid-state lithium battery

The invention provides a three-dimensional network polymer gel electrolyte, a positive plate and a solid-state lithium battery. The three-dimensional network polymer gel electrolyte comprises 80-98% of an organic solvent, 5-15% of a lithium salt, 2-8% of lignosulfonate, 2-10% of a polymeric monomer and 2-8% of an ionic liquid, and the polymeric monomer is selected from acrylamide, polyethylene glycol dimethacrylate, 3-(methacryloyloxy) propyl trimethoxy silane or tetrahydrofurfuryl acrylate and the like. Under ultraviolet light, lignosulfonate can spontaneously generate quinonyl photochemical free radicals and hydroxyl photochemical free radicals in a mixed solution of ionic liquid and specific polymer monomers, and under the action of the photochemical free radicals, the lignosulfonate reacts with unsaturated double bonds on a polymer through phenolic groups, so that the photochemical free radicals are formed. The gel electrolyte with a three-dimensional network structure is formed, the mechanical strength can be improved, the growth of lithium dendrites in a lithium metal battery can be inhibited, and the metal lithium battery containing the gel electrolyte has excellent cycle life and safety performance.
Owner:HUNAN LIFANG NEW ENERGY SCI & TECH

Preparation method and application of core-shell structure silicon dioxide blocking agent with rigid inside and soft outside for marine drilling fluid

ActiveCN119505122AEfficient pluggingimprove securityProductsReagentsMicro nanoMeth-
The invention relates to a preparation method and application of an inner-rigid outer-soft core-shell structure silicon dioxide blocking agent for marine drilling fluid, and belongs to the field of deepwater oil and gas drilling. N-vinyl-2-pyrrolidone, dimethyl diallyl ammonium chloride, acrylamide and 2-acrylamide-2-methylpropanesulfonic acid are polymerized and grafted on the surface of nano silicon dioxide to form the silicon dioxide blocking agent with a core-shell structure and a rigid inside and a soft outside; by means of rigid plugging of a nano material and deformation filling flexible plugging of a high-molecular polymer, shale micro-nano pores are efficiently plugged with rigid inside and flexible outside, so that the stability of a well wall is maintained, meanwhile, secondary generation of hydrates is effectively inhibited, and the safety and efficiency of deepwater drilling are improved; the plugging agent provided by the invention reduces the demand on a large number of thermodynamic inhibitors, not only saves the cost, but also has the characteristic of environmental protection.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Solid-free well killing fluid for shale oil reservoir and preparation method of solid-free well killing fluid

The invention relates to the field of oil well opening and killing fluid production, in particular to a solid-free well killing fluid for shale oil reservoir and a preparation method of the solid-free well killing fluid. The solid-free well killing fluid for the shale oil reservoir comprises the following raw materials in parts by mass: 50-70 parts of water, 10-30 parts of a density regulator, 3-6 parts of a copolymer tackifier, 1-3 parts of a dispersant, 3-7 parts of a filtrate reducer and 2-4 parts of a corrosion inhibitor. The copolymer tackifier is obtained by initiating copolymerization by taking acrylamide, a quaternary ammonium salt-containing monomer, an unsaturated silane coupling agent and polyethylene glycol diacrylamide as monomer free radicals, and the dispersing agent comprises gas-phase nano silicon dioxide and a fluorine-containing surfactant. Through reasonable compatibility of all the components in the formula, especially the copolymer tackifier, the effect that one agent has multiple functions is achieved, and meanwhile the high temperature resistance, the corrosion inhibition performance and the clay stability of the well killing fluid are improved.
Owner:DAQING YONGZHU PETROLEUM TECH DEV CO LTD

Coating liquid for PET optical film coating and preparation method thereof

The invention relates to the technical field of PET optical film coatings, in particular to a coating liquid for a PET optical film coating and a preparation method of the coating liquid. The coating liquid for the PET optical film coating is prepared from the following preparation raw materials in parts by mass: 20 to 25 parts of polyurethane acrylic resin, 10 to 15 parts of N-hydroxymethyl acrylamide, 1 to 2 parts of a coupling agent, 4 to 6 parts of a photoinitiator, 8 to 10 parts of modified nano titanium dioxide, 0.2 to 0.3 part of an ultraviolet light absorber and 40 to 47 parts of a reactive diluent. The coating liquid for the PET optical film coating prepared by the invention is excellent in adhesive force, weather resistance, scratch resistance, light transmittance and the like, and has a wide application prospect.
Owner:BLUE OCEAN & BLACK STONE TECH CO LTD (FUJIAN)

Intelligent production management system and method for high-concentration polyacrylamide fracturing fluid

The invention relates to an intelligent production management system and method for high-concentration polyacrylamide fracturing fluid, and the method comprises the steps: obtaining multi-source heterogeneous data through designing a unique algorithm model and an innovative data processing flow: an innovative data collection and fusion strategy, and designing a comprehensive and high-precision data collection system; based on intelligent control algorithm innovation of a fuzzy neural network and MPC, the fuzzy neural network and model prediction control are combined to carry out production process control, a robust optimization method is introduced to enhance the robustness of a control strategy, and meanwhile, a rule-based emergency processing mechanism is established; intelligent mechanism innovation of quality monitoring and optimization is realized, and real-time monitoring and analysis of product quality are realized by establishing a quality prediction model based on combination of support vector machine regression (SVR) and a particle swarm optimization (PSO) algorithm.
Owner:BEIJING SHANNUO IND TECHNOLOGY CO LTD

Flexible aqueous binder for negative electrode of lithium battery and preparation method of flexible aqueous binder

The invention relates to a flexible aqueous binder for a lithium battery negative electrode and a preparation method thereof. The preparation method comprises the following steps: firstly, preparing a flexible polyurethane prepolymer containing vinyl by taking hydroxyl-terminated polybutadiene, isocyanate and hydroxyl acrylate as main raw materials; vinyl-containing compounds such as water-soluble acrylic acid (salt) or acrylamide, oil-soluble acrylic ester or acrylonitrile and the like are used as monomers and are combined with a flexible polyurethane prepolymer to prepare the negative water-based binder with flexible cross-linking points through free radical polymerization. The aqueous binder prepared by the technical method provided by the invention can realize point-to-point and point-to-line bonding modes with a pole piece active substance on a microstructure, so that the bonding strength of the active layer material and a copper foil is improved on the premise of not influencing the electrolyte resistance of the binder; and the flexibility of the negative pole piece and the subsequent processing stability are obviously improved.
Owner:GUANGZHOU FUSIDA CHEM PROD CO LTD +1

Cellulose paper-based polymer solid electrolyte as well as preparation method and application thereof

The invention relates to the technical field of all-solid-state lithium metal batteries, in particular to a cellulose paper-based polymer solid electrolyte as well as a preparation method and application thereof. The preparation method comprises the following steps: mixing N-methylacetamide and lithium bis (trifluoromethanesulfonyl) imide to obtain a eutectic solvent; the preparation method comprises the following steps: mixing a eutectic solvent, polyethylene glycol oxalate, acrylamide and a thermal initiator to obtain a eutectic polymer electrolyte precursor; and soaking cellulose paper in the eutectic polymer electrolyte precursor, and carrying out hot-pressing polymerization to obtain the cellulose paper-based polymer solid electrolyte. The cellulose paper-based polymer solid electrolyte prepared by the invention is soft in texture and can be better attached to an electrode, the problem of poor contact between the electrode and an electrolyte interface is solved, and the interface impedance is reduced by fusing the characteristics of low viscosity and high conductivity of the eutectic solvent and the supporting effect of the cellulose paper; the ion transmission efficiency is improved, and conditions are provided for long-term stable circulation of the battery.
Owner:CHINA NAT PULP & PAPER RES INST CO LTD

Modified coal gangue-based large-flow-state grouting and water plugging material and preparation method thereof

The invention provides a modified coal gangue-based large-flow-state grouting and water plugging material and a preparation method thereof. Comprising 80-90 parts of a coal gangue sample, 1-5 parts of Portland cement, 1-5 parts of sulphoaluminate cement, 0.51-3 parts of a polycarboxylic acid water reducing agent, 1-4 parts of cellulose ether with the viscosity of 200w, 0.1-5 parts of a calcium oxide expanding agent, 0.5-5 parts of a plastic expanding agent, 0.5-1 part of redispersible latex powder, 0.5-5 parts of polyacrylamide with the molecular weight of 1000 and water, and the water-material ratio is 0.4. According to the modified coal gangue-based large-flow-state grouting and water plugging material and the preparation method thereof, the cement consumption can be remarkably reduced, the cost is reduced, the utilization rate of solid wastes (such as coal gangue) is increased, and the material has good flow-state performance and adjustable setting time; the method is suitable for deep and large shaft surrounding rock water seepage treatment in coal mining and other mine engineering.
Owner:SHAANXI TONGREN APPLIED MATERIAL CO LTD

Hydrophobic and oleophobic modified epoxy resin as well as preparation method and application thereof

The invention discloses a hydrophobic and oleophobic modified epoxy resin, which is prepared from the following components in parts by mass: 2 to 5 parts of thiolactone terminated fluorinated prepolymer, 15 to 16 parts of 4, 4 '-diaminodiphenylmethane, 0.13 to 0.14 part of base catalyst, 25 to 26.5 parts of epoxy resin and the balance of tetrahydrofuran solvent, wherein the thiolactone-terminated fluorinated prepolymer is prepared from thiolactone acrylamide, fluorinated acrylate and a photoinitiator in a mass ratio of (2-3): 1: (0.07-0.09) through a free radical polymerization copolymerization chemical reaction under the induction of ultraviolet light, and the thiolactone-terminated fluorinated prepolymer is obtained; wherein thiolactone acrylamide is prepared from DL-homocysteine thiolactone hydrochloride, a NaHCO3 solution and acryloyl chloride according to the mass ratio of 1: (1.3-1.5): (1.1-1.3), the oleophobic and hydrophobic modified epoxy resin provided by the invention effectively solves the problem that an epoxy resin coating in the prior art is poor in oleophobic performance and hydrophobic performance, and the oleophobic and hydrophobic modified epoxy resin has the advantages that the oleophobic and hydrophobic properties of the epoxy resin coating are improved; therefore, the oleophobic and hydrophobic properties of the epoxy resin coating are improved.
Owner:JIANGSU SIMBA NEW MATERIAL TECH CO LTD +1

Preparation method of high-temperature-resistant thickening agent for fracturing

The invention relates to the technical field of thickening agents, and discloses a preparation method of a high-temperature-resistant thickening agent for fracturing. According to the preparation method disclosed by the invention, acrylamide, sulfobetaine modified acrylamide and pyrrolidone modified naphthyl melamine are polymerized, so that the thickening agent for high-temperature-resistant fracturing is obtained. A triazine ring structure and naphthyl have high stability, the rigidity of a polyacrylamide molecular chain and the hydrophobic association effect between molecules are enhanced, the high temperature resistance and the salt resistance are improved, and due to the conjugation effect formed by two benzene rings in naphthyl, the thermal stability is further enhanced; by introducing vinyl pyrrolidone, hydrolysis of amido in polyacrylamide can be inhibited, and the temperature resistance and salt resistance of the thickening agent are improved; under a high-salt condition, due to weakening and shielding of mutual attraction of salt ions to anionic and cationic groups in the sulfobetaine, polyacrylamide molecules are more stretched, macroscopically, the viscosity is increased or reduced slightly, and the temperature resistance and salt resistance are improved.
Owner:PUYANG GREEN SINGULARITY NEW MATERIAL CO LTD

High density environmentally friendly polymer water-based drilling fluid with resistance to 240° C. and saturated salts, preparation method therefor and use thereof

The present disclosure relates to the technical field of drilling fluid, and discloses a high density environmentally friendly polymer water-based drilling fluid with resistance to 240° C. and saturated salts, a preparation method therefor and use thereof. The water-based drilling fluid comprises a micro-crosslinked heterocyclic polymer filtrate reducer, a hyper-branched strongly adsorbed filtrate reducer, a nanometer intercalated complex shearing potentiator, a flexible outer and rigid inner microsphere plugging agent, and water, wherein the micro-crosslinked heterocyclic polymer filtrate reducer is prepared by reacting sodium p-styrene sulfonate, N,N,N-trimethyl-3-(2-methylallylamino)-1-propyl ammonium chloride, N,N-diethyl acrylamide, N-vinyl caprolactam, tetramethyl ethylenediamine with phenyl triethoxy silane. The high density environmentally friendly polymer water-based drilling fluid with resistance to 240° C. and saturated salts of the present disclosure can exhibit good performance at high temperature and high salinity conditions, and has desirable weighting capability, it can meet the requirements of drilling well in the deep oil and gas formations.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Low-carbon polymer modified all-solid waste premixed fluid soil and preparation method thereof

The invention discloses a low-carbon polymer modified all-solid waste premixed fluid-state soil, which is prepared from the following components in parts by weight: 10-30 parts of low-carbon polymer modified all-solid waste premixed fluid-state soil, the concrete is prepared from the following components in parts by weight: 5-10 parts of a modifier, 5-10 parts of an exciting agent, 1-5 parts of an additive, 1-5 parts of a retarder, 10-20 parts of coal gangue powder, 10-20 parts of carbide slag, 10-20 parts of bentonite, 35-40 parts of fly ash, 35-40 parts of slag powder, 100 parts of clay powder, 145 parts of machine-made medium sand and 150 parts of water. According to the invention, the polymer polyacrylamide is added into the fluid soil, so that the compressive strength of the fluid soil stone body is improved; when the polyacrylamide is mixed with the fluid soil, active components in the polymer emulsion and components in the fluid soil are subjected to a cross-linking reaction to form a more complex network structure, so that a dispersion system of the slurry can be remarkably improved, the repulsive potential energy among particles in a multiphase dispersion is reduced, and the integrity and the stability of the slurry are enhanced; the slurry is not easy to separate when being injected into underground rock strata or fractures, and good uniformity and flowability are maintained.
Owner:SHANGHAI CONSTR BUILDING MATERIALS TECH GRP CO LTD +1

Demulsifier for eliminating oil-water interface emulsion layer in oilfield produced liquid treatment and preparation method thereof

The invention belongs to the technical field of sewage treatment, and particularly relates to a demulsifier for eliminating an oil-water interface emulsion layer in oilfield produced liquid treatment and a preparation method of the demulsifier. The preparation method comprises the following steps: adding acrylamide, 1-allyl-3-methylimidazolium bis (trifluoromethanesulfonyl) imine salt, allyl tributyl phosphonium chloride and deionized water into a first reactor, and heating and dissolving the acrylamide, the 1-allyl-3-methylimidazolium bis (trifluoromethanesulfonyl) imine salt, the allyl tributyl phosphonium chloride and the deionized water; adding allyl (diisopropylamino) dimethylsilane, butyl acrylate, deionized water, octylphenol polyoxyethylene ether-10, lauryl sodium sulfate and monopotassium phosphate into the second reactor, and stirring to obtain an emulsion; adding an initiator and sodium hydrogen sulfite into a second reactor, carrying out heating and heat preservation reaction, pouring the mixed solution in the first reactor, and continuously carrying out reaction, heating and heat preservation to obtain a viscous liquid; and drying and granulating the viscous liquid to obtain the demulsifier. The demulsifier provided by the invention has the characteristics of simple synthesis process and high demulsification rate.
Owner:DONGYING SPRING PETROLEUM ENG TECH

Papermaking filler wrapping agent as well as preparation method and application thereof

The invention relates to the technical field of papermaking, in particular to a papermaking filler wrapping agent and a preparation method and application thereof. The papermaking filler wrapping agent comprises a cationic polyester polyacrylamide emulsion and a high molecular weight water-soluble polymer. The papermaking filler wrapping agent has the advantages that the papermaking filler wrapping agent is insensitive to shearing action, the retention rate of filler such as calcium carbonate is high, the paper strength is not reduced, and produced paper products are good in batch stability.
Owner:YABANG FUJIAN BIOCHEMICAL CO LTD

Liquid metal / MXene / sodium alginate / polyacrylamide composite hydrogel material as well as preparation method and application thereof

ActiveCN119684737AMicrosphereCross linker
The invention relates to a liquid metal / MXene / sodium alginate / polyacrylamide composite hydrogel material as well as a preparation method and application thereof. The hydrogel material comprises liquid metal microspheres, a hierarchical porous network formed by sodium alginate and polyacrylamide, and flaky MXene. The preparation method comprises the following steps: S1, adding liquid metal into an aqueous solution, and carrying out ultrasonic dispersion to obtain dispersion liquid; s2, adding the dispersion liquid into a sodium alginate solution, and performing ultrasonic treatment to obtain a sodium alginate-coated liquid metal aqueous solution; s3, acrylamide is dissolved in deionized water, then the aqueous solution of the liquid metal wrapped by sodium alginate is added, then a cross-linking agent, an initiator and MXene are added, and the mixture is stirred to be uniform; and S4, pouring into a mold, and heating to form the hydrogel. The composite hydrogel material prepared by the invention has the advantages of high stretch rate, strong electromagnetic shielding performance and the like, and can be used as electronic skin for electromagnetic shielding, human health monitoring, man-machine communication and soft robots.
Owner:TONGJI UNIV

Concrete composite tackifier and preparation method thereof

The invention discloses a concrete composite tackifier and a preparation method thereof, and relates to the technical field of concrete. When the concrete composite tackifier is prepared, firstly, polyacrylic resin obtained by polymerizing acrylic acid, methyl methacrylate, acrylamide and vinyl diphenylphosphine reacts with modified porphyrin, and then sulfonation is performed to obtain modified polyacrylic resin; the preparation method comprises the following steps: firstly, pre-treating silica fume with vinyltrimethoxysilane, then carrying out a reaction on the silica fume pre-treated with vinyltrimethoxysilane, tetravinyltetramethylcyclotetrasiloxane and vinylboronic acid pinacol ester to obtain modified silica fume, and finally, mixing polyacrylic resin and the modified silica fume to obtain the concrete composite tackifier. The concrete composite tackifier prepared by the invention has good working performance and antibacterial property.
Owner:GANSU JINKAINING IND & TRADE GRP CO LTD

Anti-scale cross-linked polymer fracturing fluid and preparation method thereof

The invention discloses an anti-scale cross-linked polymer fracturing fluid and a preparation method thereof, and relates to the technical field of petroleum fracturing fluids. When the anti-scale cross-linked polymer fracturing fluid is prepared, allylamine hydrochloride and epoxy chloropropane react to prepare a double-bond chlorinated intermediate; reacting the double-bond chlorinated intermediate with lauramidopropyl dimethylamine to prepare a cationic monomer; copolymerizing a cationic monomer and acrylamide to prepare a cationic polymer; the preparation method comprises the following steps: reacting L-lysine with formaldehyde and phosphorous acid to prepare phosphoric acid modified lysine; reacting the phosphoric acid modified lysine with allyl glycidyl ether to prepare a phosphoric acid modified monomer; acrylamide and an anionic monomer are copolymerized to prepare an anionic polymer; the anionic polymer and the cationic polymer are dissolved in water to prepare the anti-scale cross-linked polymer fracturing fluid. The anti-scale cross-linked polymer fracturing fluid prepared by the invention has the advantages of scale prevention, good temperature resistance, good shear resistance and self-crosslinking.
Owner:KARAMAY HAOYUAN TIANCHENG ENERGY TECHNOLOGY CO LTD

Linked molecular marker of peanut hypocotyl elongation related gene locus, identification method and application of linked molecular marker

The invention belongs to the technical field of crop genetic breeding, and relates to a linked molecular marker of a peanut hypocotyl elongation related gene locus, an identification method and application of the linked molecular marker. The primer pair is C2-15-F / R, and the sequence of the primer pair is as shown in SEQ ID NO. 1 and SEQ ID NO. 2; by designing an InDel marker C2-15, the peanut hypocotyl length character can be quickly distinguished by using a primer to amplify a target band and using polyacrylamide gel electrophoresis detection. The identification method is more accurate and convenient, has good repeatability, can efficiently distinguish the phenotype and genotype of an individual, shortens the experiment process, has the advantages of simple and feasible operation steps and the like, and saves expenditure. The method disclosed by the invention has important application value in the breeding work aspects such as peanut hypocotyl elongation character related gene positioning, genotype typing and later cultivation of excellent peanut varieties.
Owner:QINGDAO AGRI UNIV +1

Viscoelastic polymer type self-assembly plugging agent and preparation method thereof

The invention relates to the technical field of plugging agents, and discloses a viscoelastic polymer type self-assembly plugging agent and a preparation method thereof. The preparation method comprises the following steps: adding acrylamide, butyl acrylate, 2-acrylamide-2-methylpropanesulfonic acid, quaternized cyclodextrin, gamma-glycidyl ether oxypropyl trimethoxy silane modified bentonite, Schiff base styrene, a sodium dodecyl benzene sulfonate emulsifier and octadecyl dimethyl allyl ammonium chloride into a reaction kettle; and adding an azodiisobutyronitrile initiator into the deionized water, uniformly mixing, and reacting for 4-5 hours at 50-65 DEG C to obtain the viscoelastic polymer type self-assembled plugging agent after the reaction is finished. The plugging agent disclosed by the invention has a relatively good plugging effect, and effectively solves the problem that the gel strength is weakened or the gelling is not thorough due to the formation shearing effect in a continuous gel migration process.
Owner:DONGYING FANGLI CHEM CO LTD

Preparation method of high-hardness and high-sulfate-radical water quality scale inhibitor

The invention relates to a preparation method of a high-hardness and high-sulfate-radical water quality scale inhibitor, and belongs to the technical field of water treatment.The preparation method comprises the steps that sodium carboxymethyl cellulose-sulfur quantum dots are prepared by using carboxymethyl cellulose as a stabilizer and then subjected to a copolymerization reaction with 2-acrylamido-2-methylpropanesulfonic acid and itaconic acid, and the high-hardness and high-sulfate-radical water quality scale inhibitor is obtained. The preparation method comprises the following steps: carrying out a reaction on sodium carboxymethyl cellulose and sulfur quantum dots to obtain modified sodium carboxymethyl cellulose-sulfur quantum dots, and carrying out a reaction on polysuccinimide, 4-amino phthalic acid and 2-aminoethanesulfonic acid to obtain a polyaspartic acid derivative; the modified sodium carboxymethyl cellulose-sulfur quantum dots and the polyaspartic acid derivative are mixed to serve as the scale inhibitor, the scale inhibition rate of the scale inhibitor is remarkably increased through the synergistic effect of the modified sodium carboxymethyl cellulose-sulfur quantum dots and the polyaspartic acid derivative, and meanwhile, due to the fact that a large number of new hydrogen bonds are generated between the modified sodium carboxymethyl cellulose-sulfur quantum dots and the polyaspartic acid derivative, the scale inhibition rate of the scale inhibitor is increased. The stability of a polymer structure is improved, so that the temperature resistance of the scale inhibitor is improved. The scale inhibitor is green and environment-friendly, and has excellent scale inhibition efficiency on high-hardness and high-sulfate-radical water.
Owner:SHANDONG MUFU ENVIRONMENTAL PROTECTION TECHNOLOGY CO LTD

Long-acting moisturizing and barrier repairing type exosome active gel and preparation method thereof

The invention relates to the field of skin care and medical cosmetology, and discloses a long-acting moisturizing and barrier repairing type exosome active gel and a preparation method thereof, and the gel comprises the following components by mass: 2-5 parts of exosome; 3 to 7 parts of trehalose; 2 to 6 parts of glycerol; 1 to 2 parts of polyvinyl acrylate; 0.5 to 1.5 parts of octyl glucoside; 0.8 to 1.5 parts of sodium hyaluronate; 0.2 to 0.5 part of low molecular peptide; 1 to 3 parts of polyacrylamide; and 0.02 to 0.05 part of a tea polyphenol antioxidant. According to the invention, through synergistic repair of the exosome and the low-molecular peptide, dual moisturizing of the trehalose and the glycerol, a thickening system is innovated to improve the stability, and the tea polyphenol antioxidant is combined, so that deep repair, lasting moisturizing, skin feeling optimization and aging resistance are effectively realized, and multiple bottleneck problems of a traditional skin care technology are comprehensively solved.
Owner:BEIJING HEALTH & BIOTECH (H&B) CO LTD

Polymeric gels with organic crosslinkers for water blocking in oil wells and their synthesis process

The present disclosure relates with the development of a process for producing gels from polymeric materials crosslinked with organic agents and their use controlling water in porous media under high salinity and temperature conditions. The characteristics of these gels enable them to have a good performance withstanding extreme conditions in mature Mexican oil wells and in others located in other parts of the world. The gels featured in the present disclosure include novel ionic terpolymers based on acrylamide (AM), N-vinylpyrrolidone (VP), N,N′-methylenebisacrylamide (BAA), 1-vinyl-3-butylimidazolium bromide (VIM4C[Br]) and organic crosslinking agents.
Owner:INST MEXICANO DEL GASOLINEEO

Solid waste-based reinforced ceramic tile adhesive and preparation method therefor

PCT designated stage expiredWO2025124213A1Solid waste managementAdhesive cementPolyacrylamide
A solid waste-based reinforced ceramic tile adhesive and a preparation method therefor. The solid waste-based reinforced ceramic tile adhesive comprises 17-22% of polyacrylamide modified solid waste residue powder, 3-7% of cement, 7-12% of tailing micro powder, 55-65% of graded tailing sand and 8-13% of a tensile adhesive. By limiting the raw material components and content of the tensile adhesive, the tensile adhesive strength of the solid waste-based adhesive with different substrates and the construction performance thereof can be ensured; and the solid waste residue powder is modified by using a very small amount of low-molecular-weight polyacrylamide, such that the stability of the system can be significantly improved, and the comprehensive performance of the solid waste-based ceramic tile adhesive can be enhanced. The solid waste-based reinforced ceramic tile adhesive comprises 90 wt% or more of solid wastes. By limiting the components and contents of each raw material, all components can act synergistically, so that the solid waste-based reinforced ceramic tile adhesive can replace traditional cementing materials such as cement, which greatly reduces the cost, realizes the comprehensive utilization of industrial solid waste materials, and has significant advantages such as saving on energy, having environmental protection and being low carbon.
Owner:XIAMEN DUITAI NEW MATERIAL TECHNOLOGY CO LTD