The invention provides a method for preparing a
lithium slag-based
molecular sieve by melting
lithium slag with assistance of eutectic salt, and relates to the technical field of molecular sieves. The method comprises the following steps: carrying out acid
pickling pretreatment on a
lithium slag raw material to obtain pretreated lithium slag; co-
grinding and uniformly mixing the pretreated lithium slag and eutectic salt, and reacting at 200-350 DEG C for 2-6 hours to obtain eutectic lithium slag; carrying out aging treatment and
crystallization treatment on the eutectic lithium slag, carrying out
solid-liquid separation, washing the
solid to be neutral, and
drying to obtain a lithium slag-based
molecular sieve; wherein the eutectic salt comprises an alkali
solvent and an auxiliary salt, the alkali
solvent is
sodium hydroxide, and the auxiliary salt is at least one of
chlorine salt, villiaumite,
carbonate,
sulfate and
nitrate; the
molar ratio of the alkali flux to the auxiliary salt is (4-19): 1. According to the method, the eutectic salt
system is introduced in the lithium slag alkali fusion stage, meanwhile, the
molar ratio of the alkali flux to the auxiliary salt in the eutectic salt is controlled to be (4-19): 1, the alkali fusion
reaction temperature is reduced, the reaction of the lithium slag and alkali is promoted, the
molecular sieve yield is increased, the product morphology can be regulated and controlled, and a specific molecular
sieve can be formed in a guiding mode.