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665 results about "Polyamine" patented technology

A polyamine is an organic compound having more than two amino groups. Alkyl polyamines occur naturally but are also synthetic. Alkylpolyamines are colorless, hygroscopic, and water soluble. Near neutral pH, they exist as the ammonium derivatives. Most aromatic polyamines are crystalline solids at room temperature.

Colorful acid and alkali resistant laser printing ink and preparation method thereof

InactiveCN104403412AGood acid and alkali resistanceOvercome the disadvantage that it is easy to produce depletion when mixed with acid and alkaliInksGlycidyl ethersPrinting ink
The invention discloses a colorful acid and alkali resistant laser printing ink and a preparation method thereof. The printing ink is composed of the following components in parts by weight: 0 to 30 parts of butanone, 10 to 30 parts of isopropanol, 2 to 6 parts of curing agent, 10 to 15 parts of pigment, and 10 to 30 parts of glycidyl ether epoxy resin. The glycidyl ether epoxy resin is adopted to produce the printing ink, aliphatic polyamine is further chosen as the curing agent, the acid and alkali resistant performance of the printing ink is strengthened through optimizing the formula, thus the shortage that the colorful laser printing ink is lost when being mixed with acid and alkali is overcome, moreover, the color of the laser printing product is more abundant, and the patterns are more clear.
Owner:SHENZHEN TIANYITONG ANTI-COUNTERFEITING PACKAGING MATERIALS CO LTD

Antifouling self-cleaning fluorocarbon finish paint as well as preparation method and application thereof

The invention provides an antifouling self-cleaning fluorocarbon finish paint as well as a preparation method and application thereof, and particularly relates to the technical field of special coatings. The antifouling self-cleaning fluorocarbon finish paint is composed of a component A and a component B in a ratio of (80-87): 16, the component A is prepared from the following components in parts by weight: 560 to 580 parts of fluorocarbon resin, 30 to 35 parts of a first solvent, 20 to 40 parts of a second solvent, 180 to 220 parts of titanium dioxide, 90 to 110 parts of filler, 11 to 20 parts of a light stabilizer, 3 to 5 parts of a thickening agent and 13 to 28 parts of an auxiliary agent; the component B comprises the following components in parts by weight: 20-22 parts of fluorocarbon resin, 4-5 parts of a chain extender, 15-20 parts of a diamine curing agent, 15-20 parts of a polyamine curing agent and 25-35 parts of a second solvent. According to the finishing paint, on the basis of enhancing the self-cleaning capability, the weather resistance of a coating is improved, and the aging and damage of the coating are delayed, so that the service life of the coating is prolonged.
Owner:ZHEJIANG JIAOGONG HIGHWAY MANTAINANCE +1

Corrosion-resistant coating material and preparation method thereof

The invention relates to the technical field of coatings, in particular to a corrosion-resistant coating material and a preparation method thereof. The corrosion-resistant coating material comprises the following components in parts by mass: 80-100 parts of epoxy resin, 5-20 parts of a modified phenolic aldehyde amine curing agent, 2-5 parts of a waterproof agent, 5-10 parts of a corrosion inhibitor and 40-55 parts of a lubricant. The modified phenolic aldehyde amine curing agent is obtained by carrying out Mannich reaction on phenol, thymol, aliphatic polyamine and formaldehyde. The phenol provides a rigid benzene ring structure, and endows a cured product with good heat resistance and chemical resistance. Thymol improves the flexibility and adhesive force of the cured product and enhances the hydrophobicity of the cured product at the same time. The epoxy resin and the modified phenolic aldehyde amine curing agent are polymerized, the waterproof agent, the corrosion inhibitor and the lubricant are wrapped, and the obtained coating material has good adhesive force and corrosion resistance.
Owner:BIOPAG (CHONGQING) BIOTECHNOLOGY CO LTD

Non-ribosome peptide-polyketone-polyamine bactericidal active substance Fcl-8 and application thereof

The invention relates to a brand-new microbial natural metabolite, namely Fcl-8, which is derived from a fermentation solution of Xenorhabdius budapestensis XBD8, and is characterized in that the Fcl-8 is a new microbial natural metabolite, namely Fcl-8, which is derived from the fermentation solution of the Xenorhabdius budapestensis XBD8. The purified Fcl-8 is a snow white flocculent crystal and is very easy to dissolve in water, and the solid state of the purified Fcl-8 is as shown in Figure 1. The chemical structural formula of the Fcl-8 is as shown in a figure 2, the chemical formula is C57H102N14O12, the molecular weight is 1175.78744, and the typical secondary mass spectrum information of the Fcl-8 is as shown in a figure 3. The Fcl-8 is derived from a microbial natural metabolite, is novel in structure and high in biological activity, and has very high potential to be developed into a novel biopesticide.
Owner:INST OF PLANT PROTECTION CHINESE ACAD OF AGRI SCI

Bionic strong acid-resistant nanofiltration membrane and preparation method thereof

The invention relates to a bionic strong acid-resistant nanofiltration membrane and a preparation method thereof, and the bionic strong acid-resistant nanofiltration membrane comprises a porous support layer and an active separation layer formed on the surface of the porous support layer, the active separation layer is a polymer network layer formed by carrying out interfacial polymerization reaction on a water-phase solution containing polyamine and an oil-phase solution containing polyacyl chloride on the surface of the porous support layer. The water-phase solution and / or the oil-phase solution also contains a bionic amphiphilic phosphate compound, the bionic amphiphilic phosphate compound participates in interfacial polymerization reaction through an active functional group in a molecular structure of the bionic amphiphilic phosphate compound, and the phosphate structure of the bionic amphiphilic phosphate compound is covalently connected into a skeleton of the polymer network layer. The preparation method has the beneficial effects that the bionic amphiphilic phosphate compound with a hydrophilic phosphate head, a hydrophobic alkyl tail and a reaction site is synthesized, so that the bionic amphiphilic phosphate compound is spontaneously and orderly arranged on a water / oil interface and participates in interfacial polymerization, the film forming uniformity is improved, the pore size distribution is narrowed, and the intelligent response characteristic is given to the film.
Owner:HANGZHOU WATER TREATMENT TECH DEV CENT

Anticorrosive coating composition

This anticorrosive coating composition comprises a main agent (I) and a curing agent (II), wherein: the main agent (I) contains an epoxy resin (a); the epoxy resin (a) contains at least one of a bisphenol A epoxy resin (a-11) and a novolac epoxy resin (a-12) each having a weight average molecular weight of 6,000-12,000; the curing agent (II) contains a polyamine (b) and an alkylphenol (c); the polyamine (b) contains an alicyclic polyamine (b-1) having a cyclic aliphatic hydrocarbon group to which an amino group is bonded and contains a non-alicyclic polyamine (b-2) having no cyclic aliphatic hydrocarbon group to which an amino group is bonded; at least one of the main agent (I) and the curing agent (II) includes a vinyl-based defoaming agent (d) that has a constituent unit derived from at least one monomer selected from the group consisting of alkyl (meth)acrylates, alkyl vinyl ethers, and olefins and that has a number average molecular weight of 30,000-100,000 or 300,000-2,000,000; the content of the alicyclic polyamine (b-1) is 30%-80% by mass of the solid content of the curing agent (II); the content of the non-alicyclic polyamine (b-2) is 2%-45% by mass of the solid content of the curing agent (II); the content of the alkylphenol (c) is 5%-60% by mass of the solid content of the curing agent (II); and the content of the vinyl-based defoaming agent (d) is 0.005-3 parts by mass with respect to 100 parts by mass of the anticorrosive coating composition.
Owner:NIPPON PAINT CO LTD

Acid-resistant polyamide nanofiltration membrane and arsenic removal application thereof in hair dye preparation

The invention discloses a polyamide acid-resistant nanofiltration membrane and arsenic removal application thereof in hair dye preparation. According to the amide acid-resistant nanofiltration membrane, a polyamine monomer and trimesoyl chloride are subjected to an interface reaction on an ultrafiltration supporting bottom membrane, and the polyamide acid-resistant nanofiltration membrane containing the Telogen structure is obtained. According to the method for removing the arsenic in the hydroxyethyl diphosphoric acid, a polyamide acid-resistant nanofiltration membrane containing a Troger structure is adopted for at least one time of filtration treatment, the concentration of arsenate in the hydroxyethyl diphosphoric acid after secondary filtration treatment is reduced to 4.60 mg / kg from 480.02 mg / kg, and the arsenic content of the hair dye prepared from the hydroxyethyl diphosphoric acid is smaller than 0.07 mg / kg. According to the polyamide acid-resistant nanofiltration membrane containing the Troger structure, which is obtained by adopting a limited preparation method, the acid resistance is greatly improved, the separation selectivity is higher, arsenic in hydroxyethyl diphosphate can be effectively removed, and the arsenic content in a hair dye is greatly reduced.
Owner:ZHEJIANG UNIV OF TECH +1

Polythiourea composite nanofiltration membrane as well as preparation method and application thereof

The invention relates to the technical field of membrane separation, and discloses a polythiourea composite nanofiltration membrane as well as a preparation method and application thereof. The composite nanofiltration membrane comprises a bottom layer, a porous support layer and a polythiourea separation layer which are arranged in sequence, wherein the polythiourea separation layer comprises a structural unit A from polyamine and a structural unit B from a polyisothiocyano compound; wherein the structural unit A and the structural unit B are connected through a structure shown in a formula I, Ar1 is a residue obtained after a reaction of a compound containing polyisothiocyano groups, and Ar2 is a residue obtained after a reaction of polyamine. The separation layer structure of the polythiourea composite nanofiltration membrane contains C = S bonds, a large number of hydrogen bonds can be formed, the polythiourea composite nanofiltration membrane has excellent chemical stability, the structural stability of the composite nanofiltration membrane in a strong acid environment is remarkably improved on the premise that the separation performance of the composite nanofiltration membrane is guaranteed, and the acid resistance of the composite nanofiltration membrane is improved.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Functionalized nanofiber material as well as preparation method and application thereof

The invention provides a functional nanofiber material as well as a preparation method and application thereof, and the preparation method comprises the following steps: (1) adding raw materials into water to form an electrostatic spinning solution; performing electrostatic spinning to obtain a nanofiber membrane; (2) cross-linking the nanofiber membrane in an organic solvent under the catalysis of acid to obtain a cross-linked nanofiber membrane; and (3) carrying out grafting reaction on the cross-linked nanofiber membrane in a polyamine cross-linking agent, and then reacting with a sulfur-containing reagent to obtain the functional nanofiber material, the functionalized nanofiber material prepared by the preparation method disclosed by the invention combines good biocompatibility of polyvinyl alcohol, high specific surface area and high porosity of nanofiber and a synergistic adsorption effect of the polyamine cross-linking agent and cysteine, and has the advantages of large adsorption capacity, high adsorption rate, strong selectivity, good biocompatibility, stable structure and the like; the heavy metal ions in the plasma can be efficiently and safely removed, and a plurality of defects of the existing adsorption material are overcome.
Owner:SUNEVERYWHERE SHANGHAI TECHNOLOGY CO LTD

Preparation method and application of metal sulfide adsorbent for adsorbing iodine and methyl iodide

The invention discloses a preparation method and application of a metal sulfide adsorbent for adsorbing iodine and methyl iodide. The preparation method comprises the following steps: uniformly mixing an antimony source, a sulfur source, a deep eutectic solvent, polyamine and water to obtain a mixed solution; and transferring the mixed solution into a high-pressure reaction kettle, sealing, carrying out hydrothermal reaction at 110-220 DEG C for 2-9 days, cooling to room temperature to separate out crystals, and filtering, washing and drying to obtain the metal sulfide adsorbent. The invention also discloses application of the metal sulfide adsorbent in adsorption of iodine and methyl iodide. The metal sulfide adsorbent disclosed by the invention has a good adsorption effect on iodine and methyl iodide, and compared with an ethylenediamine-oriented metal sulfide adsorbent, the diethylenetriamine-oriented metal sulfide adsorbent has higher adsorption capacity on iodine and methyl iodide.
Owner:FUZHOU UNIV

Preserving solution for stably preserving sample DNA (deoxyribonucleic acid) at normal temperature and preparation method of preserving solution

The invention discloses a preserving fluid for stably preserving sample DNA at normal temperature and a preparation method thereof, and belongs to the technical field of biological sample preservation. The preserving fluid comprises a lysis system, a nucleic acid protection system and a buffering and stabilizing system, the cracking system comprises a composite surfactant and an enzymolysis auxiliary agent; the composite surface active agent is prepared from polyether polyol fatty acid ester and cocamidopropyl hydroxy sulfobetaine; the enzymolysis auxiliary agent comprises lysozyme Lyso-V and protease K; the nucleic acid protection system comprises a nitrogen heterocyclic polyamine-carboxylic acid derivative and dextran sulfate; the nitrogen heterocyclic polyamine-carboxylic acid derivative comprises 1, 4, 7, 10-tetraazacyclododecane-N, N ', N' ', N ''tetraacetic acid, 1, 4, 7-triazacyclononane-N, N', N''-triacetic acid, disodium ethylene diamine tetraacetate-nitrogen heterocyclic derivative, and diethylenetriamine pentaacetic acid-piperazine derivative, and the nitrogen heterocyclic polyamine-carboxylic acid derivative comprises 1, 4, 7, 10-tetraazacyclododecane-N, N ', N '', N'' tetraacetic acid, 1, 4, 7-triazacyclononane-N, N', N ''-triacetic acid. The buffering and stabilizing system comprises an amphoteric buffering agent and a polymer stabilizer; the amphoteric buffering agent comprises 2-(N-morpholino) ethanesulfonic acid and N-tri (hydroxymethyl) methylglycine.
Owner:PEKING UNION MEDICAL COLLEGE HOSPITAL +1

Low-viscosity ternary eutectic solvent as well as preparation method and application thereof

The invention discloses a low-viscosity ternary eutectic solvent as well as a preparation method and application thereof, and belongs to the technical field of CO2 absorbents. The low-viscosity ternary eutectic solvent is composed of polyamine hydrochloride, steric hindrance amine and organic alcohol, the polyamine hydrochloride has multiple active amino groups and is used for guaranteeing the high CO2 absorption rate and absorption load of the ternary eutectic solvent, the steric hindrance amine can inhibit formation of a hydrogen bond network due to the unique steric hindrance structure, and the high CO2 absorption rate and absorption load of the ternary eutectic solvent are improved. The organic alcohol can be used as a viscosity regulating agent, active hydroxyl of the organic alcohol can promote proton transfer in a CO2 desorption reaction, and the CO2 desorption efficiency is enhanced. The ternary eutectic solvent provided by the invention can still maintain a low-viscosity homogeneous liquid state after absorbing CO2, can effectively reduce the reduction of mass transfer efficiency caused by high viscosity, influence on contact with a target compound, heat transfer efficiency and the like, and solves the ubiquitous problems of overhigh viscosity and insufficient regeneration efficiency of the existing DESs system.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Adhesive with improved adhesion to epoxy adhesive residues

The invention relates to the use of an epoxy resin adhesive for bonding substrates at least partially coated with a cured epoxy resin adhesive, characterized in that the adhesive comprises a resin component comprising at least one epoxy resin and a curing agent component comprising at least one epoxy resin, the curing agent component comprises at least one amine having at least one aliphatic amino group wherein the amine is selected from the group consisting of polyetheramines and linear or branched but non-cyclic aliphatic polyamines wherein the amine comprises at least 50% by weight of all amine curing agents having at least one amine hydrogen contained in the curing agent component, the curing agent component is based on all amine curing agents in the curing agent component. The use according to the invention allows the adhesion of substrates at least partially coated with a cured epoxy adhesive, forming a stable weather-resistant adhesive connection, and is particularly suitable for repairing rotor blades in wind turbines.
Owner:SIKA TECH AG

Microcapsule material, microcapsule using microcapsule material and preparation method of microcapsule

The invention discloses a microcapsule material, a microcapsule using the microcapsule material and a preparation method of the microcapsule, and relates to the technical field of daily chemical products. The microcapsule material comprises an addition polymer formed by a ring-opening reaction of epoxy resin and bio-based polyamine, poly (beta-amino ester) formed by a Michael addition reaction of acrylate and phenyl polyamine, and at least one cationic polymer containing quaternary ammonium groups. The microcapsule material shows certain biodegradability, the biodegradation rate of the microcapsule material exceeds 20% within 28 days, and the applied microcapsule can effectively meet the friction fragrance release performance requirement required by essence wrapping, so that after the obtained essence-encapsulated microcapsule is stored in a lotion at 45 DEG C for 28 days, the fragrance release performance of the microcapsule material is not influenced by the friction fragrance release performance, and the fragrance release performance of the microcapsule material is not influenced by the friction fragrance release performance. The excellent friction aroma releasing capability and the adhesion capability on the fabric can still be maintained, and the excellent thermal stability is shown.
Owner:GUANGZHOU LIBAI TECH GRP CO LTD

Culture medium for high-density serum-free suspension culture of BHK-21 cells and application of culture medium

The invention relates to a culture medium for high-density serum-free suspension culture of BHK-21 cells and application of the culture medium. The culture medium contains inorganic salt, amino acid, vitamins, energy substances, a buffer substance, an antioxidant, sterol, polyamine, an additive and an indicator, and the antioxidant comprises dihydrolipoic acid and S-acetyl-L-glutathione. According to the invention, the culture medium for serum-free suspension culture of the BHK-21 cells, which is clear in components and remarkable in culture effect, can be provided. The added dihydrolipoic acid and S-acetyl-L-glutathione are combined as antioxidants of the culture medium, so that the survival rate of BHK-21 cells cultured in the culture medium is improved while the oxidation resistance of the serum-free suspension culture medium is improved.
Owner:ZHONGSHENG TIANXINHE (WUXI) BIOTECHNOLOGY CO LTD

Flexible chain cable reinforcing material and preparation method thereof, flexible chain cable reinforcing material liquid injection equipment and method for reinforcing soft outburst coal seam

The invention provides a flexible chain cable reinforcing material and a preparation method thereof, flexible chain cable reinforcing material liquid injection equipment and a method for reinforcing a soft outburst coal seam, and belongs to the technical field of coal seam curing materials. The flexible chain cable reinforcing material provided by the invention comprises a material A and a material B which are subpackaged, wherein the volume ratio of the material A to the material B is 1: (0.8-1.2); the material A is prepared from components in percentage by mass as follows: 60%-75% of an epoxy modified polyurea semi-prepolymer, 12%-18% of nanoparticles, 10%-20% of a first flame retardant and 2%-3% of a catalyst; and the material B comprises the following components in percentage by mass: 45-65% of a polyamine curing agent, 25-40% of resin and 10-15% of a second flame retardant. The flexible chain cable reinforcing material provided by the invention is a mining intrinsic safety type rapid solidification high polymer material with high toughness and high strength, is used for reinforcing a soft outburst coal seam, can permeate into a deep crack of the soft outburst coal seam, and is simple to operate and good in safety.
Owner:CHONGQING UNIV +1

Application of piperidinyl polyamine in carbon dioxide capture

The invention provides application of piperidinyl polyamine in carbon dioxide capture, and relates to the technical field of carbon dioxide capture. The piperidinyl polyamine provided by the invention has additional amino groups or hydroxyl groups which are bonded on a ring instead of in the ring, and can strengthen anti-volatility by promoting intermolecular hydrogen-bond interaction while constructing a synergistic effect of multiple active sites, so that the dual effects of improving reaction activity and reducing volatilization loss are achieved. The piperidinyl polyamine combined absorbent composed of the piperidinyl polyamine and water has the advantages of large absorption capacity and low volatilization loss.
Owner:DALIAN UNIV OF TECH

Drinking water difunctional filtering carbon material as well as preparation method and application thereof

The invention belongs to the technical field of drinking water purification materials, and discloses a drinking water difunctional filtering carbon material which is capable of efficiently removing heavy metals, high in mineral substance retention rate and high in safety, and a preparation method and application of the drinking water difunctional filtering carbon material. The preparation method comprises the following steps: (1) mixing a primary carbonized material, a binder, a pore forming agent and a transition metal salt solution, kneading and forming, and drying to obtain a green body; (2) sequentially carrying out secondary carbonization treatment and thermal activation treatment on the green body, cooling, washing with water until the conductivity of a washing solution is constant, and drying to obtain a porous carrier; (3) immersing the porous carrier in the oxidation modification solution, carrying out solid-liquid separation, washing with water, and drying to obtain a porous oxidation carrier; and (4) immersing the hot porous oxidation carrier in the alkaline polyamine modified solution, adjusting the pH value of the mixture to be close to neutral when the temperature is reduced to room temperature, carrying out solid-liquid separation, and carrying out heat treatment to obtain the drinking water dual-function filtering carbon material, wherein the temperature of the porous oxidation carrier is higher than that of the alkaline polyamine modified solution.
Owner:成都达奇科技股份有限公司

Application of engineered citrobacter freundii in fermentation synthesis of stabilizers

The invention discloses an application of engineered citrobacter freundii in fermentation synthesis of a stable body. The engineered citrobacter freundii is citrobacter freundii overexpressing a polyphosphate kinase gene Ppk1. The stable body prepared by fermenting the engineered citrobacter freundii is rich in polyphosphates and polyamines, particularly, the content of the polyamines can be up to 21wt%, the polyphosphates in the stable body can store the polyamines in an ionic bond combination mode, the combined polyamines are insoluble in water, a natural anion coating is generated, and the stability of the stable body is improved. And the sustained-release tablet is not easily taken by intestinal epithelial cells, so that the sustained-release tablet has a certain sustained-release effect. The medicine prepared by taking the compound as a main active ingredient shows a remarkable curative effect in ulcerative colitis treatment, has the comprehensive effects of reducing oxidative stress, enhancing the anti-inflammatory ability of a body and regulating immunity, is suitable for patients of all ages, and has outstanding application value and market prospect.
Owner:NANJING UNIV

Reverse osmosis membrane with ultrathin functional layer and preparation method of reverse osmosis membrane

The invention belongs to the technical field of reverse osmosis membranes, and particularly relates to a preparation method of a reverse osmosis membrane with an ultrathin functional layer, which comprises the following steps: (1) preparing a membrane casting solution; (2) forming an ultrafiltration porous support layer; (3) forming a polyamide / polyester functional layer: sequentially contacting the ultrafiltration support layer with an organic phase solution I containing a polyamine / polyphenol monomer and an acid-binding agent and an organic phase solution II containing polyacyl chloride; (4) post-treatment; (5) drying; in the interfacial polymerization process, a strong-polarity organic solvent is adopted to replace pure water to serve as a carrier solvent of polyamine / polyphenol, the limitation of a traditional water / oil interface is broken through, and the method has the advantages that the monomer selection range is greatly expanded, a functional layer is ultrathin, the surface smoothness is improved, hydrolysis of multi-acyl chloride is avoided, the crosslinking degree of the functional layer is improved, and the service life of the functional layer is prolonged. The surface charge property of the membrane is improved, the process is simple, commercialized popularization is easy, and the comprehensive performance of the membrane is improved.
Owner:VONTRON TECH CO LTD

Polyamide composite membrane containing amino-carboxyl bifunctional COFs (covalent organic frameworks) as well as preparation method and application of polyamide composite membrane

The invention belongs to the technical field of membrane separation, and particularly relates to a polyamide composite membrane containing amino-carboxyl bifunctional COFs as well as a preparation method and application of the polyamide composite membrane. The preparation method comprises the following steps: by taking 1, 3, 5-tri (4-aminophenyl) benzene, 4, 4 '-diaminobiphenyl-2, 2'-dicarboxylic acid and 1, 3, 5-trialdehyde phloroglucinol as monomers, carrying out solvothermal reaction to prepare a bifunctional COFs material rich in amino groups and carboxyl groups at the same time; the preparation method comprises the following steps: dispersing a COFs material in a water phase containing polyamine, and carrying out interfacial polymerization on the water phase and an oil phase containing polyacyl chloride to prepare the composite membrane. COFs are firmly anchored in a polyamide network through a covalent reaction between amino and an acyl chloride monomer, so that the problems that the COFs are easy to fall off and non-uniform in dispersion are solved; the water flux is improved by regular pore channels of COFs, the membrane is endowed with strong hydrophilicity and electronegativity by carboxyl, the desalination rate and the pollution resistance are remarkably enhanced, and the COFs-based composite membrane has a wide application prospect in seawater desalination and high-salinity wastewater treatment.
Owner:BEIJING JIUZHANG ENVIRONMENTAL ENG CO LTD

Thiourea-polyamine polycondensate, epoxy adhesive and preparation method of thiourea-polyamine polycondensate

The invention relates to a thiourea-polyamine condensation polymer, an epoxy adhesive and a preparation method of the thiourea-polyamine condensation polymer, and the thiourea-polyamine condensation polymer is obtained by reacting thiourea with 3, 3 '-dimethyl-4, 4'-diaminodicyclohexylmethane. According to the preparation method, thiourea is used for modifying 3, 3 '-dimethyl-4, 4'-diaminodicyclohexylmethane under a proper condition, so that the modified thiourea-polyamine condensation polymer is obtained. The modified thiourea-polyamine polycondensate is simple in preparation process and high in yield. Moreover, the modified thiourea-polyamine polycondensate can be used as a chain extender for preparing an epoxy adhesive, the impact toughness and tensile property of the epoxy adhesive can be remarkably improved, the epoxy adhesive has better heat resistance, and the application field and scene of the epoxy adhesive are expanded.
Owner:GUANGZHOU BAIYUN CHEM IND +1

Bi-component epoxy coating, wire winding, preparation method of wire winding and electric reactor

The invention relates to a bi-component epoxy coating, a wire winding, a preparation method of the wire winding and an electric reactor. The bi-component epoxy coating comprises an epoxy prepolymer, an epoxy curing agent and a self-repairing microcapsule, wherein the self-repairing microcapsule contains an epoxy microcapsule and an amine microcapsule; wherein the amine microcapsule and the capsule wall of the epoxy microcapsule comprise polyurea, so that core liquid of the epoxy microcapsule and the amine microcapsule can be effectively preserved during primary thermocuring, and is not easy to flow out in advance. When the coating has cracks, bisphenol F diglycidyl ether in the amine microcapsules and aliphatic polyamine in the epoxy microcapsules can flow out and are gradually mixed, due to the high reaction activity of the aliphatic polyamine, secondary curing can be achieved without high temperature, microcracks can be repaired, further spreading of defects is prevented, and the service life of the coating is prolonged. And the long-term service capability of the self-repairing resin layer is effectively improved.
Owner:GUANGZHOU POWER SUPPLY BUREAU GUANGDONG POWER GRID CO LTD

Nitrogen-phosphorus intumescent flame retardant based on hypophosphorous acid derivative and oligomerization Schiff base as well as preparation method and application of nitrogen-phosphorus intumescent flame retardant

The invention discloses a nitrogen-phosphorus intumescent flame retardant based on a hypophosphorous acid derivative and oligomerization Schiff base as well as a preparation method and application thereof, and relates to the technical field of macromolecular flame-retardant materials. The invention discloses a nitrogen-phosphorus intumescent flame retardant based on a hypophosphorous acid derivative and oligomeric Schiff base. The nitrogen-phosphorus intumescent flame retardant has a structure as shown in a general formula (I), wherein the Schiff base chain segment is an oligomerization Schiff base chain segment formed by condensation of aromatic polyamine and aromatic polyaldehyde and has a linear or hyperbranched structure, m, n and x are positive integers larger than 0, m + n is larger than or equal to 2 and smaller than or equal to 8, and x is larger than or equal to 2 and smaller than or equal to 30. According to the flame retardant provided by the invention, an oligomer structure and an introduced benzene ring structure have good compatibility with a polymer matrix and are not easy to migrate and separate out, so that long-acting flame retardance and mechanical properties of a material can be maintained, expensive DOPO is successfully replaced by hypophosphorous acid which is low in cost and easy to obtain, and a solid foundation is laid for large-scale industrial popularization and application.
Owner:GUANGDONG SHUNDE TONGCHENG NEW MATERIALS TECH CO LTD

Silver-coated copper powder and preparation method thereof

The invention discloses silver-coated copper powder and a preparation method thereof, and the preparation method comprises the following steps: etching copper powder by using a composite alkaline reagent to obtain pretreated copper powder; the composite alkaline reagent is a mixed solution containing a surfactant and aliphatic polyamine; preparing a copper solution by using the pretreated copper powder; and dropwise adding the silver plating solution into the copper solution, and carrying out chemical silver plating reaction to obtain the silver-coated copper powder. Compared with the prior art, the method has the advantages that the chemical silvering reaction is a one-step method and can be achieved in a single container, the chemical silvering reaction is short in time and can be completed within 60 min, the prepared silver layer is compact under the resolution ratio of 5 nm, the silver content in the silver-coated copper powder is adjustable within the range of 15 wt%-60 wt%, the silver ion utilization rate is close to 100%, and the temperature process window is wide.
Owner:ZHEJIANG UNIV

Calcium hydroxide and industrial wastewater co-treatment method

The invention discloses a calcium hydroxide and industrial wastewater co-treatment method, and relates to the technical field of environmental engineering, and the method comprises the following steps: S100, adopting global dynamic light scattering and electromotive force imaging combined monitoring, and monitoring surface charge change and particle size evolution of nanoparticles in industrial wastewater in a calcium hydroxide adding process in real time, and extracting a dynamic threshold index of dispersion stability mutation. According to the invention, a dispersion stability threshold is extracted through dynamic light scattering and electromotive force imaging, a particle dispersion risk index is constructed, real-time evaluation of aggregation failure of nanoparticles and dynamic prediction of a feeding strategy are realized, linkage feeding of a chelating organic polyamine flocculant is combined, bridging and surface energy mutation are blocked, and stability of charges and particle sizes is maintained. By means of closed-loop feedback and on-line early warning, the adding proportion is optimized, the gathering and settling efficiency is improved, membrane pollution and filtering blockage are reduced, and the stability and economical efficiency of wastewater treatment are improved.
Owner:DEXING LONGSHENG CALCIUM CARBONATE CO LTD

A polymer flooding crude oil produced fluid demulsifier, its preparation method and application

PendingCN122326275ADemulsifierDiethylene glycol
This invention discloses a demulsifier for polymer flooding crude oil produced fluids, its preparation method, and its application, belonging to the field of chemical additives for petrochemicals. The technical solution includes a main agent, an auxiliary agent, a penetrant, and water; the main agent is a polyene-polyamine block polyether, the auxiliary agent is a triethanolamine block polyether quaternary ammonium salt, and the penetrant is selected from at least one of methanol, ethanol, ethylene glycol, and diethylene glycol butyl ether; in the demulsifier, the ratio of the main agent to the auxiliary agent is 4-9:1, the amount of penetrant is 30% of the total amount of the main agent and auxiliary agent, and the amount of water is 70% of the total amount of the main agent and auxiliary agent. This invention, applied to demulsification of polymer flooding crude oil produced fluids, features high demulsification efficiency and rapid demulsification effect.
Owner:DONGYING JINMEI CHEM CO LTD +1

Post-treatment method of reverse osmosis membrane and reverse osmosis membrane

The present application relates to a reverse osmosis membrane post-processing method and a reverse osmosis membrane, wherein the reverse osmosis membrane post-processing method comprises the following steps: sequentially placing a reverse osmosis membrane prepared by an interfacial polymerization method in an acid solution containing a dialdehyde, water, an alkaline solution and a hydroxyl polyethylene glycol mercapto aqueous solution for cleaning treatment, wherein the hydroxyl polyethylene glycol mercapto aqueous solution is acidic. The reverse osmosis membrane post-processing method can effectively reduce the content of amino groups and polyamines on the reverse osmosis membrane while still having the performance of high retention and high water flux.
Owner:BLUESTAR (HANGZHOU) MEMBRANE IND CO LTD +1

Laminates and packaging materials

To provide a laminate that is highly recyclable and has excellent heat-sealing properties. [Solution] A laminate comprising at least a base layer, an adhesive layer, and a sealant layer in this order, wherein a protective layer is provided on the outermost side of the base layer, the protective layer is made of a thermosetting resin, both the base layer and the sealant layer are made of polyethylene resin, the base layer has a probe drop temperature of 180°C or higher, the proportion of polyethylene in the laminate is 90% by mass or higher, and the adhesive layer is formed from a polyamine-based adhesive or a urethane-based adhesive having gas barrier properties.
Owner:TOPPAN HOLDINGS INC

High-thermal-stability epoxy amine adduct, single-component pouring sealant and preparation process

The invention discloses a high-thermal-stability epoxy amine adduct, a single-component pouring sealant and a preparation process of the high-thermal-stability epoxy amine adduct, the high-thermal-stability epoxy amine adduct is prepared by reacting a single-epoxy compound containing a cyclic structure, aromatic polyamine and a double-epoxy compound containing a flexible chain segment according to a specific molar ratio, and the molecular structure of the high-thermal-stability epoxy amine adduct has rigidity, flexibility and latency; the single-component pouring sealant taking the addition product as a curing agent comprises epoxy resin, the addition product, inorganic filler, a silane coupling agent and the like, the pouring sealant can be stably stored at room temperature, a three-dimensional network structure formed after heating and curing is compact, and the pouring sealant has high glass transition temperature, high thermal decomposition temperature and excellent long-term thermal aging performance; and the epoxy resin is especially suitable for potting protection of electronic components with extremely high requirements on heat resistance and reliability.
Owner:SHENZHEN DST TECH CO LTD