78 results about "Polyamine Compound" patented technology

The invention provides a carrier material as well as a preparation method and application thereof, the preparation method of the carrier material comprises the following steps: 1) mixing a mixed solution containing a polyhydroxy compound and / or a polyamine compound, polycarboxylic acid and a metal source with a porous material to obtain a mixed system; wherein the mass of the mixed solution is 40-60% of the mass of the porous material; and 2) carrying out post-treatment including polymerization treatment, drying treatment and roasting treatment on the mixed system to obtain the carrier material. According to the preparation method of the carrier material provided by the invention, metal ions enter the pore channels of the porous material, the metal material can be uniformly distributed on the inner surfaces of the pore channels under the pore channel confinement effect, and the carrier material is applied to a catalyst, so that the temperature of a catalytic oxidation reaction of a volatile organic compound can be reduced.

A paving material composition containing: an epoxy resin; an epoxy resin curing agent containing a reaction composition (A) containing a reaction product of styrene and a polyamine compound represented by the following formula (1); and an aggregate.wherein X is a phenylene group.

The invention provides a waterborne epoxy curing agent based on enamine bonds as well as a preparation method and application of the waterborne epoxy curing agent, and belongs to the technical field of coatings. The waterborne epoxy curing agent based on the enamine bond is prepared from the following raw materials in parts by weight: 12 to 14 parts of a polyepoxy compound, 7 to 12 parts of a polyamine compound, 37 to 42 parts of a polyether-based polyacetoacetate compound, 9 to 14 parts of a diacetoacetate compound, 5 to 7 parts of a monoacetoacetate compound and 20 to 50 parts of a solvent. According to the waterborne epoxy curing agent constructed through enamine bonds, the free amine content of the obtained waterborne epoxy curing agent can be effectively reduced, and the activation period of the waterborne epoxy curing agent during use is prolonged.

A process for preparing polyamines via (meth)acrylonitrile and / or crotononitrile addition to an amine followed by hydrogenation in the presence of a catalyst and hydrogen and optionally in the additional presence of ammonia, primary and / or secondary amine, comprises a) reacting at least one amine of general formula (I) with (meth)acrylonitrile and / or crotononitrile, thereby obtaining at least one first intermediate (I1), b) hydrogenating the at least one first intermediate (I1) to at least one polyamine compound (II), or hydrogenating the at least one first intermediate (I1) in the additional presence of ammonia, primary and / or secondary amine.

Embodiments of the present disclosure generally relate to epoxy resin compositions and uses thereof. The epoxy resin composition includes an epoxy component including a first epoxy compound and a second epoxy compound. The epoxy resin composition includes a curing agent component including a first polyamine compound and a second polyamine compound.

The invention discloses a clay stabilizer for a polymer dry powder direct distribution variable-viscosity fracturing fluid. The clay stabilizer is prepared from quaternary ammonium salt, an alcohol amine compound and a polyamine compound as raw materials in a solvent. The quaternary ammonium salt is quaternary ammonium salt with the carbon chain length of C12-C18; the alcohol amine compound is selected from at least one of ethanolamine, dimethyl propanolamine, hydroxyethyl piperazine, piperidine, isopropanolamine, triisopropanolamine, aminomethyl propanolate, hydroxyethyl ammonium salt and the like; the polyamine compound is selected from any one of poly dimethyl diallyl ammonium chloride, polyquaternary ammonium salt, poly allylamine, polyurea, polybutanediamine, polyethyleneimine, polyethylene polyamine and a polyethyleneimine cross-linked substance. The clay stabilizer disclosed by the invention is particularly suitable for polymer dry powder direct distribution variable-viscosity fracturing fluid, the stability of clay can be remarkably improved, particularly, excellent inhibition performance can still be kept under high-temperature and high-salt conditions, stratum damage is reduced, and the application requirements in complex environments of oil fields are met.

The invention relates to the technical field of rice stress-resistant cultivation, and discloses a rice root system salt tolerance adjusting method based on exogenous spermidine, which comprises the following core steps: in the critical period of rice root system development, directionally applying a spermidine solution subjected to purity verification to a rice root system area, by accurately regulating and controlling the application concentration, frequency, duration and application environment conditions of spermidine, the osmotic regulation capability and the anti-oxidation system function of a rice root system in a high-salt environment with the soil conductivity larger than or equal to 2 dS / m are improved, the salt tolerance of the root system is remarkably improved, and then growth and development of rice are guaranteed. The spermidine is a straight-chain polyamine compound with good biocompatibility, the chemical purity is not lower than 98%, no heavy metal is left, and the contents of lead, cadmium and mercury are all smaller than or equal to 0.1 mg / kg. According to the invention, precise targeted regulation and control of the salt tolerance of the rice root system are realized, and the regulation effect is stable and remarkable.

The application belongs to the field of engineering plastics, and particularly relates to long-chain polyamide resin with easy processing and high tensile property, and a preparation method and application thereof. The long-chain polyamide resin comprises the following raw material components: component a: aliphatic carboxylic acid compound component; component b: polyamine compound component; and component c: a compound with a structure shown in the following formula (1), wherein n and m can be any number between 1 and 10. The long-chain polyamide resin of the application introduces structural diacid with an asymmetric benzene ring structure, utilizes the asymmetric structure to reduce the crystallinity of the material, and introduces the benzene ring structure to improve the mechanical property of the polyamide material, so that the low processing temperature is realized from the polyamide material component itself, the energy consumption is reduced, and the mechanical property of the polyamide material is ensured. The problem that the processing temperature and mechanical property of the polyamide material and the processing energy consumption are difficult to be considered in the prior art is solved.

The invention relates to the technical field of high polymer materials, and discloses a temperature latent curing agent and a preparation method thereof.The curing agent is prepared from a polyamine compound and a polythiol compound through a proton transfer reaction at the temperature of 15-30 DEG C. In the reaction, the molar ratio of active amine hydrogen to thiol groups is 1: (0.9-1.1), and a stable ion pair structure is formed. The invention also discloses a single-component epoxy curing system containing the curing agent, epoxy resin and a dielectric constant jump additive. The system is endowed with excellent storage stability by utilizing an ion pair structure; meanwhile, after heating, the compatibility of the dielectric constant jump additive and the epoxy resin is changed, and the dielectric constant of the system is triggered to rise, so that ion pair constraint is weakened, and the curing agent is dissociated and rapidly cured at a moderate temperature. According to the technology, the contradiction between latency and curing conditions is solved, and a cured product has good thermal and mechanical properties.

The invention discloses a polymer gel profile control and displacement system and a preparation method thereof, and belongs to the technical field of chemical oil displacement. The profile control and flooding system is prepared by the following method: reacting methyl allyl polyoxyethylene ether with 4-(2-bromoethyoxyl) benzaldehyde to obtain a functional monomer containing an aldehyde group; polymerizing a functional monomer containing an aldehyde group and acrylamide to obtain a polymer rubber block, hydrolyzing the rubber block, continuously drying, and crushing to obtain dry polymer powder containing the aldehyde group; and mixing the dry powder with a multi-primary amine compound cross-linking agent according to a mass ratio of 1: 0.6-1: 1 to form a polymer gel profile control and flooding system with good salt tolerance. In the profile control system disclosed by the invention, polymer gel with higher cross-linking strength can be formed between the aldehyde group-containing polymer and the multi-primary amine compound under the dual action of primary amine, the aldehyde group and the amide group; the gel formed by the aldehyde group-containing polymer and the multi-primary amine compound has better salt tolerance.

The application discloses an LED chip roughening liquid and a preparation method and application thereof, and belongs to the field of surface roughening of semiconductor material multi-element metal compounds. The roughening liquid comprises inorganic acid, organic acid, polyamine compound, oxidizing agent, wetting agent and the like; by adding a perfluorinated surfactant with high stability and low surface tension, the roughening interface tension is effectively reduced, the roughening product and bubbles are quickly separated from the reaction interface, the roughening interface is promoted to be in a uniform state, the problem of uneven roughening surface depth is effectively solved, the roughening surface quality is improved, the light output rate is effectively increased, and the LED light emitting intensity is improved. The roughening liquid can perform surface micro patterning on the LED chip under normal temperature conditions to form a concave-convex rough surface. The roughening agent is easy to operate and low in cost, the reaction condition is normal temperature and easy to control, and can be applied to industrial production.

A paving material composition containing:an epoxy resin:an epoxy resin curing agent containing 50% by mass or more of a polyamine compound represented by the following formula (1) or a modified product thereof. (A); and an aggregate.wherein X is a cyclohexylene group.

The purpose of the present invention is to provide a cement additive which can improve the strength of carbon dioxide gas fixation concrete. The present invention is a cement additive used in a cement composition for carbon dioxide fixation. The cement additive contains a compound represented by formula (1) and / or a polyamine compound (A1) which is a heterocyclic polyamine. (In the formula, R1, R2, R3, R4, R5 and R6 are the same or different, and represent a hydrogen atom or a hydrocarbon group having one or more carbon atoms; n and m are the same or different, and represent an integer of 0 or more; the number of nitrogen atoms included in formula (1) is 2-6; x1 and x2 are the same or different, and represent an integer of 0 or more; and P is the same or different, and represents a hydrogen atom or a structural unit having a separate amino group due to branching.)

The invention relates to a porous polymer material and a preparation method and application thereof.The preparation method comprises the steps that firstly, a compound containing sulfydryl and thiolactone is designed and synthesized, a mixed solution of the compound, a polar solvent and a surfactant serves as a continuous phase, a non-polar solvent serves as a dispersion phase, oil-in-oil type high-internal-phase emulsion is formed after emulsification, and the porous polymer material is obtained; and reacting with a polyamine compound to obtain the sulfydryl-containing porous polymer material. The prepared porous material can adsorb heavy metal ions in water and can be used in the field of water treatment.

The invention relates to the technical field of concrete admixtures, in particular to a high-performance cross-linked cationic concrete air entraining agent and a preparation method thereof. The preparation process of the air entraining agent comprises the following steps: under the protection of inert atmosphere, carrying out reflux reaction on a polyamine compound and brominated alkane, and then mixing and emulsifying with an emulsifier and a sodium citrate solution to obtain pre-emulsified liquid; mixing the pre-emulsion with hydrophilic polyoxyethylene ether, an initiator and a phosphate modifier, and carrying out initiation cross-linking reaction by adopting ultraviolet irradiation to obtain an intermediate product; mixing and stirring the intermediate product with a micro-nano bubble solution, pretreated nano cellulose and a foam stabilizer, and then performing reduced pressure distillation and filtration to obtain an air entraining agent; a highly uniform and stable micro-nano bubble system is formed in the concrete, the air entraining agent can significantly improve the freeze-thaw cycle resistance, mechanical strength and durability of the concrete, and the preparation process is mild in condition and environmentally friendly.

A method of producing a polyamine compound, the method including: a first step of generating a polyurea compound by reacting a thiourethane resin and an amine compound A with each other; and a second step of generating a polyamine compound by reacting the polyurea compound and an amine compound B with each other.

The invention relates to a nanocapsule with high transparency as well as a preparation method and application thereof. The preparation method comprises the following steps: carrying out polymerization reaction on a polyisocyanate compound, at least one hydrophilic diol compound and at least one hydrophobic diol compound to form an amphiphilic block copolymer with an isocyanate end group; the preparation method comprises the following steps: dissolving an amphiphilic block copolymer and an active component into a water-soluble organic solvent, dropwise adding deionized water or an organic solvent at a speed of 10-100 mL / min under mechanical stirring, and carrying out self-emulsification to form a uniformly dispersed dispersion; and adding a polyamine compound into the dispersion, and carrying out a cross-linking reaction to form the nanocapsule. Through material design and a process route, the contradiction that high-activity component loading capacity and high optical transparency cannot be achieved at the same time in the field of nano carriers is systematically solved.

This invention relates to the field of microencapsulation technology, and more specifically, to an organic-inorganic hybrid sustained-release fragrance microcapsule and its preparation method. By weight percentage, the components include: 10-35% fragrance oil, 1-10% silane precursor, 0.01-2% silane coupling agent, 1-15% polyisocyanate, 0.01-10% emulsifier, 0.01-10% polyamine compound, and deionized water to make up the balance. Through the combination of sol-gel and interfacial polymerization methods, the stability of the fragrance is improved, making it less prone to volatilization or decomposition during long-term storage or under different environments, effectively preventing direct contact between the fragrance and air, thereby prolonging the duration of the aroma. During use, the organic-inorganic hybrid fragrance microcapsule releases active substances through sustained release, reducing environmental pollution and diffusion.

Provided are an epoxy resin adhesive for a medical device and its cured product, and a medical device member and a medical device. The epoxy resin adhesive includes the following components (A) to (C):(A) an epoxy resin;(B) a polyamine compound having two or more unsubstituted amino groups; and(C) a compound having a nonaromatic carbon-carbon double bond group and a phenolic hydroxy group.

The present disclosure provides a reaction system for producing a polymer, the reaction system comprising: side A) an isocyanate component comprising a polyisocyanate compound; and side B) an isocyanate-reactive component comprising: a polyol compound, a polyamine compound, or a mixture thereof; and a polyurea-containing compound represented by structure (1), wherein X is a substituted or unsubstituted aromatic group, a substituted or unsubstituted aliphatic group, a substituted or unsubstituted alicyclic group, or a substituted or unsubstituted polymeric group; R' is H or a substituted or unsubstituted hydrocarbon group which may contain one or more unsaturated carbon to carbon bonds and / or one or more heteroatoms in a main chain of the hydrocarbon group; Y is a substituted or unsubstituted hydrocarbon group which may contain one or more unsaturated carbon to carbon bonds and / or one or more heteroatoms in a main chain of the hydrocarbon group; R'' is an isocyanate-reactive group; and n is from 2 to 10.

The application belongs to the technical field of CO2 adsorption materials, and discloses an amine modified mesoporous activated carbon for CO2 adsorption with high adsorption capacity and excellent cycle stability and a preparation method thereof. The preparation method of the amine modified mesoporous activated carbon for CO2 adsorption comprises the following steps: (1) kneading and forming bamboo charcoal powder, a binder and a dispersing agent to obtain a green body; (2) performing carbonization treatment on the green body to obtain carbonized material; (3) performing one-stage activation treatment on the carbonized material to obtain a precursor; (4) performing two-stage activation treatment on the precursor to obtain mesoporous activated carbon; (5) performing amine modification treatment on the mesoporous activated carbon by using a polyene polyamine compound and a crosslinking agent to obtain the amine modified mesoporous activated carbon; wherein the one-stage activation treatment and the two-stage activation treatment are continuous water vapor heat activation treatments, the one-stage activation treatment temperature is higher than the two-stage activation treatment temperature, and the water vapor consumption of the one-stage activation treatment is less than that of the two-stage activation treatment.

This invention discloses a modified polyester nonwoven fabric, its preparation method, a filter assembly, and a filter cartridge. The modified polyester nonwoven fabric comprises an amine-containing polyester nonwoven fabric and a three-dimensional network; the amine groups are derived from amine monomers; the amine monomers contain at least two amine groups; the three-dimensional network originates from a chemical reaction between tannic acid and a polyamine compound; the polyester nonwoven fabric and the three-dimensional network are connected by amide groups formed by the chemical reaction between the amine groups and the polyester nonwoven fabric, and by chemical bonds formed by the chemical reaction between tannic acid and the amine groups; the three-dimensional network also includes adsorption sites; the adsorption sites are formed by the complexation reaction of metal salts with tannic acid and polyamine compounds to form coordinate bonds, followed by breaking the coordinate bonds using an acidic solution with a pH of 3-4. This modified polyester nonwoven fabric, filter assembly, and filter cartridge exhibit good heavy metal adsorption performance and a long heavy metal adsorption lifespan, while also retaining beneficial minerals and removing organic matter.

This invention belongs to the field of polyamide resin technology, and particularly relates to a polyamide resin, its preparation method, and its application. The polyamide resin comprises the following raw materials: a) carboxylic acid compounds; b) polyamine compounds; c) compounds with the structure shown in formula (I); in formula (I), R is selected from H or hydroxyl groups. The polyamide resin obtained by this invention not only has good alcohol solubility and water resistance, but also high heat resistance and good adhesion to substrates.

In some aspects, the present disclosure relates to a system for forming a hydrogel composition comprising a first reservoir containing an iodinated polymer composition, a second reservoir containing a buffer diluent solution having a first pH, and a third reservoir containing a buffer accelerator solution having a second pH higher than the first pH, the iodinated polymer composition includes an iodinated polymer having a plurality of cyclic imide ester groups, the buffer diluent solution includes water, a first buffer, and a polyamine compound, and the buffer accelerator solution includes water and a second buffer. Other aspects of the present disclosure relate to methods of forming hydrogel compositions using such systems.

The application provides an oleic acid modified polyene polyamine compound, a preparation method and application thereof, and a chemical structural formula of the compound is shown in formula I: in the formula, n is a positive integer greater than or equal to 1 and less than or equal to 10. The compound can improve the process performance of a solid propellant and also can improve the mechanical property of the solid propellant.

This invention relates to an acid-resistant electro-driven thin film for electro-driven separation, its preparation method, and its application. The preparation method includes the following steps: (1) Base film activation: The base film is activated sequentially with water, alkaline solution, and acid solution to obtain an activated base film; (2) Interfacial polymerization reaction: The activated base film is sequentially immersed in an aqueous phase solution and an organic phase solution, and then subjected to heat treatment to obtain the acid-resistant electro-driven thin film; The aqueous phase solution includes a polyamine compound; The organic phase solution includes an organic solvent and an organic monomer, The organic monomer includes cyanuric chloride and terephthalic diisocyanate. This invention obtains an acid-resistant electro-driven thin film with excellent conductivity and acid resistance and a reasonable pore structure by combining the base film activation process with the interfacial polymerization reaction of polyamine compounds in the aqueous phase solution and cyanuric chloride and terephthalic diisocyanate in the organic phase solution. This enables efficient separation between ions under acidic and electro-driven conditions.

The present application belongs to the technical field of biomedical functional materials, and particularly relates to a multifunctional drug structure coating with regulation of lesion microenvironment homeostasis and a preparation method thereof. The nano drug carrier can load drugs with anti-smooth muscle cell growth or regulation of inflammation, the drugs can resist the growth of smooth muscle cells or regulate microenvironment inflammation, and provide a stable and safe microenvironment for the adhesion and growth of endothelial cells. Under the action of an oxidizing agent, polyphenol and polyamine compounds undergo oxidation, crosslinking and polymerization reactions, and a polyphenol nanoparticle (10 nanometer level) film layer is generated outside the nano drug carrier (100 nanometer level). The polyphenol nanoparticle film layer not only serves as a protective layer for the nano drug carrier and crosslinking substances therebetween, but also can fix the nano drug carrier on the surface of a base material, and together with the drug carrier, a drug structure coating with a topological structure is constructed. The hydrophilic groups contained in the coating make the surface super-hydrophilic and negatively charged.

The invention belongs to the technical field of high polymer materials, and discloses a Janus cage, a preparation method of the Janus cage, a Janus cage compound and application of the Janus cage compound. The Janus cage is a Janus silicon dioxide cage with an oleophylic group on the outer side and a hydrophilic group on the inner side, and the inner side of the Janus cage is grafted with an amino polymer or a polyamine compound or coated with a water-soluble amino polymer. The preparation method of the Janus cage comprises the following steps: carrying out an interface sol-gel reaction on a water-in-oil emulsion to obtain a Janus silicon dioxide cage of which the outer side is oleophylic and the inner side is hydrophilic, and grafting an amino polymer or a polyamine compound on the inner side of the Janus cage; or carrying out an interface sol-gel reaction through a water-in-oil emulsion to obtain the Janus silicon dioxide cage which is oleophylic on the outer side and hydrophilic on the inner side and is coated with the water-soluble amino polymer. The Janus cage compound disclosed by the invention has good dispersity and efficient CO2 trapping capacity in a polyolefin matrix and a foaming material.

The application discloses a kind of nanoparticles with multi-amino active groups, organic-inorganic composite crosslinking agent and preparation method and application, organic-inorganic composite crosslinking agent is with nano-alumina, nano-zirconia and other nanoparticles as carrier, graft polyamine compound on the surface of nanoparticle by catalytic reaction, and organic-inorganic composite nanometer crosslinking agent with delaying function can be prepared by composite crosslinking control agent.The molecular structure of the synthesized organic-inorganic composite crosslinking agent has rigid benzene ring structure and rich active groups, so it has good temperature resistance and activity.Compared with conventional crosslinking agent, the activity is higher, and it can also react with amide group and carboxyl group on polymer molecule at low temperature;By adjusting the amount of crosslinking control agent, the gelation time and strength of the system can be controlled to meet different construction requirements of oilfield site;Synthetic nanometer crosslinking agent is green and environmentally friendly, and meets the requirements of green medicine, and can be applied to water plugging and profile control in medium-low temperature reservoirs.

The present invention relates to a process for treating keratin fibers using a basic pH composition, one or more compounds with acetoacetate functions and one or more specific polyamine compounds.