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155 results about "Tetramine" patented technology

Tetramine is a typical name for a chemical containing four amine groups. Tetramine is also used as a synonym for the tetramethylammonium cation.

Diffusion plate printing quantum dot ink and preparation method thereof

PendingCN120098484AInksPolymer scienceMeth-
The invention relates to the field of quantum dot ink, and discloses diffusion plate printing quantum dot ink and a preparation method thereof.The diffusion plate printing quantum dot ink comprises acrylic resin, hyperbranched polyester resin, a quantum dot material, modified boron nitride, a reactive diluent, a photoinitiator, a wetting agent and a defoaming agent; the hyperbranched polyester resin is prepared by reacting hyperbranched polyester acrylate and a sulfydryl-terminated silicon-containing reaction monomer, wherein the hyperbranched polyester acrylate is prepared by reacting pentaerythritol with 2, 2-dimethylolpropionic acid and then carrying out esterification reaction with acrylic acid; the sulfydryl-terminated silicon-containing reaction monomer is prepared by reacting eugenol with 1, 1, 3, 3-tetramethyldisiloxane and then carrying out esterification reaction with 3-mercaptopropionic acid; the modified boron nitride is prepared by modifying a cationic polymer which is prepared by carrying out a Mannich reaction on triethylene tetramine, formaldehyde and acetone and then carrying out a condensation polymerization reaction with formaldehyde. After the ink prepared by the invention is cured, a coating film is high in hardness, adhesive force and heat conductivity coefficient, and good in flexibility, heat resistance and migration barrier property.
Owner:SHENZHEN CHENGYUXING PHOTOELECTRICITY CO LTD

Photovoltaic POSS (Polyhedral Oligomeric Silsesquioxane)-containing antireflection film coating liquid and preparation method thereof

The invention discloses a photovoltaic POSS (polyhedral oligomeric silsesquioxane)-containing antireflection film coating liquid and a preparation method thereof, the coating liquid comprises the following raw materials in parts by weight: 80-100 parts of modified emulsion, 10-15 parts of modified graphene, 3-5 parts of sodium dodecyl benzene sulfonate, 1-3 parts of triethylene tetramine and 40-60 parts of deionized water, a modified additive in the coating liquid contains a polyhedral oligomeric silsesquioxane structure, the polyhedral oligomeric silsesquioxane structure can form uniformly-distributed nanopores and is matched with a two-dimensional honeycomb lattice structure in the graphene oxide, the surface roughness can be increased, the microstructure can scatter incident light and reduce specular reflection, so that the surface light transmittance is improved, and meanwhile, the modified additive molecule contains a fluoroalkyl structure, so that the surface light transmittance is improved. The fluoroalkane has a high refractive index, so that light reflection can be reduced, and the light transmittance is further improved.
Owner:NINGBO OSDA SOLAR CO LTD

Nitrogen-doped zinc ion battery manganese-based positive electrode material and preparation method and application thereof

The invention discloses a nitrogen-doped zinc ion battery manganese-based positive electrode material and a preparation method and application thereof, and the preparation method comprises the following steps: mixing a strong oxidant and a manganese salt, putting the mixture into a beaker, adding deionized water, and uniformly stirring to form a mixed solution; transferring the mixed solution into a high-pressure reaction kettle with a polytetrafluoroethylene lining, and heating the high-pressure reaction kettle in a drying oven; cooling, precipitating, filtering and washing for multiple times, and then putting into a drying oven for vacuum drying to obtain an original manganese-based positive electrode material; the preparation method comprises the following steps: respectively weighing an original manganese-based positive electrode material and hexamethylenetetramine, flatly laying the original manganese-based positive electrode material at the bottom of a lining of a reaction kettle, and putting the hexamethylenetetramine into a beaker; and putting the beaker into a reaction kettle, moving the beaker and the reaction kettle into a drying oven, and heating to obtain the surface nitrogen-doped manganese-based positive electrode material.
Owner:HEBEI UNIVERSITY

Self-lubricating aluminum coating and preparation method thereof

The invention discloses a self-lubricating aluminum coating and a preparation method thereof.The preparation method comprises the steps that molybdenum disulfide is pretreated through a silane coupling agent, tetraethoxysilane mixed liquor is added, the pH is adjusted to be 9-10, a water bath reaction is conducted, and molybdenum disulfide-silicon dioxide microcapsules are obtained after high-temperature strengthening treatment; respectively adding a zinc nitrate solution and a hexamethylenetetramine solution, adjusting the pH value to 10-11, carrying out a high-temperature and high-pressure hydrothermal reaction to obtain zinc oxide nanorods, and carrying out ball milling treatment on the zinc oxide nanorods, microcapsules, stearic acid and zirconium oxide balls under the protection of argon to obtain doped microcapsules; after raw materials are pretreated, the raw materials and a dispersing agent solution are added into a mixer respectively, spraying powder, a pretreated base body and the spraying powder are obtained after mixing treatment, spraying treatment is conducted on the surface of the base body through a plasma spraying method, and the self-lubricating aluminum coating is obtained after vacuum annealing treatment. Therefore, the obtained self-lubricating aluminum coating is low in friction coefficient, high in performance and excellent in self-lubricating property.
Owner:SHENZHEN ASIA PACIFIC AVIATION TECH CO LTD

Compound corrosion inhibitor for CO2 oil displacement produced liquid and preparation method of compound corrosion inhibitor

The preparation method comprises the following steps: weighing oleic acid and a catalyst, adding the weighed oleic acid and catalyst into a reaction container, heating by stages by adopting a programmable electric heating jacket, respectively dropwise adding a water carrying agent at 80-100 DEG C, dropwise adding diethylenetriamine or triethylene tetramine at 110-130 DEG C, controlling the reaction temperature and time, and reacting for 2-4 hours to obtain the compound corrosion inhibitor for the CO2 oil displacement produced liquid. After water is separated out, further reaction is carried out at 200-230 DEG C, then the system is cooled to 60-70 DEG C, a quaternization reagent is added for reaction, and a corrosion inhibitor E and a corrosion inhibitor S are prepared respectively; finally, the corrosion inhibitor E and the corrosion inhibitor S are compounded according to a certain proportion, and the compound corrosion inhibitor for the CO2 oil displacement produced liquid is obtained. The preparation method is simple and easy to implement, and the cost can be reduced; when the prepared corrosion inhibitor is applied to CO2 oil displacement produced liquid corrosion inhibition, an excellent corrosion inhibition effect can be shown, and corrosion hazards in CO2 oil displacement application are greatly reduced.
Owner:CHINA UNIV OF MINING & TECH

Electrolytic silver germanium alloy plating solution

To provide an electrolytic silver germanium alloy plating solution capable of codepositing a sufficient amount of germanium in a film, having good liquid stability, and hardly causing foaming.SOLUTION: The problem is solved by an electrolytic silver germanium alloy plating solution containing a silver source and a germanium source characterized by containing a nitrogen-containing coordination compound having a molecular weight of 500 or less. Specific examples of the nitrogen-containing coordination compound include N,N-di(2-hydroxyethyl)glycine, diethanolamine, N,N-bis(2-hydroxyethyl)-2-aminoethanesulfonic acid, triethylenetetramine, glycine, tris(hydroxymethyl) aminomethane, N-methylglucamine, bis(2-hydroxyethyl)aminotris(hydroxymethyl)methane, tricin, N,N,N',N'-tetrakis(2-hydroxypropyl)ethylenediamine, and salts of these compounds.SELECTED DRAWING: None
Owner:JAPAN PURE CHEM

Preparation method and application of porous hydrogel adsorbent based on Radix Astragali residue

The present disclosure provides a preparation method of a porous hydrogel adsorbent based on Radix astragali residues, including the following steps: subjecting residues of Chinese herbal medicine Radix astragali as a precursor to bleaching with NaClO2, alkaline washing with KOH, and high power ultrasonic treatment, thereby obtaining a precursor solution of uniformly dispersed cellulose nanofibers (CNFs); adding the precursor solution of CNFs to a mixed solution of N,N′-methylene bisacrylamide (MBA), acrylic acid (AA) and ammonium persulfate (APS), shaking evenly, and initiating a polymerization reaction at a predetermined temperature to form a monolithic gel; and cleaning the monolithic gel, putting the cleaned monolithic gel into a dimethyl sulfoxide (DMSO) solution containing epichlorohydrin to allow reaction, and transferring the product of the reaction to an aqueous sodium hydroxide solution containing triethylene tetramine to allow reaction, thereby finally obtaining an amino-functionalized porous hydrogel adsorbent.
Owner:SHANGHAI JIAOTONG UNIV

Crystalline form of triethylenetetramine tetrahydrochloride and its pharmaceutical use

The present invention describes a new crystalline form of triethylenetetramine tetrachloride which has improved room temperature stability over known forms and over the dichloride salt. The new crystalline form is characterised by having peaks in an XRPD spectrum at 22.9, 25.4, 25.8, 26.6, 34.6 and 35.3±0.1°2θ and Raman shifts 943, 1173, 1527 and 1612±5 cm−1. The crystalline form of triethylenetetramine tetrachloride is useful in the treatment of Wilson's disease.
Owner:ORPHALAN SA

Method for carbon dioxide mineralization and carbon dioxide mineralization device

ActiveCN116637478BOrganic basePropylamine
The present application relates to a kind of carbon dioxide mineralization method and carbon dioxide mineralization device.The carbon dioxide mineralization method includes the following steps: mixing absorption liquid and industrial solid waste at room temperature, obtain mortar;Make mortar solid-liquid separation, obtain clear liquid and thick slurry;Carbon dioxide in flue gas is absorbed by clear liquid, obtain carbon-rich absorption liquid;Carbon-rich absorption liquid and thick slurry occur mineralization reaction at 180 DEG C-220 DEG C, obtain mineralized slurry;Make mineralized slurry solid-liquid separation, obtain mineralized ash and mineralized clear liquid;Wherein, absorption liquid includes inorganic base and organic base, organic base includes monoethanolamine, diethanolamine, triethanolamine, 3-methylaminopropylamine, N-methyl diethanolamine, piperazine, diethylene triamine, triethylene tetramine, tetraethylene pentamine and 2-amino-2-methyl-1-propanolamine at least two kinds.The method greatly improves CO2 capture rate and CO2 utilization rate, and organic base consumption is less, absorption liquid regeneration energy consumption is low, and overall economy is good.
Owner:GUANGZHOU ORIENTAL POWER CO LTD +1

A method for preparing a silica sol using an ion exchange method

The present application belongs to the technical field of silica sol preparation, and particularly relates to a silica sol preparation method using ion exchange method. In the prior art, the silica sol growth time is shortened by optimizing the preparation and impurity removal process, and the silica sol seed mother liquor is prepared under ultrasonic assistance. The organic alkali catalyst maintains the silica sol growth pH and the metal ions in the complex solution, so that the impurities are reduced during the silica sol growth. After the introduction of dodecyltrimethoxysilane, hexadecyltrimethoxysilane and methyltrimethoxysilane as the hydrophobic group surface modification, the impurity metal ions are filtered through the complexing agent and the ammonium type resin. The three ethylene tetramine ethanol solution modifies the ammonium type resin, enhances the selective adsorption of the resin to the metal ions, and the maleic anhydride crosslinking agent and nano silicon dioxide modify the ammonium type resin, increase the service life of the ammonium type resin. The prepared silica sol has high purity, good mechanical properties and dispersibility, and excellent hydrophobic performance.
Owner:HUBEI JIANS CHEMICAL NEW MATERIALS CO LTD

Environment-friendly wet strength agent and preparation method thereof

The invention relates to the technical field of paper wet strength agents, in particular to an environment-friendly wet strength agent and a preparation method thereof. The preparation method of the wet strength agent comprises the following steps: under the action of a catalyst, succinic acid, maleic acid and triethylene tetramine react to obtain an unsaturated polyamide polyamine prepolymer; adding water into the unsaturated polyamide polyamine prepolymer to adjust the solid content, heating, adding double-bond-containing nanocellulose, tea saponin, glycidyl acrylate and an initiator, and reacting to obtain an intermediate emulsion; cooling the intermediate emulsion to room temperature, adding epichlorohydrin to react for 0.5-3 hours, heating to 50-75 DEG C, continuing to react for 1-5 hours, cooling reaction liquid to 25-30 DEG C, adding glyoxal to react for 0.5-1 hour, adjusting the pH value of the reaction liquid after the reaction is completed, and adding water to adjust the solid content, thereby obtaining the product. The preparation method is simple in process, and the prepared wet strength agent can reduce organic chlorine residues.
Owner:JINING NANTIAN AGRI CHEM CO LTD +1

Analysis method for measuring high cobalt content by EDTA (Ethylene Diamine Tetraacetic Acid) complexation back titration method

The invention relates to the technical field of zinc hydrometallurgy, and discloses an analysis method for measuring high cobalt content by an EDTA complexing back titration method, which is based on the following steps: oxidizing Co < 2 + > into Co < 3 + > by using potassium nitrite in an acetic acid medium to form cobalt potassium nitrite precipitate so as to realize separation of cobalt and interfering ions, dissolving the precipitate, complexing with excessive EDTA, and performing back titration by using a zinc standard solution. Xylenol orange is used as an indicator, and determination is completed at room temperature in a hexamethylenetetramine buffer system with the pH value being approximately equal to 5.8. Coexisting ion interference is effectively eliminated through tartaric acid, sodium fluoride, thiourea and other masking agents, the method has the advantages of being easy and convenient to operate, sensitive in end point, high in accuracy and low in cost, and the requirement for conventional analysis of high-cobalt materials can be met.
Owner:GANSU CHANGBA NONFERROUS METALS CO LTD +1

Magnesium carbonate crystal prepared based on hexamethylenetetramine and preparation method thereof

The invention discloses a magnesium carbonate crystal prepared based on hexamethylenetetramine and a preparation method thereof, and belongs to the technical field of magnesium carbonate materials. The preparation method comprises the following steps: dissolving urea and magnesium chloride, adding hexamethylenetetramine, oscillating in water bath ultrasonic to fully react, then transferring the reaction system into a hydrothermal reaction kettle to perform hydrothermal reaction, and washing and drying a reactant to obtain magnesium carbonate crystals. According to the invention, magnesium chloride and urea are taken as raw materials, hexamethylenetetramine is taken as an additive, the nucleation-growth process is directionally regulated by the hexamethylenetetramine additive, and an optimized reaction process is adopted, so that the magnesium carbonate crystal with high purity, good crystallinity and an excellent pore structure is successfully synthesized; the prepared magnesium carbonate crystal has an optimized porous structure. According to the structure, the mass transfer efficiency is effectively improved, diffusion and transmission of substances in the material are facilitated, and the preparation method is simple and has wide application potential.
Owner:HEBEI MEISHEN TECH CO

Preparation methods and applications of indium sulfide photocatalysts with specific vacancies

This invention proposes a method for preparing and applying an indium sulfide photocatalytic material with specific vacancies. The method involves forming a first solution with ethanol and deionized water; dissolving InCl3·4H2O and thioacetamide, or InCl3·4H2O, thioacetamide, and hexamethylenetetramine, in the first solution by stirring; obtaining a clear solution; reacting the clear solution at a constant temperature; cooling after the reaction; and collecting the product by centrifugation; washing the product; and drying it at a constant temperature; finally, obtaining the photocatalytic material with specific vacancies. This invention introduces vacancies into In2S3, thereby regulating the surface active sites, enhancing its light utilization efficiency and the separation and transfer ability of photogenerated carriers, and improving the photocatalytic activity of N2 to NH3 reduction.
Owner:JIANGXI UNIV OF SCI & TECH

Layered bimetallic oxide surface modified waste pollen biomass as well as preparation method and application thereof

The invention belongs to the technical field of chemical separation, and relates to a layered bimetal oxide surface modified waste pollen biomass and a preparation method thereof.The preparation method comprises the steps that soluble magnesium salt and lanthanum salt are added into deionized water and ultrasonically dispersed to be uniform, then hexamethylenetetramine is added and ultrasonically dispersed to be uniform, PL-coated Al2O3 is added, a mixed solution is transferred into a reaction kettle, a reaction is conducted for 8-36 h at the temperature of 80-160 DEG C, and the layered bimetal oxide surface modified waste pollen biomass is obtained; after the reaction kettle is cooled to the room temperature, centrifugal separation is conducted, deionized water is used for washing till supernate is neutral, then a powdery product is collected and dried, and the waste pollen biomass PL (at) Mg / La-LDH with the surface modified by the layered bimetal oxide is obtained. The prepared adsorbent is applied to adsorption removal of phosphate in a water body. The adsorbent with the hierarchical structure is obtained through in-situ surface modification by taking the waste biomass as a precursor, the defect of poor adsorption effect of pure biomass can be overcome, the specific surface area of the adsorbent can be increased, the adsorption removal effect of phosphate in a water body can be improved, and the adsorbent has a relatively good application prospect.
Owner:ZHENJIANG COLLEGE

Method of cleaning a fouled reverse osmosis membrane

A method of cleaning a fouled reverse osmosis (RO) membrane using a comb-shaped polymer which includes dissolving the comb-shaped polymer and a base in water to form a solution, contacting the fouled RO membrane with the solution to produce a cleaned RO membrane. The comb-shaped polymer includes reacted units of poly(isobutylene-alt-maleic anhydride) and an oligoethylene amine where, the oligoethylene amine is triethylenetetramine, tetraethylene pentaamine, or pentaethylenehexamine.
Owner:KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS

A photoelectrocatalyst and its preparation method

This invention discloses a photoelectrocatalyst and its preparation method, wherein the photoelectrocatalyst comprises Zn 2+ Ce 4+ Au; Zn 2+ Including ammonium acetate, zinc nitrate, and hexamethylenetetramine; Ce 4+ Including cerium nitrate, ammonium chloride, and potassium chloride; Au includes PVP, sodium citrate, potassium bromide, and chloroauric acid; Zn 2+ Ce 4+ The molar ratio of Au to Zn is... 2+ Ce 4+ Au = 1:0.5 ~ 1:2.5 * 10 ‑7 ~7.5*10 ‑7 This method uses electrodeposition to prepare ZnO as a substrate. Its vertically aligned one-dimensional (1D) nanostructures exhibit quantum size-dependent effects, effectively shortening the carrier diffusion distance. CeO2 coats the ZnO, forming a stable, acid- and alkali-resistant substrate material. CeO2 traps electrons from Ce... 4+ Restored to Ce 3+ This forms oxygen voids and Ce 3+ / Ce 4+ Electron pairs produce high catalytic activity.
Owner:GUANGZHOU UNIVERSITY

Triamine-functionalized MCM-41-based filtration membrane

A filtration membrane including a first layer having a triamine-functionalized polysilicate mesoporous material, a second layer including a polysulfone; and a third layer including a polyester terephthalate is described. An orthosilicate group of the triamine-functionalized polysilicate mesoporous material is bonded to a silicon atom of a silicon-containing triamine to form a triamine-functionalized polysilicate backbone, wherein the silicon-containing triamine and one or more tetramines are covalently crosslinked with terephthaloyl chloride to form a polyamide, and wherein the triamine-functionalized polysilicate mesoporous material has a hierarchical structure of MCM-41. The membrane is adapted for use selected from the use group consisting of oil and water separation, water treatment, desalination, and pharmaceutical filtration.
Owner:KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS

Modified molecular sieve for PSA nitrogen preparation and preparation method and application thereof

The invention discloses a modified molecular sieve for PSA nitrogen preparation and a preparation method and application thereof, and belongs to the technical field of gas separation materials. The modified molecular sieve comprises a silicon-aluminum molecular sieve matrix, a transition metal oxide and an organic amine compound; the molar ratio of SiO2 to Al2O3 of the silicon-aluminum molecular sieve matrix is 5-8; the transition metal oxide is a compound of copper oxide and cobalt oxide, the mass ratio of the copper oxide to the cobalt oxide is 2: 1, and the total loading amount of the transition metal oxide is 3%-8% of the mass of the silicon-aluminum molecular sieve matrix; the organic amine compound is ethylenediamine or triethylene tetramine, and the loading capacity of the organic amine compound is 1-5% of the mass of the silicon-aluminum molecular sieve matrix. The modified molecular sieve takes a silicon-aluminum molecular sieve as a matrix, bifunctional modification is performed by loading transition metal oxides (copper oxide and cobalt oxide) and an organic amine compound, and the synergistic effect of the modified molecular sieve and the silicon-aluminum molecular sieve is optimized, so that the limitation of the prior art is broken through, and the sustainable development of the ammonia synthesis industry is promoted.
Owner:XIAN THERMAL POWER RES INST CO LTD +2

Crystalline form of triethylenetetramine tetrahydrochloride and its pharmaceutical use

The present invention describes a new crystalline form of triethylenetetramine tetrachloride which has improved room temperature stability over known forms and over the dichloride salt. The new crystalline form is characterised by having peaks in an XRPD spectrum at 22.9, 25.4, 25.8, 26.6, 34.6 and 35.3±0.1° 2θ and Raman shifts 943, 1173, 1527 and 1612±5 cm−1. The crystalline form of triethylenetetramine tetrachloride is useful in the treatment of Wilson's disease.
Owner:ORPHALAN SA

Method for synthesizing polybenzimidazole polymer material based on furandicarboxylic acid monomer

The invention relates to a preparation method of furan-containing polybenzimidazole (PBI), in particular to a method for preparing furan-containing polybenzimidazole (PBI) by using bio-based furandicarboxylic acid (FDCA) as a diacid monomer instead of a traditional petroleum-based monomer and by using specific aromatic tetramine including 3, 3 ', 5'-tetracarboxylic acid (FDCA) as a diacid monomer. The novel polybenzimidazole polymer is synthesized by the following steps of: reacting 3, 3 '-diaminobenzidine, 3, 3', 4, 4 '-tetraamino diphenyl ether or 3, 3', 4, 4 '-tetraamino diphenyl sulfone at 150-160 DEG C for 2-4 hours under the protection of nitrogen in the presence of an ionic liquid solvent and a dehydrating agent phosphorus pentoxide, and reacting at 165-215 DEG C for 4-30 hours. The invention solves the problems of high processing difficulty, high cost and fossil raw material dependence of the traditional petroleum-based PBI.
Owner:ZHONGKE JINDING (BEIJING) NEW MATERIALS CO LTD +1

Anti-cracking and anti-corrosion concrete and preparation method thereof

The invention discloses anti-cracking and anti-corrosion concrete and a preparation method thereof, and relates to the technical field of concrete preparation, the concrete comprises the following raw materials by weight: 350-400 parts of cement, 80-90 parts of fly ash, 170-190 parts of water, 5-8 parts of a water reducer, 1100-1200 parts of gravel, 700-800 parts of medium sand, 3-5 parts of a modified filler, 8-10 parts of a modified additive, and 3-5 parts of triethylene tetramine. In the raw material mixing process, epoxy groups in the modified additive and epoxy groups on the surface of the modified filler can react with amino groups on triethylene tetramine to form a cross-linked network, and the modified filler contains iron-based layered double hydroxides which can quickly absorb chloride ions, so that the corrosion resistance effect of the concrete is improved, and the service life of the concrete is prolonged. The modified additive forms a polysiloxane network, so that a hydrophobic network is formed in the concrete, and the anti-permeability effect of the concrete is effectively improved.
Owner:SICHUAN JINGYIDA ENG INSPECTION CO LTD

A high-hardness corrosion-resistant coating material suitable for steel doors and windows and a preparation method thereof

The application discloses a high-hardness corrosion-resistant coating material suitable for steel doors and windows and a preparation method thereof, and relates to the technical field of coating materials. In the preparation of the high-hardness corrosion-resistant coating material suitable for steel doors and windows, an inhibition and flame-retardant agent is prepared by reacting tris(aminomethyl) phosphine oxide and 8-hydroxyquinoline-5-formaldehyde; a functional epoxy monomer is prepared by sequentially reacting 2,4,6-trimethyl-1,3,5-triazine with 3-hydroxyfluorene-9-ketone and epichlorohydrin; modified graphene is prepared by reacting pre-modified graphene with 3-mercapto-1-propylamine; and the high-hardness corrosion-resistant coating material suitable for steel doors and windows is prepared by uniformly mixing epoxy resin, the functional epoxy monomer, the modified graphene, the inhibition and flame-retardant agent, triethylenetetramine, a defoaming agent and acetone. The high-hardness corrosion-resistant coating material suitable for steel doors and windows prepared by the application has excellent corrosion resistance, flame retardation and anti-aging performance.
Owner:SHANTOU TIANLING SECURITY & SURVEILLANCE TECH ENG CO LTD

Method for measuring calcium content of seamless pure calcium line

The invention discloses a method for measuring the calcium content of a seamless pure calcium line, and aims to solve the problem of inaccurate detection of a sample containing an oxide layer. According to the method disclosed by the invention, a two-step acidolysis strategy of diluted hydrochloric acid-hexamethylenetetramine and glacial acetic acid warming is adopted, so that comprehensive and rapid dissolution of metal calcium and calcium oxide and super-strong protection of iron sheets are realized; a gradient alkalization masking strategy of triethanolamine-ammonia water-potassium hydroxide is adopted, so that deep masking of interference ions and an acute titration end point are realized. The method has the advantages of good selectivity, strong anti-interference capability, high accuracy and simple operation, and is especially suitable for accurate quality evaluation of seamless pure calcium line products in iron and steel enterprises.
Owner:TANGSHAN RUIFENG IRON & STEEL (GRP) CO LTD

Conductive earth and method of backfilling to prevent pipeline corrosion from underground stray current

The application discloses a conductive soil for preventing underground stray current from corroding pipelines and a filling method. If the underground pipelines of a city are corroded, the harm is immeasurable. The conductive soil comprises the following components in percentage by weight: gypsum powder 55-65%, diatomite or bentonite 20-15%, sodium sulfate 9.5-4.5%, fly ash or carbon residue 15%, and hexamethylene tetramine or thiourea 0.5%. When the pipelines are filled after installation, the pipelines are filled with the conductive soil with a thickness of 100-200 mm, so that the stray current flowing into the ground is transmitted to the ground through the conductive soil preferentially, and does not enter the oil and gas pipelines, thereby achieving the purpose of preventing the corrosion of the stray current on the underground pipelines.
Owner:CHINA RAILWAY FIRST SURVEY & DESIGN INST GRP

Carbon dioxide capture agent, and preparation method and application thereof

The application discloses a carbon dioxide capturing agent and a preparation method and application thereof, relates to the technical field of chemical synthesis, and the formula of the carbon dioxide capturing agent comprises the following components: diethanolamine 2-15 mL, triethylenetetramine 6-20 mL, tetraethylenepentamine 20-80 mL, ethanolamine 2-15 mL, triethanolamine 5-20 mL, methanol 10-50 mL, polyethyleneimine 1-10 mL, piperazine 1-12 g and an initiator 2-10 mL. The carbon dioxide capturing agent can simultaneously meet the three conditions of efficient capturing, low-cost absorption and normal application (temperature 15 DEG C-30 DEG C, pressure 101 kPa), and can very properly compatibly solve the bottleneck problem of the development of the CCUS technology, i.e. economic benefits and cost.
Owner:CHINA PETROLEUM ENG & CONSTR +1

Nanocrystalline magnetic core and method for producing same

The application provides a nanocrystalline magnetic core and a preparation method thereof, and the preparation raw material of the magnetic core comprises the following components in parts by weight: Nd2Fe 14 B magnetic powder 30-35 parts; Fe 75 CuNb2V2Si 15 B9 nanocrystalline magnetic powder 20-30 parts; hydrogenated bisphenol A type epoxy resin 15-30 parts; polypropylene 10-20 parts; hexamethylenetetramine 5-10 parts as a curing agent; triallyl isocyanurate 6-15 parts as a crosslinking agent. 75 CuNb2V2Si 15 After the annealing pretreatment of the B9 nanocrystalline magnetic powder, the ball milling and the reannealing are beneficial to improving the dispersity of the Nd2Fe 14 B magnetic powder, and further improving the anisotropy of the whole magnetic core and the magnetic permeability of the nanocrystalline magnetic core.
Owner:FUYANG NORMAL UNIVERSITY +1

Liquid detergent composition for textile product

To provide a liquid detergent composition for a textile product having excellent detergency to pigment stains.SOLUTION: There is provided a liquid detergent composition for a textile product which comprises a component (A): a nonionic surfactant, a component (B): a non-soap-based anionic surfactant and a component (C): one or more chelating agents selected from ethylenediamine disuccinic acid, hydroxyiminodisuccinic acid, 1,3-propanediaminetetraacetic acid, hydroxyethylethylenediamine triacetic acid, 1,3-diamino-2 hydroxypropane tetraacetic acid, triethylenetetraamine hexaacetic acid and salts thereof, wherein the total of the content of the component (A) and the content of the component (B) is 28 mass% or more based on the total mass of the liquid detergent composition for a textile product and the mass ratio represented by the component (A) / the component (B) is 2 or more.SELECTED DRAWING: None
Owner:LION CORP

Additive for processing water and processing method for processed material

To reduce the degree of discoloration in an additive and reduce the amount of bubbles generated in the additive.SOLUTION: An additive for processing water to be added to processing water used when processing a metal-containing region of a workpiece with a processing tool contains an organic acid, an oxidizing agent, and a chelating agent, and the organic acid and the chelating agent contain different substances. The chelating agent has one or a combination of two or more of ethylenediaminetetraacetic acid, nitrilotriacetic acid, hydroxyethylethylenediaminetriacetic acid, diethylenetriaminepentaacetic acid, triethylenetetraminehexaacetic acid, and gluconic acid.SELECTED DRAWING: Figure 1
Owner:DISCO CORP

Corrosion inhibition inhibitor for hydrochloric acid pickling as well as preparation method and application of corrosion inhibition inhibitor

The invention belongs to the technical field of metal surface treatment, and particularly discloses a corrosion inhibition inhibitor for hydrochloric acid pickling and a preparation method and application thereof, and the corrosion inhibition inhibitor comprises hexamethylenetetramine, ferric chloride, ethyl silicate, glacial acetic acid, dibutyl phthalate, sodium hydroxide, ethylenediamine tetraethanol and desalted water. The inhibitor can form a protective film on the metal surface, effectively inhibits corrosion of acid liquor to a strip steel matrix, reduces iron loss, hydrogen embrittlement and acid mist emission, is suitable for a cold-rolled strip steel hydrochloric acid pickling process, and has the advantages of being small in addition amount, high in inhibition efficiency, environmentally friendly and the like.
Owner:侯立宁