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1367 results about "Ultrasound - action" patented technology

Method and Apparatus for Demulsifying an Oil-Water Emulsion Via Ultrasonic

A method for demulsifying water-oil emulsions through ultrasonic action, comprises a step of making the water-oil emulsions flow through at least one ultrasonic acting region in a flow direction, wherein: within the ultrasonic acting region, a concurrent ultrasonic wave whose traveling direction is the same as the flow direction of the water-oil emulsions is generated by at least a one first ultrasonic transducer provided at the upstream end of the ultrasonic acting region, and at same time, a countercurrent ultrasonic wave whose traveling direction is opposite to the flow direction of the water-oil emulsions is generated by at least a one second ultrasonic transducer provided at the downstream end of the ultrasonic acting region; and the concurrent ultrasonic wave and the countercurrent ultrasonic wave act simultaneously on the water-oil emulsions which flow through the ultrasonic acting region, so as to demulsify the water-oil emulsions. After being demulsified, the water-oil emulsions gravity settle and separate, or settle and separate under an electric field, so as to be dewatered. The present invention can apply to various water-oil separating technologies in the procedures from mining to processing of crude oil.
Owner:CHINA PETROCHEMICAL CORP

Optical fiber extrinsic Fabry-Perot interference ultrasonic sensing and detection device

The invention discloses an optical fiber extrinsic Fabry-Perot interference ultrasonic sensing and detection device, comprising a 1550nm light source, a 1550nm optical circulator, an optical fiber Fabry-Perot ultrasonic sensor, a photoelectric transition module, a signal amplification module, an oscillograph, a piezoelectric transducer and a signal generator. The basic structure of the optical fiber Fabry-Perot ultrasonic sensor is composed of a single mode optical fiber, a quartz vibrating membrane, an outer ceramic bushing, an inner ceramic bushing and a metal base. The light emitted by the 1550nm light source reaches the optical fiber Fabry-Perot ultrasonic sensor through the optical circulator, when ultrasonic wave acts on the ultrasonic sensor, as the light reflected by the optical fiber Fabry-Perot ultrasonic sensor is modulated by the ultrasonic signal, the reflected light reaches the photoelectric conversion module by the circulator and then is converted into an electric signal, and the ultrasonic signal can be observed by the oscillograph after amplification. The invention has simple structure, easy manufacture, low cost and high sensitivity, strong practicability, easy encapsulation and is convenient for mass production, and can be applied to related fields of industrial detection, power system safety and the like.
Owner:SHANGHAI UNIV

Low-silver-loaded electromagnetic wave shielding fabric preparation method

The invention belongs to the technical field of electromagnetic wave shielding material and relates to a low-silver-loaded electromagnetic wave shielding fabric preparation method, comprising the following specific steps: modifying the surface of polyester fabric, introducing an active group--sulphydryl under the premise of not increasing the surface area of the fabric, and then plating silver with ultrasonic wave; wherein, Ag-S chemical bond is formed between sulphydryl and silver so that the compactness of the silver coating and the adhesion force of the fabric substrate are increased; in the process of chemical plating, fresh plating solution is always on the surface of the fabric and the materials which are absorbed on the surface of the fabric through physical adsorption are removed timely owning to the action of ultrasonic wave so that the continuity and compactness of the silver coating can be improved further; the silver loading content of the prepared silver-loaded electromagnetic wave shielding fabric is 6.7-7.0% by weight; the fabric is more resistant to the corrosion of the air and water, the electromagnetic shielding effectiveness is more than 32dB in the range of 0.01-18GHz, namely the anti-electromagnetic radiation rate is more than 99.9%; the fabric can be widely used in electromagnetic wave antiradiation clothes and in the field of electromagnetic wave shielding for special departments such as military, national defense and the like.
Owner:FUDAN UNIV

Method for preparing flexible carbon nano tube transparent conductive thin-film material and electrodeposition device

The invention relates to a method for preparing a flexible carbon nano tube transparent conductive thin-film material and an electrodeposition device, which are suitable for preparing uniform, high-transparency and high-conductivity flexible transparent conductive thin films. The method comprises: dispersing carbon nano tubes in aqueous solution by using an anionic surfactant under the action of ultrasonic waves, centrifuging the solution, using supernate as a plating solution and adding ammonia to make the plating solution alkaline; uniformly depositing the carbon nano tubes dispersed in theplating solution on a polished surface of a stainless steel electrode by using an electro-deposition method to obtain uniform carbon nano tube thin films with a thickness of 20 to 200 nanometers; andtransferring the carbon tube thin films to the surface of a flexible and transparent polymer substrate to form flexible, transparent and conductive thin films. The electrodeposition device mainly comprises an adjustable stabilized direct current power supply and a rectangular electrophoresis tank with a stainless steel inert electrode plate, wherein carbon nano tubes deposits on a polished positive plate to form films. The method and the electrodeposition device are simple and easily controllable in process parameters and can be used in large-area and continuous preparation of flexible, transparent and conductive films.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Preparation method of graphene oxide/amphoteric chitosan intercalation composite for sewage treatment

The invention relates to a preparation method of a graphene oxide/amphoteric chitosan intercalation composite for sewage treatment. At present, the dewatering effect of a cationic type polymeric flocculant is limited. The preparation method has the steps of oxidizing graphite by virtue of concentrated sulfuric acid, sodium nitrate and potassium permanganate to prepare graphene oxide; modifying chitosan by virtue of chloroacetic acid and a quaternization reagent to obtain amphoteric chitosan; and then under the action of ultrasonic waves, realizing intercalation compounding of the graphene oxide and the amphoteric chitosan, and carrying out dispersion to obtain a graphene oxide nanometer ion dispersion liquid. According to the preparation method, by virtue of an intercalation method, controllable dispersion of a graphene oxide sheet layer and grains is realized; as being provided with active groups of carboxyl groups, hydroxy groups, quaternary ammonium groups and the like, the surface of the graphene oxide in a dispersed state can adsorb suspended pollutants in wastewater; and the graphene oxide/amphoteric chitosan intercalation composite can be applied to wastewater treatment and has the advantages of little dosage, high efficiency and low water content of sludge, and the preparation method has the characteristics that the preparation technology is unique, equipment is easily botained, and the operation is simple.
Owner:DONGYING DAOYI BIOLOGICAL MEDICINE TECH CO LTD

Method for decoloring burned waste water by using zero-valent iron/ultrasonic wave synergistic reaction

The invention relates to environmental chemistry, in particular to a method for decolorizing coking wastewater by using synergetic effect of zero-valent iron / ultrasonic waves, which specifically comprises the following steps: wastewater and zero-valent iron chips / powders are added into a reactor; the pH value of the wastewater is adjusted to be 1 to 6; then stirring is carried out under the effect of the ultrasonic waves with the power of 150 to 200W; the reaction is lasted for 30 to 60 minutes; the wastewater is decolorized and COD is removed. During the process, the use amount of zero-valent iron in each liter of wastewater is 2 to 500g, and the reaction temperature is 10 to 80 DEG C. By applying the method for decolorizing coking wastewater by using synergetic effect of zero-valent iron / ultrasonic waves, the chromaticity of the coking wastewater can drop from 1,500 times to 140 times, and the removal efficiency can reach over 90 percent; in addition, after the synergetic effect of the zero-valent iron and ultrasonic waves, the removal efficiency of COD in the coking wastewater is higher than the efficiency under the signal effect of the zero-valent iron and the ultrasonic waves. The obtained BOD5 / COD is increased from 0.08 to 0.36, and the biodegradability of the wastewater is also increased remarkably.
Owner:SHENYANG INST OF APPL ECOLOGY CHINESE ACAD OF SCI

Method for preparing nanoscale zero-valent iron and nanoscale duplex metal Cu/Fe

ActiveCN104308181ANo obvious oxidation phenomenonGood dispersionNanotechnologySimple Organic CompoundsUltrasound - action
The invention discloses a method for preparing nanoscale zero-valent iron and nanoscale Cu/Fe particles. The method comprises the steps of dropwise adding KBH4 or NaBH4 aqueous solution into soluble ferrite aqueous solution under the condition of adopting ultrasonication and continuously stirring with nitrogen introduction, wherein the amount of substance ratio between KBH4 or NaBH4 and soluble ferrite substances is 2-4:1; continuously stirring after dripping, completely reacting to acquire nanoscale zero-valent iron particles; separating, washing and storing; adding CuSO4 or CuCl2 aqueous solution into the nanoscale zero-valent iron particles, wherein the amount of substance ratio between CuSO4 or CuCl2 and the soluble ferrite substances is 1:11-19; stirring and reacting to prepare nanoscale Cu/Fe particles. The high-dispersing type nanoscale zero-valent iron and nanoscale duplex metal Cu/Fe prepared by the method can be used for simultaneously repairing chlorinated organic compounds, nitrate and heavy metal polluted water. The preparation method is simple, and rapid in speed; through the cavatition effect of ultrasonic wave, the dispersion is completely accelerated, and the agglomeration is reduced; the high-dispersing type nanoscale zero-valent iron and nanoscale duplex metal Cu/Fe with smaller grain size, larger specific surface area and higher reactivity can be prepared.
Owner:浙江聚盾科技有限公司

Method for preparing carbon nanometer paper enhanced conductive polymer matrix composite material

The invention provides a method for preparing a carbon nanometer paper enhanced conductive polymer matrix composite material, which is intended to solves a problem that integral mechanical properties and electroconductivity of a current carbon nanotube composite material cannot completely reaches engineering application requirements. Multi-walled carbon nanotubes or single-walled carbon nanotubes and graphene oxide are dispersed in a plasma aqueous solution under action of supersonic waves by an anionic surfactant, after high speed centrifugation, a supernatant liquid of the carbon nanotubes and graphene oxide solution is obtained, and flexible carbon nanometer paper with thickness of 10-100mum can be prepared as an enhanced material by a vacuum filtration method. The carbon nanometer paper enhanced conductive polymer matrix composite materials can be prepared by an RTM forming or vacuum bag method, and conductivity can be raised by raising the content of the carbon nanotubes and dispersion uniformity of carbon nanotube grids in the composite material, wherein the conductivity of the nanocomposite can be raised in several orders of magnitude, and can reach 1-200S / m, thereby making the polymer matrix composite materials go into a semiconductor conductive material field from an insulator.
Owner:SHENYANG AEROSPACE UNIVERSITY

Preparation method of nano-titanium dioxide coated nano-aluminium oxide

The invention discloses a preparation method of nano-titanium dioxide coated nano-aluminium oxide, which comprises the following steps: firstly, dropwise adding an alkaline solution in an aluminium salt solution under the conditions of stirring and ultrasonication, controlling the pH value of a system, and still standing to acquire aluminum hydroxide sol; drying the aluminum hydroxide sol, mixing the aluminum hydroxide sol and water, ball milling, washing the mixture with water until eluate is neutral, filtering by decompression or centrifugalizing, and thermally decomposing to acquire nano-aluminium oxide powder; secondly, adding the nano-aluminium oxide powder into a mixed solution of glacial acetic acid, water and absolute alcohol to acquire the mixture under the conditions of ultrasonication and stirring; adding the mixed solution of butyl titanate and absolute alcohol into the mixture under the conditions of ultrasonication and stirring, still standing, drying and ball milling to acquire the powder; and placing the powder into a furnace at constant temperature, and thermally decomposing to acquire the nano-titanium dioxide coated nano-aluminium oxide powder. The grain diameter of nano-titanium dioxide coated nano-aluminium oxide composite material grains is 1-50 nm, and the purity is higher than 99.8 percent.
Owner:STATE GRID CORP OF CHINA +1

Method and device for preparing lithium hexafluorophosphate through dynamic crystallization

The invention discloses a method and device for preparing lithium hexafluorophosphate through dynamic crystallization. The method includes the following steps of 1, ultrasound induced nucleation, wherein a lithium hexafluorophosphate solution is cooled to minus 10-minus 15 DEG C within 2-3 hours under the action of ultrasonic waves, and a crystallization solution A is obtained; 2, stirring and crystallization, wherein the crystallization solution A is crystallized while being stirred at the cooling rate of 2-3 DEG C/h, and lithium hexafluorophosphate suspension liquid is obtained; filtering and drying are conducted, and the lithium hexafluorophosphate is obtained. According to the method, at the early stage of crystallization, ultrasound induced nucleation is adopted so that the lithium hexafluorophosphate can be subjected to homogeneous nucleation in a supersaturated interface stability zone; gradient cooling crystallization is achieved at a certain cooling rate under the stirring condition along with change of the concentration of the lithium hexafluorophosphate, so that crystal nucleus grows gradually, and a product with even particle size is obtained; the purity of the obtained product reaches 99.99%, the particle size is 40-120 meshes, the whole crystallization process only needs 6-13 hours, wall hanging does not occur easily in the crystallization process, and good economic benefits and social benefits are achieved.
Owner:DO FLUORIDE CHEM CO LTD
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