6185 results about "Spinning" patented technology

The invention discloses a mixed gas-imitating gel fiber as well as a preparation method and application thereof, and belongs to the technical field of fiber materials. The mixed gas-imitating gel fiber is prepared from the following components: cellulose dispersion liquid, a silane coupling agent and viscose in a mass ratio of (1-3): (0.2-0.8): (5-10), comprising the following steps: adding sodium hydroxide into a cellulose dispersion liquid, adjusting the pH value to be alkaline, adding viscose and a silane coupling agent, and carrying out ultrasonic stirring to prepare a mixed spinning solution; the mixed spinning solution is extruded into a coagulating bath through a wet spinning device to be drafted, wet fibers are obtained, and the mixed gas-imitating gel fibers are obtained after freeze drying. The aerogel fiber disclosed by the invention has low heat conductivity coefficient, high mechanical strength and extreme temperature resistance, can solve the problem that the densification and porosity of a traditional fiber structure are difficult to balance, and effectively expands the application prospect of the aerogel fiber in the fields of cold protection, warm keeping and the like.

The invention discloses a preparation method of a cellulose acetate / thermoplastic polyurethane / polypyrrole composite conductive nanofiber aerogel composite pressure sensing material. The preparation method comprises the following steps: (1) preparing a cellulose acetate and thermoplastic polyurethane spinning solution; (2) preparing a cellulose acetate / thermoplastic polyurethane composite nanofiber membrane; (3) preparing cellulose acetate / thermoplastic polyurethane short nano dispersion liquid; (4) preparing a cellulose acetate / thermoplastic polyurethane / polypyrrole polymerization solution; and (5) preparing the cellulose acetate / thermoplastic polyurethane / polypyrrole composite conductive nanofiber aerogel. According to the preparation method, a high-temperature thermal annealing process is not needed, and the prepared nanofiber composite aerogel has high conductivity, ultralow volume density, high compression deformation performance and high pressure resistance sensing sensitivity.

The invention relates to the technical field of fibers, and discloses an antistatic warm-keeping fiber and a preparation method thereof. The preparation method comprises the following steps: carrying out graft modification on a far infrared material graphene oxide through functionalized POSS, introducing the modified graphene oxide and an ionic liquid into polypropylene, carrying out melt grafting to prepare an antistatic polypropylene master batch, introducing the master batch into polypropylene slices for spinning, and carrying out a synergistic antistatic effect of an inorganic antistatic agent graphene and an organic antistatic agent ionic liquid to prepare a composite material. The prepared fiber has antistatic performance and far infrared heating performance, and meanwhile, the POSS structure with excellent thermal stability is introduced, so that the heat resistance of the fiber is further improved.

The invention belongs to the technical field of textile materials, and particularly relates to an antibacterial regenerated wool blended yarn and a production process thereof.The antibacterial regenerated wool blended yarn is prepared from, by weight, 35 parts of regenerated wool fibers, 25-33 parts of LF tencel, 15-27 parts of cellulosic fibers, 8-12 parts of antibacterial chinlon 6 and 5 parts of an antibacterial complexing agent; according to the regenerated wool fiber prepared from the waste wool product through a synergistic improvement process of biological enzyme targeted cleaning and plasma etching, the natural properties of the wool fiber are reserved, and meanwhile, a surface pore structure capable of being combined with an antibacterial complexing agent is also formed; through a Z / S double-twist asynchronous spinning process, dynamic balance of a multilayer structure and hygroscopicity and strength of the blended yarn is achieved, and environment friendliness and commercial feasibility are both achieved.

The invention provides a polyimide multilayer composite membrane material as well as a preparation method and application thereof, and belongs to the technical field of gas separation. According to the method, through collaborative design of a functional support layer, a gradient MOF layer and an ultrathin selection layer structure, the problems of support layer pore seepage, MOF agglomeration, weak interface bonding and the like in an existing composite membrane material are solved. The preparation method comprises the following steps: firstly, carrying out electrostatic spinning on a polyamide acid glue solution, and synchronously introducing dopamine by adopting a chemical imidization method to prepare a functionalized polyimide fiber membrane containing hydroxyl and amino on the surface, so that the mechanical property of a supporting layer and the MOF anchoring capability are remarkably improved; growing MOF layers with different particle sizes on the surface of the fiber membrane by regulating and controlling the concentration gradient of ligand / metal salt and the reaction time, and passivating through a silane coupling agent after each step of growth so as to avoid heterogeneous nucleation and construct a gradient structure; after the MOF gradient layer is subjected to Ar plasma pretreatment to introduce hydroxyl, the ultrathin polyamide selection layer is formed by utilizing interfacial polymerization of fluorine-containing acyl chloride and a macrocyclic amine monomer, and the ultrathin polyamide selection layer is suitable for gas separation work.

The invention relates to a device and a method for preparing nanofiber core-spun yarn through batch coaxial electrostatic spinning. The device comprises a needleless dish-shaped spray head, an air blowing auxiliary device, a liquid supply device, an annular twisting device, a high-pressure generator, a negative-pressure air suction device, a winding device and an unwinding device. The core yarn penetrates through the axis of the needleless dish-shaped nozzle, the nanofiber generated by the needleless dish-shaped nozzle coaxially wraps the surface of the core yarn through the whole spinning device, and batch preparation can be achieved. The device is further provided with an air blowing auxiliary device and a negative pressure air suction device, under the air blowing effect of an air blowing nozzle and the adsorption effect of a negative pressure air suction shell, airflow force can be generated to promote jet flow to be further stretched in a straightened mode, under the common influence of electric field force and the airflow force, the jet flow is fully stretched, bending is reduced, and the service life of the jet flow is prolonged. Therefore, the nanofiber bundles can continuously cover the surface of the core yarn in a high-orientation state under the traction of the annular twisting device, and the continuous nanofiber core-spun yarn is formed.

The invention discloses a three-fluid three-dimensional flow guide spinning head, electrostatic spinning equipment and a batch preparation method of three-chamber embedded parallel structure nanofibers, three different fluids are synchronously guided into a high-voltage electrostatic field by simultaneously arranging a plurality of nozzle outlets with combined structures, and a plurality of complex combined nozzle outlets are used as macroscopic templates, so that the three-chamber embedded parallel structure nanofibers are prepared under the high-voltage electrostatic field. Through interaction of a high-voltage electrostatic field and fluids, batch preparation of the three-chamber embedded and column-structured nanofibers by multi-fluid common electrospinning is realized. The three spinning solutions are guided to a common outlet through the first series of metal capillary tubes, the second series of metal capillary tubes and the spinning solution insulating container respectively; the first series of metal capillary tubes and the second series of metal capillary tubes are respectively dispersed from respective capillary tube gathering inlets, penetrate through the interior of the spinning solution insulating container to the bottom of the spinning solution insulating container and vertically penetrate out to form a plurality of outlets which are parallel in pairs; a through hole outlet is formed in any parallel outlet at the bottom of the spinning solution insulating container to form a common outlet of the three spinning solutions, and the three-chamber embedded and arrayed nano structure is directly prepared in batches in a single step.

The invention relates to the technical field of biomedical materials, and discloses an electret electrostatic therapy membrane and a preparation process thereof.The electret electrostatic therapy membrane is prepared from, by mass, 15%-20% of fluorinated polyether ester, 10%-20% of a composite nano-fiber material, 10%-20% of a composite nano-fiber material, 10%-20% of a composite nano-fiber material and the balance water. 1%-2% of carboxymethyl chitosan; 2-5% of nano cerium oxide particles with the particle size of 50-100 nm; 0.5-1.0% of graphene quantum dots, the particle size of which is 5-10 nm; 1%-2% of sodium hyaluronate; the components are prepared into a film through an electrostatic spinning method, electret performance is given to the film through a charge injection process, finally, the film body is attached to a flexible silica gel adhesion layer, and the flexible silica gel adhesion layer is externally coated with a peelable protective film so that the structural integrity can be kept before the flexible silica gel adhesion layer is used. The composite membrane body disclosed by the invention shows excellent adhesion, charge activation capability and thermal response performance in applications of electrostatic therapy, dielectric assisted stimulation and the like, and has good multi-scene adaptability and clinical application potential.

The invention discloses a conductive yarn and a preparation method thereof, relates to the technical field of functional textile materials and composite conductive fiber preparation, and can solve the problems that an existing conductive yarn is poor in flexibility, insufficient in durability, prone to oxidation failure and difficult to integrate multiple functional performances. The preparation method comprises the following steps that S1, PBO yarn is soaked in a dopamine solution, a PDA modification layer is formed on the surface of the PBO yarn through a polydopamine self-polymerization reaction, and the PDA modification layer provides a chelation site and a bonding interface for metal deposition; s2, the PDA modified PBO yarn obtained in the step S1 is subjected to chemical silver plating, silver is deposited on a PDA modified layer to form a continuous conductive layer, and conductive PBO core yarn is prepared; s3, carrying out melt blending and granulation on the low-dielectric-constant flame-retardant filler and thermoplastic polymer resin to prepare flame-retardant composite particles; and S4, spinning by taking the conductive PBO core yarn prepared in the step S2 as a core layer and a melt formed by melting the flame-retardant composite particles prepared in the step S3 as a skin layer to prepare the conductive yarn.

The invention relates to the technical field of high-performance polyester fibers, and discloses a dry skin-friendly fiber fabric, a preparation method thereof and application of the dry skin-friendly fiber fabric in underwear. The preparation method of the dry and comfortable skin-friendly fiber fabric comprises the following steps: carrying out reaction on terephthalic acid, ethylene glycol and an antibacterial modified diamide diol monomer to obtain modified polyester; the modified polyester and the polyester master batch are mixed and spun, and the modified profiled polyester fiber is obtained; dipping the modified profiled polyester fiber in a finishing liquid containing a biopolymer finishing agent to obtain the high-performance polyester fiber, blending and knitting high-performance polyester fibers, cotton fibers and mulberry silk fibers to obtain a dry skin-friendly fiber fabric; the dry and comfortable skin-friendly fiber fabric has excellent antibacterial performance, moisture absorption performance and skin-friendly performance, the skin can be kept dry and comfortable, safe and comfortable wearing experience is provided for a wearer, and the dry and comfortable skin-friendly fiber fabric can be used for underwear and other underwear materials.

The invention relates to the technical field of textile material and fiber processing, in particular to a high-elasticity moisture-absorption breathable acetate fabric and a preparation method thereof. The invention discloses a high-elasticity moisture-absorption breathable acetate fabric and a preparation method thereof.The acetate fabric takes a bio-based degradable thermoplastic polyester elastomer as an island and acetate as a sea, a homothermal double-hole structure is embedded in the acetate fabric, and the surface of the acetate fabric is covered with a polyglutamic acid and chitosan oligosaccharide self-repairing hydrophilic layer; the preparation method comprises the following steps: pre-burying alkali-resistant microspheres in a marine facies through solid island-solution sea double-path spinning of a bio-based degradable thermoplastic polyester elastomer and acetate, synchronously forming groove-closed pore double channels through simultaneous heating one-step alkali etching-baking, and finally forming a dynamic reversible hydrogen bond network through polyglutamic acid and chitosan oligosaccharide, so as to obtain the marine-based degradable alkali-resistant hydrogel. A bio-based finishing layer with a self-repairing function is obtained, and the finally obtained fabric has the characteristics of high elasticity, breathability, lasting moisture absorption, greenness and degradability.

The invention discloses a novel textile material with eiderdown wrapped by rainbow yarn nanofibers and a preparation method. The novel textile material comprises skeleton fibers located at the axis, an eiderdown component with a heat preservation effect and a rainbow yarn nanofiber reinforcing layer wrapping the outer surface of the eiderdown component. The wrapping reinforcing layer is of a three-dimensional network structure formed by continuous or quasi-continuous nanofibers in a winding, interweaving and lap joint mode, so that stable compounding and structural shaping of down feather components and skeleton fibers are achieved under the condition that the down feather components and the skeleton fibers do not depend on adhesive fixation. The preparation method comprises the following steps: cleaning, drying and opening down for pretreatment; performing melt differential electrostatic spinning on the polymer melt under a high-voltage electrostatic field to form rainbow yarn nanofibers; the down flocs are introduced into the coating area through the framework fibers, so that the rainbow yarn nanofibers are deposited and wound to form a coating reinforcing layer; after being gathered and shaped and twisted into yarns, the yarns can be continuously dragged and wound. The novel textile material has spinnability, structural stability and long-acting thermal insulation performance, and is suitable for spinning, weaving and knitting processing.

The invention belongs to the technical field of spinning, and particularly relates to atmosphere-controllable needleless electrostatic spinning equipment and a method for preparing micro-nano fibers. The equipment comprises a needleless electrode wire, a liquid brushing tank, a direct-current high-voltage power supply, a winding roller, a metal plate, an air inlet, a sliding rail, an air outlet and a closed outer cover. The needle-free electrode wire is connected with the liquid brushing groove in series and connected with the positive electrode of the direct-current high-voltage power source, the metal plate is arranged over the needle-free electrode wire and connected with the negative electrode of the direct-current high-voltage power source or grounded, and the air inlet can reciprocate on the sliding rail. The atmosphere-controllable needleless electrostatic spinning equipment is used for stabilizing jet flow, the fiber forming quality is improved, generated beads are reduced, it is ensured that fibers are uniform and fine, and the mechanical property and stability of the fibers are remarkably improved; one-step preparation of porous fibers and fibers needing secondary reaction modification is achieved, and the consistency of the fibers in the fiber membrane is improved.

The application relates to a continuous macro-preparation device and method of a soft and elastic ceramic superfine fiber material, which sequentially comprises a feeding and liquid preparation system, a multi-jet uniform electrostatic spinning system, a low-temperature calcination system and a winding system. Raw materials are mixed, low-temperature dispersed and vacuum concentrated to obtain a sol; the sol and a polymer flow into a polymer mixing device to be mixed and bubble removed; the mixed sol flows into an inorganic component content control device to be pumped by negative pressure to obtain a spinning solution; the spinning solution flows into a multi-jet electrostatic spinning module to adjust and control the temperature, humidity and multi-directional differential speed during spinning to obtain a fiber membrane material or a fiber flake material; the fiber material is sequentially transmitted to a drying area, a microwave pretreatment area, a polymer removal area, an oxygen-poor atmosphere heat treatment area and a cooling area to be calcined in multiple temperature zones to obtain the soft and elastic ceramic superfine fiber material; and winding and packaging are realized to realize the continuous macro-manufacture of the soft and elastic ceramic superfine fiber material.

The invention discloses an electrostatic ionization device and an array spinning ionization box, and relates to the field of textile processing machinery, the electrostatic ionization device comprises an ionization assembly, the ionization assembly is provided with a backflow groove with a top opening, and a metal wire which is horizontally arranged and can be externally connected with a power supply is arranged above the backflow groove; the reciprocating assembly comprises a liquid supply brush making contact with the upper surface of the metal wire and can drive the liquid supply brush to reciprocate along the axis of the metal wire and coat the surface of the metal wire with a polymer solution used for electrostatic ionization. The liquid supply assembly can store a polymer solution and convey the stored polymer solution to the liquid supply brush, and the backflow groove is communicated with the liquid supply assembly and can collect the polymer solution dripping in the process that the surface of a metal wire is brushed by the liquid supply brush and flow back into the liquid supply assembly. According to the electrostatic ionization device and the array spinning ionization box, the solution utilization rate can be increased, rapid replacement of multiple solution varieties can be achieved, raw material waste is reduced, and the production cost is reduced.

The invention provides an intelligent control method and system for the spinning forming thickness of a tank. According to the method, a spinning tank surface thickness fluctuation signal is collected, and a thickness gradient tensor is generated through time sequence decomposition; extracting a thickness fluctuation intensity value in the tensor and a time sequence lag amount of thickness change of adjacent points to calculate a phase deviation feature; based on the characteristics, the curvature of a laser scanning lens on an annular spinning roller is dynamically adjusted, and a three-dimensional wall thickness cloud picture for identifying the thickness abnormal area is output through focusing and scanning of the tank body; a spinning roller motion track is obtained, thickness change-track space deviation is calculated by associating the thickness abnormal area with the phase deviation characteristics, and a track compensation vector is generated; and according to the vector, a spinning roller feeding path is dynamically optimized, and wall thickness fluctuation caused by material springback is inhibited. Dynamic wave suppression of the wall thickness of the spinning tank is achieved, thickness fluctuation is compressed, and the rejection rate is reduced.

The invention relates to the technical field of sewage treatment, in particular to an electrostatic spinning PVDF nanofiber membrane for sewage treatment and a preparation method and application of the electrostatic spinning PVDF nanofiber membrane. The preparation method comprises the following steps: dissolving PVDF (Polyvinylidene Fluoride) particles in a mixed solvent of DMF (Dimethyl Formamide) and acetone, adding nano TiO2 particles subjected to APTES (Aminopropyltriethoxysilane) surface modification, and adding PVP (Polyvinyl Pyrrolidone) into the solution to obtain a uniform spinning solution; spinning by adopting electrostatic spinning equipment to obtain a PVDF / TiO2 / PVP nanofiber membrane; the nanofiber membrane is soaked in a sodium hydroxide solution, then the membrane is soaked in a Tris-HCl buffer solution containing dopamine, and the final electrostatic spinning PVDF nanofiber membrane is obtained. The average diameter of nanofibers of the nanofiber membrane is 200-300nm, the porosity of the membrane is 70-80%, and the water contact angle is less than 60 degrees; when the nanofiber membrane is used for treating sewage containing organic pollutants and heavy metal ions, the removal rate of the nanofiber membrane on methyl orange can reach 95% or above; the rejection rate of copper ions can reach 90% or above; the removal efficiency of organic pollutants and heavy metal ions is obviously improved.

The invention belongs to the related technical field of flexible electrodes, and discloses a preparation method, a product and application of a high-temperature-resistant flexible metallized ceramic nanofiber composite electrode. The method comprises the following steps: carrying out electrostatic spinning on electrostatic spinning sol doped with an organic polymer to obtain a precursor of a flexible ceramic nanofiber membrane; carrying out primary high-temperature calcination on the precursor to remove the doped organic polymer so as to obtain a flexible ceramic nanofiber membrane; growing and coating a metal conductive layer on the surface of the flexible ceramic nanofiber membrane to obtain an electrode precursor; and carrying out secondary high-temperature calcination on the electrode precursor to obtain the required composite electrode. The invention also discloses a product obtained by the preparation method and application. According to the invention, the problem that the flexible sensor is not resistant to high temperature is solved.

The invention discloses a preparation method of a flexible electromagnetic shielding type force sensor based on a coaxial structure, and belongs to the field of flexible electronics and intelligent sensors. According to the method, a coaxial wet spinning process is adopted, a core-sheath structure conductive fiber is constructed, a core layer is made of a multi-walled carbon nanotube (CNT) and thermoplastic polyurethane (TPU) composite material, and a sheath layer is made of a nickel-coated carbon nanotube (Ni-CNT) and TPU composite material. By regulating and controlling the proportion of the core sheath, the construction of the gradient conductive network is realized, and the sensing sensitivity, the electromagnetic shielding performance and the mechanical flexibility are improved. The obtained Ni-CNT-coated CNT fiber is made into fabric and integrated in a sensing glove, and multi-finger bending detection and wireless man-machine interaction control are achieved. The sensor has the advantages of high sensitivity, wide strain detection range and excellent electromagnetic shielding effectiveness, is suitable for the fields of intelligent wearing, anti-interference man-machine interface and fire-fighting equipment, and can also be expanded to complex application scenes such as aerospace teleoperation.

The invention provides a preparation method of high-performance polyacrylonitrile pre-oxidized fibers, and belongs to the technical field of preparation of carbon filaments from polyacrylonitrile. The preparation method comprises the following steps: adding hydroxylated carbon nanotubes into deionized water, performing ultrasonic dispersion, adding a modifier and a catalyst, continuing ultrasonic dispersion, heating to 80-90 DEG C, performing constant-temperature reaction, fully washing with water, and drying to obtain modified carbon nanotubes; dispersing the modified carbon nanotube in an N, N '-dimethylformamide solution, adding an acrylonitrile monomer, hydroxyethyl acrylate and an initiator, copolymerizing to form a carbon nanotube / acrylonitrile copolymer, and spinning to obtain a carbon nanotube / acrylonitrile copolymer fiber; the carbon nano tube / acrylonitrile copolymer fiber is placed in a microwave treatment device, and a plurality of microwave generators are arranged in the microwave treatment device and are used for carrying out segmented pre-oxidation on the carbon nano tube / acrylonitrile copolymer fiber. The problems that an existing polyacrylonitrile fiber pre-oxidation technology is high in energy consumption and low in strength, poor in flame retardance and the like due to the difference between internal and external pre-oxidation effects can be solved.

The invention discloses a near-isothermal hot spinning forming method and a heat compensation method for a metal workpiece. The forming method comprises the steps that a blank heated to the spinning preheating temperature is transferred and clamped on a workbench, and the blank is located in an effective heat compensation area arranged in a heat compensation system; the blank is subjected to temperature measurement to judge whether the blank temperature meets the temperature before blank spinning so as to determine whether the blank is subjected to temperature compensation waiting in a heat compensation system or not; and then near-isothermal hot spinning forming is completed in a heat compensation system according to a preset spinning program, the heat compensation system continuously compensates the temperature of the blank during spinning and monitors the spinning temperature in real time, and it is guaranteed that the fluctuation range of the spinning temperature does not exceed + / -20 DEG C in the process from spinning deformation to spinning deformation ending. According to the near-isothermal spinning forming technology, spinning equipment of a measurable and controllable semi-closed active heat compensation system is utilized, and the deformation temperature of high-temperature alloy, titanium alloy and other difficult-to-deform metal materials is controlled within a small fluctuation range in the spinning process.

The invention discloses a phase spinning fancy yarn and a production device thereof, and belongs to the technical field of spinning. The phase spinning fancy yarn is formed by a base yarn section and a wave-shaped yarn section in a staggered mode, the wave-shaped yarn section is of a conical transition structure with the thick middle and the two gradually-thin ends, and the key improvement is that the base yarn section and the wave-shaped yarn section are equal in linear density. The production device comprises a phase spinning mechanism arranged between a front drafting device and a yarn guide mechanism, the phase spinning mechanism comprises a driving wheel, a driven wheel and a circular ring belt, and yarn strands wind two edge strips of the circular ring belt in an S shape; the second driving device drives the driving wheel to rotate; the control unit controls all the components in a coordinated mode. The yarn diameter change is formed under constant-speed feeding through the periodic change of friction force, the problems that traditional bunchy yarn is uneven in twist, low in strength, much in hairiness and difficult in yarn density control are effectively solved, and the yarn quality and the weaving performance are remarkably improved.

The present invention relates to the field of the preparation of polyurethane elastic fibers, and relates to a preparation method for a bio-based polyurethane elastic fiber, comprising: preparing polyether polyol from sucrose, glycerol, dimethylamine and propylene oxide; adding a solvent, i.e., N,N-dimethylacetamide, and polyether polyol and polyisocyanate into a reaction tank, and adding p-Toluenesulfonyl semicarbazide and aluminum methylenebis(2,4-di-tert-butylphenoxy) phosphate to prepare a spinning solution; and subjecting the spinning solution to spinning and oil application by means of dry spinning technology to obtain the bio-based polyurethane elastic fiber. The present invention ensures that the properties of polyurethane elastic fibers do not deteriorate or are partially enhanced, while the cost and performance advantages are achieved.

The invention discloses an MXene / rGO (at) SA coaxial composite fiber based on a core-shell structure and a preparation method and application thereof, and belongs to the technical field of nano composite materials and flexible electronics. The invention solves the problems of many interface defects, unstable performance and the like of the existing coaxial fiber. The MXene / rGO-SA coaxial composite fiber is prepared by adopting a coaxial wet spinning method, a high-performance SA fiber with excellent mechanical properties is used as a tough shell layer, a multi-element nano material MXene / rGO composite fiber is used as a core layer, a calcium chloride-ethanol mixed solution in a certain proportion is used as a coagulating bath, and the coaxial composite fiber is prepared by utilizing a coaxial needle head; the interface bonding force and the conductive network of the MXene / rGO (at) SA coaxial composite fiber are optimized by accurately controlling the core-shell ratio, and the mechanical strength, the conductivity and the stability are synergistically improved.

The application discloses a kind of bundled biaxial skin-core structure tensile yarn spinning processes, specifically including the following steps, step S1: one low modulus high elongation fiber filament one and one low modulus high elongation fiber filament two are unwound by active feeding roller, and are respectively fed into lower layer hollow spindle center tube one and lower layer hollow spindle center tube two, as two core filaments;Step S2: high modulus low elongation fiber filament one is wrapped on the surface of the core filament in positive helical line configuration at lower layer guide hook one;High modulus low elongation fiber filament two is wrapped on the surface of the core filament in reverse helical line configuration at lower layer guide hook two;Form biaxial skin-core structure covering yarn system, and pass through upper layer hollow spindle center tube;Step S3: at upper layer guide hook, the fiber filament yarn with excellent elastic elongation wound on upper layer hollow spindle is bound to the surface of the biaxial skin-core structure covering yarn system with low spiral covering density, to form bundled biaxial skin-core structure tensile yarn.

The invention provides an impurity deep removal and purification device in ES fiber solvent recovery. Relates to the technical field of electrostatic spinning process and solvent recovery, and comprises a pre-separation module used for removing fiber residues and solid particles larger than 5 microns in solvent-enriched gas; the multi-stage deep condensation module comprises two stages of condensers, and the two stages of condensers condense the solvent steam according to the gradually decreased temperature and intercept micro-droplet impurities; and the composite adsorption module is used for adsorbing residual organic trace impurities and removing water. The impurity deep removal and purification device in ES fiber solvent recovery has the advantages of being low in energy consumption, easy and convenient to maintain, stable in operation and capable of being continuously online for 72 h or above without shutdown, the solvent recovery rate is remarkably increased, the operation cost is reduced, and the potential risk of organic vapor emission to the environment and operation safety is effectively avoided.

The invention discloses a flexible light heat-insulation streamline oxide nanofiber aerogel and a preparation method and application thereof.The fiber aerogel is prepared through preparation of a spinning precursor solution, an air flow spinning technology and a heat treatment process, the spinning solution is stretched into fibers through the air flow spinning technology, and under the influence of a flow field, the flexible light heat-insulation streamline oxide nanofiber aerogel is obtained. The fibers present streamlines with different curvatures, high-quality dry fibers are obtained through a heating field, and the high-quality dry fibers are stacked in a receiver to form a three-dimensional structure; and finally, the three-dimensional streamline oxide nanofiber aerogel with ultralow thermal conductivity and low density is obtained by combining thermal treatment with a folding process, has excellent thermal protection performance and can be widely applied as a light high-temperature-resistant thermal insulation material.

The invention discloses a lasting aromatic lyocell fiber of a biological enzyme immobilized temperature-sensitive microcapsule and a preparation method of the lasting aromatic lyocell fiber, and relates to the technical field of polyester fabrics. The method comprises the steps that firstly, a temperature-sensitive microcapsule of a three-layer structure is prepared, an inner core contains aromatic substances of lavender essential oil, ambrota ether and rosin glycerin ester, a middle layer enables N-isopropylacrylamide monomers to be polymerized to form PNIPAM temperature-sensitive hydrogel, and a shell is a nanocellulose crystal-polydopamine compound; then spinning by taking the NMMO aqueous solution containing the microcapsules as an inner layer solution and taking the NMMO aqueous solution containing the eucalyptus pulp as an outer layer solution by adopting a coaxial micro-fluidic spinning technology; and finally carrying out crosslinking treatment through a biological enzyme coagulating bath, wherein the coagulating bath contains an NMMO aqueous solution, horse radish peroxidase and a hydrogen peroxide solution with gradient concentration. The aromatic lyocell fiber prepared by the invention has excellent temperature-sensitive aroma release performance and washing fastness, and solves the technical problems that microcapsules in traditional aromatic textiles are easy to break and fall off and aromatic substances are easy to volatilize.

The invention discloses a lightweight alumina foamed ceramic refractory material and a preparation method thereof, and relates to the technical field of ceramic materials. When the light aluminum oxide foamed ceramic refractory material is prepared, zirconium acetylacetonate, yttrium nitrate hexahydrate and aluminum nitrate nonahydrate are mixed to prepare a spinning solution for electrostatic spinning, nano aluminum titanate is loaded by using a nano spraying technology during spinning, and doped modified zirconium oxide fibers are prepared after high-temperature heat treatment and defibering and dispersing; mixing aluminum oxide micro powder, hollow aluminum oxide, a high-temperature foaming agent, doped modified zirconium oxide fibers and a sintering aid, and then performing ball milling and sieving to prepare aluminum oxide-based mixed powder; and carrying out mold pressing on the alumina-based mixed powder to prepare a green body, sintering, and cooling to prepare the lightweight alumina foamed ceramic refractory material. The light aluminum oxide foamed ceramic refractory material prepared by the invention has the advantages of light weight, low thermal conductivity, high compressive strength, high bending strength and good thermal shock resistance.

The invention relates to the technical field of functional fiber materials, in particular to a fiber material with an antibacterial function and a preparation method thereof, and the preparation method comprises the following steps: S1, preparing composite antibacterial powder; s2, preparing antibacterial functional particles; s3, preparing a spinning solution; s4, performing wet spinning and post-treatment to obtain the fiber material with the antibacterial function. A triple antibacterial system is formed by constructing the ferroferric oxide core body, the zinc oxide middle layer and the chitosan shell and is fused into the fiber preparation process, and the fiber material which is excellent in antibacterial effect, resistant to washing and good in environmental adaptability and has the antibacterial function is obtained.