The invention discloses a
fluidized bed reactor for preparing
porous carbon through collaborative graded activation of
water vapor and CO2 and a method for preparing the
porous carbon through collaborative graded activation of the
water vapor and the CO2, and belongs to the technical field of material
chemical engineering. The
fluidized bed reactor is composed of a shell, a
fluidization section, a
sedimentation section, a porous distribution plate, a gas distribution chamber, a stirring device and a
temperature control system, and uniform
fluidization and multi-section
temperature control of superfine
powder are achieved. According to the
activation method, steam and CO2 collaborative graded
etching pore-forming is adopted, specifically, in the first stage, quick pore-forming is conducted mainly through steam at the temperature of 500-800 DEG C, in the second stage, pore-expanding is conducted cooperatively through steam and CO at the temperature of 700-900 DEG C, and in the third stage, fine control is conducted mainly through CO2 at the temperature of 850-1050 DEG C; the continuous preparation of the high-performance
porous carbon with the specific surface area of 1500-2500m < 2 > / g, the pore volume of more than or equal to 0.8 cm < 3 > / g and the 2-10nm mesopores accounting for 20-60% is realized by adjusting the gas velocity, the
activation temperature, the activation time and the ratio of
water vapor to CO2, the bottlenecks of low specific surface area, single
pore diameter, large batch difference and the like of physical activation are solved, and the method is suitable for green and low-cost production of high-end
energy storage carbon materials such as supercapacitors,
lithium /
sodium ion batteries and the like.