The invention discloses a rapidly synthesized
ferric sodium pyrophosphate electrode material, a preparation method thereof and a positive
electrode. Relates to the technical field of batteries. The preparation method comprises the following steps: S1, mixing a
sodium source, an
iron source, a
phosphorus source and a
carbon source, adding a preset volume of deionized water, and stirring until the raw materials are completely dissolved to obtain a light yellow transparent solution; s2, adding a preset amount of
modified carbon nanotubes into the light yellow transparent solution, and dispersing in an ultrasonic environment to obtain a stable suspension; s3, starting a
spray dryer, and collecting yellow green spherical precursor
powder from a
discharge port; s4, placing the yellow green spherical precursor
powder obtained by
spray drying in a magnetic boat, and carrying out heat preservation at 300 DEG C in a pure
argon environment at a heating rate of 2 DEG C / min for 5 h to obtain black
powder; and S5, transferring the black powder into
Joule thermal equipment, and reacting for a preset time under a preset condition to obtain a final black powdery product. Through innovative
process design and material modification, the core problems of long period, poor
conductivity, low tap density and the like in the traditional preparation technology are solved.