194 results about "Sulfur" patented technology

The invention discloses a method for preparing a single-layer tungsten diselenide nanoband based on a space confinement strategy. By changing the flow and the growth time of hydrogen, effective control on the width and the thickness of a nanoband can be realized. The method comprises the following steps: uniformly spraying tungsten trioxide powder to one substrate, then covering the substrate by the other substrate, and forming micro reaction space which is of a 'sandwich'-like structure. Growth of a tungsten diselenide nanoband is carried out by utilizing a constant-pressure chemical vapor deposition method; physicochemical characteristics of a one-dimensional transition metal chalcogenide strongly depend on suspension key types on the edge of the one-dimensional transition metal chalcogenide, metallic properties are displayed by an ultranarrow band, and conversion from the metallic properties to semiconductor properties can be displayed from the edge to the center of a wider band; the tungsten diselenide nanoband is widely applied to micro-nano photoelectric devices due to the special property; industrial production of the tungsten diselenide nanoband can be realized through an experimental method of the invention.

An embodiment of the present invention provides a steel material, for a pressure vessel, comprising, in weight %, 0.06-0.25% of carbon (C), 0.05-0.50% of silicon (Si), 1.0-2.0% of manganese (Mn), 0.005-0.40% of aluminum (Al), 0.010% or less of phosphorus (P), 0.0010% or less of sulfur (S), 0.001-0.03% of niobium (Nb), 0.001-0.03% of vanadium (V), 0.001-0.03% of titanium (Ti), 0.01-0.20% of chromium (Cr), 0.05-0.15% of molybdenum (Mo), 0.01-0.50% of copper (Cu), 0.05-0.50% of nickel (Ni), 0.0005-0.0050% of magnesium (Mg), 0.0005-0.0050% of calcium (Ca), 0.0020% or less of oxygen (O), and the remainder being Fe and other unavoidable impurities. A microstructure comprises in terms of area fraction 30% or less of pearlite and the remainder being ferrite. A non-metallic inclusion contains Mg—Al—Ca—O composite oxide.

The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 %, 0.15% ≤ Manganese ≤ 0.25%, 3.2% ≤ Silicon ≤ 3.8%, 0.7% ≤ Aluminum ≤ 1.3 %, 0 % ≤ Phosphorus ≤ 0.15 %, 0 % ≤ Sulfur ≤ 0.006 %, 0 % ≤ Nitrogen ≤ 0.09% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1%, 0% ≤ Titanium ≤ 0.1%, 0% ≤ Vanadium ≤ 0.1%, 0% ≤ Chromium ≤ 1%, 0% ≤ Molybdenum ≤ 0.5%, 0% ≤ Tungsten≤ 0.1%, 0% ≤ Cobalt ≤ 1%, 0% ≤ Arsenic ≤ 0.05%, 0.001% ≤ Calcium ≤ 0.01%, 0% ≤ Copper ≤ 1%,0.001% ≤ Nickel ≤ 0.01, 0 % ≤ Boron ≤ 0.05%, 0 % ≤ Lead ≤ 0.2%, 0% ≤ Tin≤ 0.2%, 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current loss in total iron loss less than 33 % when calculated in accordance with Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.630T to 1.65T.

The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 %, 0.15% ≤ Manganese ≤ 0.25%, 2.9% ≤ Silicon ≤ 3.4%, 0.8% ≤ Aluminum ≤ 1.1 %, 0 % ≤ Phosphorus ≤ 0.15 %, 0 % ≤ Sulfur ≤ 0.006 %, 0 % ≤ Nitrogen ≤ 0.09%,with 3.85% ≤ Si+Al+Mn ≤ 5.5% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1%, 0% ≤ Titanium ≤ 0.1%, 0% ≤ Vanadium ≤ 0.1%, 0% ≤ Chromium ≤ 1%, 0% ≤ Molybdenum ≤ 0.5%, 0% ≤ Tungsten≤ 0.1%, 0% ≤ Cobalt ≤ 1%, 0% ≤ Arsenic ≤ 0.05%, 0.001% ≤ Calcium ≤ 0.01%, 0% ≤ Copper ≤ 1%, 0% ≤ Nickel ≤ 1%, 0 % ≤ Boron ≤ 0.05%, 0 % ≤ Lead ≤ 0.2%, 0% ≤ Tin≤ 0.2%, 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current loss in total iron loss less than 25% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.625T to 1.690T.

A high-performance steel bar, according to one embodiment of the present invention comprises 0.08-0.26 wt% of carbon (C), 0.50 wt% or less (excluding 0) of silicon (Si), 0.6-3.0 wt% of manganese (Mn), 0.025 wt% or less (excluding 0) of phosphorus (P), 0.025 wt% or less (excluding 0) of sulfur (S), 0.002-0.50 wt% of chromium (Cr), 0.50 wt% or less (excluding 0) of copper (Cu), 0.01-3.40 wt% of nickel (Ni), 0.002-0.10 wt% of molybdenum (Mo), 0.005-0.040 wt% of aluminum (Al), 0.10 wt% or less (excluding 0) of vanadium (V), 0.1 wt% or less (excluding 0) of niobium (Nb), 0.001-0.050 wt% of titanium (Ti), 0.015 wt% or less (excluding 0) of nitrogen (N), and the balance of iron (Fe) and inevitable impurities, wherein the room-temperature yield strength (YS) satisfies at least 500 MPa.

A nickel-based alloy composition consisting, in weight percent, of: 1.5 to 4.5% aluminium, 1.1 to 3.4% titanium, 0.0 to 4.0% niobium, 0.0 to 5.2% tantalum, 0.9 to 6.6% tungsten, 0.0 to 3.0% molybdenum, 0.0 to 24.0% cobalt, 12.5 to 20.6% chromium, 0.02 to 0.15% carbon, 0.001 to 0.015% boron, 0.0 to 0.1% zirconium, 0.0 to 3.0% rhenium, 0.0 to 2.0% ruthenium, 0.0 to 3.0% iridium, 0.0 to 0.5% vanadium, 0.0 to 1.0% palladium, 0.0 to 1.0% platinum, 0.0 to 0.5% silicon, 0.0 to 0.1% yttrium, 0.0 to 0.1% lanthanum, 0.0 to 0.1% cerium, 0.0 to 0.003% sulphur, 0.0 to 0.25% manganese, 0.0 to 0.1 magnesium, 0.0 to 5.0% iron, 0.0 to 0.5% copper, 0.0 to 1.0% hafnium, the balance being nickel and incidental impurities, wherein the following equations are satisfied in which WAl, WTi, WNb, WTa and WW are the weight percent of aluminium, titanium, niobium, tantalum and tungsten in the alloy respectively 0.65≤0.3 WNb+0.15 W 3.6≤WAl+0.5 WTi+0.3 WNb+0.15 WTa≤5.7 WTa+0.92WW≤6.1.

The invention relates to the technical field of resin aging analysis, in particular to a nuclear power plant cation resin aging decomposition evaluation method. The evaluation method comprises the following steps: taking a water sample of cation resin of a nuclear power plant, and then measuring the boron concentration of the water sample; diluting the sulfur standard mother liquor by taking solutions with the same boron concentration as a matrix to obtain sulfur standard solutions with different sulfur concentrations; measuring the luminous intensity of the sulfur standard solutions with different sulfur concentrations, and establishing a standard working curve of the corresponding relationship between the sulfur concentrations and the luminous intensity; measuring the luminous intensity of the water sample, substituting the luminous intensity into the standard working curve to obtain the sulfur concentration of the water sample, and converting the sulfur concentration into the sulfonic group content of the water sample; measuring the sulfo group content of the water sample at different time points, and then evaluating the aging decomposition condition of the cation resin of the nuclear power plant. The method can quickly and accurately judge the aging decomposition condition of the cation resin, and provides a basis for a replacement strategy of the cation resin of a nuclear power plant.

The invention provides a method for predicting the flammability upper limit volume percentage of a pure compound. The method can be used for predicting a mathematical model of the flammability upper limit volume percentage of the pure compound which is composed of 12 or less elements of hydrogen, carbon, nitrogen, oxygen, sulfur, fluorine, chlorine, bromine, iodine, silicon, phosphorus, arsenic and the like and has the atom number of 25 or less (excluding hydrogen) with high accuracy. Wherein the model is obtained as a universal quantitative structure-property relationship model by determining an optimal model from a plurality of multiple linear regression models by means of a step-by-step selection method, and the model takes some of the various molecular descriptors as independent variables, takes flammability upper limit volume percent as a dependent variable, and takes the flammability upper limit volume percent as a dependent variable. The value of the molecular descriptor included in the model can be received and input in a short time, and the flammability upper limit volume percentage can be output, so that only the specific value of the molecular descriptor included in the model is known. And the flammability upper limit volume percentage of the compound purely formed by the molecule can be predicted for any molecule meeting the requirements of the invention.

The invention relates to an indium phosphide crystal containing sulfur and tin, a single crystal wafer, a preparation method of the indium phosphide crystal and the single crystal wafer and a device. Specifically, the invention relates to an indium phosphide crystal which is an N-type indium phosphide crystal, and the indium phosphide crystal contains 0.5 ppm to 500 ppm of sulfur and also contains 0.5 ppm to 1000 ppm of tin. The invention also relates to a method for preparing the indium phosphide crystal doped with sulfur and tin and a device prepared by using the indium phosphide crystal. The indium phosphide crystal doped with sulfur and tin obtained according to the invention has the advantages of low dislocation density, few defects and high yield.

A grease composition that includes at least an oil-based medium, a thickener, and a fullerene-like nano-structure. The fullerene-like nano-structure includes a plurality of layers each comprised of a metal chalcogenide composition has a molecular formula of MX2, where M is a metallic element selected from the group consisting of titanium (Ti), vanadium (V), chromium (Cr), manganese (Mn), iron (Fe), cobalt (Co), nickel (Ni), copper (Cu), zinc (Zn), zirconium (Zr), niobium (Nb), molybdenum (Mo), technetium (Tc), ruthenium (Ru), rhodium (Rh), palladium (Pd), silver (Ag), cadmium (Cd), hafnium (Hf), tantalum (Ta), tungsten (W), rhenium (Re), osmium (Os), iridium (Ir), platinum (Pt), gold (Au), mercury (Hg) and combinations thereof, and X is a chalcogen element selected from the group consisting of sulfur (S), selenium (Se), tellurium (Te), oxygen (O) and combinations thereof.

This invention relates to a method for the recovery of metal from a material comprising: contacting a material with a first reagent comprising a thiocarbonyl group and a second reagent under various conditions. The metal may be a base metal, a precious metal, or a combination thereof. The conditions include, but are not limited to, recovery in the presence of a microbe; optimal material size and / or shape; geolocation parameters; elemental sulfur; added pyrite; or a combination thereof.

Provided is a cold-rolled steel sheet consisting of carbon (C): 0.23 wt% to 0.35 wt%, silicon (Si): 0.05 wt% to 0.5 wt%, manganese (Mn): 0.3 wt% to 2.3 wt%, phosphorus (P): more than 0 wt% and not more than 0.02 wt%, sulfur (S): more than 0 wt% and not more than 0.005 wt%, aluminum (Al): 0.01 wt% to 0.05 wt%, chromium (Cr): more than 0 wt% and not more than 0.8 wt%, molybdenum (Mo): more than 0 wt% and not more than 0.4 wt%, titanium (Ti): 0.01 wt% to 0.1 wt%, boron (B): 0.001 wt% to 0.005 wt%, a balance of iron (Fe), and unavoidable impurities, wherein a final microstructure of the cold-rolled steel sheet includes cementite, a transition carbide, and a fine precipitate, the transition carbide including ε-carbide having an atomic ratio of a substitutional element selected from Fe, Mn, Cr, and Mo, to C of 2.5:1, or η-carbide having an atomic ratio of the substitutional element to C of 2:1, and the fine precipitate having an atomic ratio of an alloying element selected from Mo and Ti, to C of 1:1.

The invention discloses a method for simultaneously determining total barium and sulfur in barite by inductively coupled plasma emission spectrometry. In this method, the sample is decomposed by melting with sodium carbonate and sodium hydroxide. The molten slag is extracted with hot water, nitric acid and a chromium internal standard solution are added, the crucible and the beaker are washed with dilute hydrochloric acid, water is added and shaken well, heated to boiling gently on a hot plate and then taken off and shaken well. After cooling, it is determined on an inductively coupled plasma emission spectrometer. The method of the invention makes use of the characteristic that barium sulfate has a relatively large solubility in reverse aqua regia, enabling barium and sulfur to coexist stably, and then simultaneously determines total barium and sulfur by inductively coupled plasma emission spectrometry, which has the characteristics of high detection efficiency, high precision, simple operation and low cost, and solves the technical problems that when determining total barium and sulfur in barite by traditional methods, sulfur and barium are difficult to coexist in the solution, usually two different methods are required to complete the determination, and even barium and sulfur need to be separated in advance, resulting in a long process and low detection efficiency.

The present invention is a method for producing glass, which comprises a step for holding or flowing molten glass while in contact with a metal wall comprising platinum or a platinum alloy, the method being characterized in that the molten glass has an SO3 saturation solubility of 0.05 (wt%) or less, and in that the method also has an adjustment step for adjusting at least one of the sulfur concentration CS, the water vapor partial pressure pH2O and the oxygen partial pressure pO2, where the sulfur concentration in the molten glass is denoted by CS (wt%), the water vapor partial pressure in an outer space of the metal wall is denoted by pH2O (atm), and the oxygen partial pressure in the outer space of the metal wall is denoted by pO2 (atm), so that the SP value calculated from formula (1) is such that SP≤3.10.　Formula (1): SP = CS × pH2O / pO2.

1. The name of the design product: flame photometric detector. 2. The use of the design product: for detecting phosphorus-containing compounds and sulfur-containing compounds. 3. The design points of the design product: in shape. 4. The picture or photo that best indicates the design points: perspective view.

Provided is a mathematical model that can predict, with high accuracy, the saturated liquid density of a pure compound at 298.15 K, said pure compound comprising 12 or less elements such as hydrogen, carbon, nitrogen, oxygen, sulfur, fluorine, chlorine, bromine, iodine, silicon, phosphorus, and arsenic and having 25 or less atoms (excluding hydrogen). The model is a quantitative structure-property relation model and is obtained by solving an optimal model from a plurality of multiple linear regression models by a step-by-step selection method, and the model takes some molecule descriptors in various molecule descriptors as independent variables, takes saturated liquid density under 298.15 K as a dependent variable, and takes the saturated liquid density under 298.15 K as a dependent variable. The value of the molecule descriptor included in the input model can be received in a short time, and the saturated liquid density at 298.15 K can be output, so that the saturated liquid density at 298.15 K of a compound formed by the molecule singly can be predicted for any molecule meeting the requirements of the invention as long as the specific value of the molecule descriptor included in the model is known.

The invention relates to a pre-hardened die steel alloy and a preparation method thereof, the alloy comprises the following chemical components in percentage by mass: 0.40-0.50% of carbon, 0.20-0.40% of silicon, 1.20-1.60% of manganese, less than or equal to 0.010% of sulfur, less than or equal to 0.025% of phosphorus, 1.50-1.80% of chromium, 0.35-0.50% of molybdenum, 0.15-0.25% of vanadium, 1.65-1.85% of nickel, less than or equal to 0.20% of copper and the balance of iron, and the content of residual gases is less than or equal to 70ppm of nitrogen, less than or equal to 1.0 ppm of hydrogen and less than or equal to 20ppm of oxygen. The pre-hardened die steel alloy is directly pre-hardened to 44-46 HRC, meanwhile has good machining performance, can be directly cut and machined into a die finished product, does not need secondary quenching, saves the cost of vacuum heat treatment and the heat treatment time, can replace die steel 1.2343, and has great performance advantages and competitive advantages.

The invention relates to an inhibitor for efficiently separating copper and sulfur under a low-alkalinity condition, a flotation reagent and a flotation method. The inhibitor is a compound as shown in a formula I (formula I), wherein R1, R2, R3 and R4 are respectively and independently selected from one of-R5X,-X,-H and-N + R6, R5 is alkyl of C1-C10, naphthenic base of C3-C10 or heterocyclic group of C3-C10, and the ring of the heterocyclic group is provided with or not provided with a substituent group; x is one of F, Cl, Br, I, tertiary amine positive ions, nitro, cyano, sulfo, formyl, acyl and carboxyl; r6 is a C1-C5 alkyl group or a C3-C5 cycloalkyl group; the inhibitor is low in viscosity and good in fluidity, pyrite and chalcopyrite in complex copper sulfide ore copper-sulfur ore can be effectively separated under the low-alkalinity condition, and the separation effect is remarkable.

The invention discloses a preparation method of FePS3, which comprises the following steps: mechanically mixing pyrite powder, sulfur-containing small molecules and elemental phosphorus, calcining the fully mixed powder in two temperature stages under a protective atmosphere, and cooling to obtain FePS3 nano-powder; wherein in the first temperature stage, the temperature is 200-300 DEG C, and the heat preservation time is 120-240 minutes, and in the second temperature stage, the temperature is 400-600 DEG C, and the heat preservation time is 120-180 minutes; the sulfur-containing small molecules are thiourea, thioacetamide or a mixture of the thiourea and the thioacetamide; the molar ratio of sulfur atoms to phosphorus atoms in FeS2 molecules and sulfur-containing small molecules in the pyrite powder is (1: 3: 5)-(1: 1: 5). According to the method, pyrite is used as an iron source and a sulfur source, sulfur-containing small molecules are used as a second sulfur source, and the FePS3 nano-powder is directly obtained through solid-phase reaction with the simple substance phosphorus without additional purification treatment. The method is low in solid-phase reaction temperature and simple in process, does not need harsh reaction conditions, and is easy for large-scale production.

The present invention relates to a sulfide solid electrolyte which has a crystal phase containing a crystal that is represented by composition formula RaMbScXd (wherein 3 ≤ a ≤ 7, b = 1, 3 ≤ c ≤ 6, 0.1 ≤ d ≤ 2, R represents an alkali metal element, M represents an element which can have a four-coordinate structure with S and is selected from among the elements in groups 2 to 15 of the periodic table, S represents elemental sulfur, and X represents a halogen element), wherein: in the composition formula, M is composed of a total of three or more elements that include a group 14 element MA and a group 15 element MB; the crystal has three or more tetrahedral structures that include MAS4 and MBS4; and the proportion of Ge in M in the crystal is 0.05 or less in terms of the molar ratio.

A nickel-iron-chromium alloy having excellent high-temperature corrosion resistance is used as a powder, the powder containing spherical particles of a size of 5 to 250 pm, and the alloy including (in wt. %): 35.0 to 38% nickel, 26.0 to 30.0% chromium, >0.7 to 1.50% silicon, 0.40 to 1.30% aluminum, 0.00 to 1.0% manganese, 0.0001 to 0.05% each of magnesium and / or calcium, 0.015 to 0.12% carbon, 0.001 to 0.150% nitrogen, 0.001 to 0.030% phosphorus, 0.0001 to 0.020% oxygen, a maximum of 0.010% sulfur, less than 1.0% molybdenum, less than 1.0% cobalt, less than 0.5% copper, less than 1.0% tungsten, the remainder being iron and the usual process-related impurities, it being necessary to satisfy the following equation: Fc=−1.2+0.29*Ni−4.6*Si−4.4*Al<2.5 (1 a), where Ni, Si and Al are the concentration of the elements in question in wt. %.

The invention relates to the technical field of commercial vehicle air compressor air cylinder bodies, in particular to an air cylinder body casting and a preparation method thereof.The air cylinder body casting comprises, by weight, 3.2%-3.45% of carbon element, 1.7%-1.9% of silicon element, 0.85%-0.9% of manganese element, 0.06%-0.08% of phosphorus element, 0.06%-0.09% of sulfur element, 0.45%-0.54% of copper element, 0.12%-0.20% of chromium element, 0.026%-0.040% of antimony element, 0.053%-0.061% of tin element and the balance iron element. The cylinder block casting has the advantages of high tensile strength and hardness, and the application range of the cylinder is effectively widened.

The invention relates to the preparation of sulfur suspension, in which molten sulfur is atomized and the resulting atomized sulfur droplets are incorporated in a dispersion medium. In the process the formation of atomized sulfur droplets is separated in space and time from their incorporation. The invention also relates to the sulfur suspension produced, as well as the atomizing-suspending device used for the preparation of sulfur suspension and the rotary disc used in the atomizing-suspending device.

Provided is an ultra-high-strength reinforcing bar and a method for manufacturing the same are disclosed. In an exemplary embodiment, the ultra-high-strength reinforcing bar includes an amount of 0.10 to 0.45 wt % carbon (C), an amount of 0.5 to 1.0 wt % silicon (Si), an amount of 0.40 to 1.80 wt % manganese (Mn), an amount of 0.10 to 1.0 wt % chromium (Cr), an amount greater than 0 and less than or equal to 0.2 wt % vanadium (V), an amount greater than 0 and less than or equal to 0.4 wt % copper (Cu), an amount greater than 0 and less than or equal to 0.5 wt % molybdenum (Mo), an amount of 0.015 to 0.070 wt % aluminum (Al), an amount greater than 0 and less than or equal to 0.25 wt % nickel (Ni), an amount greater than 0 and less than or equal to 0.1 wt % tin (Sn), an amount greater than 0 and less than or equal to 0.05 wt % phosphorus (P), an amount greater than 0 and less than or equal to 0.03 wt % sulfur (S), an amount of 0.005 to 0.02 wt % nitrogen (N), and the remainder being iron (Fe) and other inevitable impurities.

The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 %, 0.15% ≤ Manganese ≤ 0.2%, 3% ≤ Silicon ≤ 3.6%, 0.7% ≤ Aluminum ≤ 1.3 %, 0 % ≤ Phosphorus ≤ 0.15 %, 0 % ≤ Sulfur ≤ 0.006 %, 0 % ≤ Nitrogen ≤ 0.09% with 3.85% ≤ Si+Al+Mn ≤ 5.5% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1%, 0% ≤ Titanium ≤ 0.1%, 0% ≤ Vanadium ≤ 0.1%, 0% ≤ Chromium ≤ 1%, 0% ≤ Molybdenum ≤ 0.5%, 0% ≤ Tungsten≤ 0.1%, 0% ≤ Cobalt ≤ 1%, 0% ≤ Arsenic ≤ 0.05%, 0.001% ≤ Calcium ≤ 0.01%, 0% ≤ Copper ≤ 1%, 0% ≤ Nickel ≤ 1%, 0 % ≤ Boron ≤ 0.05%, 0 % ≤ Lead ≤ 0.2%, 0% ≤ Tin≤ 0.2%, 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and eddy current loss in total iron loss of 35 to 55% when calculated in accordance with Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.635T to 1.670T.

The invention discloses a separation process for improving the quality of copper fine sulfur concentrate, and relates to the technical field of mineral processing engineering, the separation process comprises the following steps: S1, raw material pretreatment; s2, performing size mixing and activation with acidic water; s3, closed-loop flotation is conducted; and S4, product combination and collection. The core indexes of the total sulfur concentrate obtained through the technology are that the S + Fe grade is larger than or equal to 90%, the sulfur operation recovery rate is larger than or equal to 89%, the sulfur grade is larger than or equal to 47%, the iron grade is larger than or equal to 42%, the copper grade is smaller than or equal to 0.3%, and the arsenic grade is smaller than or equal to 0.24%, the industrial upgrading target is completely achieved, and the problem that traditional sulfur concentrate is difficult to sell is solved. The S + Fe grade of the first sulfur concentrate is larger than or equal to 91%, the first sulfur concentrate can serve as high-end sulfur concentrate to be sold independently, and the product additional value is increased.

The invention relates to a nickel-based alloy powder, that comprises in weight percentages, 14.00 to 15.25% of chromium, 14.25 to 15.75% of cobalt, 4.00 to 4.60% of aluminium, 0 to 0.50% of iron, 0 to 0.15% of manganese, 3.00 to 3.70% of titanium, 3.90 to 4.50% of molybdenum, 0 to 0.015% of sulphur, 0 to 0.06% of zirconium, 0.012 to 0.020% of boron, 0 to 0.20% of silicon, 0 to 0.10% of copper, 0 to 150 ppm of carbon, 0 to 0.5 ppm of bismuth, 0 to 5 ppm of lead, 0 to 1000 ppm of platinum, 0 to 1000 ppm of palladium, 0 to 50 ppm of hydrogen, 0 to 5 ppm of silver, 0 to 120 ppm of nitrogen, 0 to 1000 ppm of rhenium, 0 to 410 ppm of oxygen and 0 to 500 ppm of inevitable impurities, the rest being made up of nickel, and has a particle size D10 between 3 and 10 μm, a particle size D90 between 20 and 40 μm and a particle size D50 between 10 and 20 μm, the values of the particle sizes D10, D50 and D90 having been measured by laser diffraction according to standard ISO 13322-2. The invention also relates to a method for manufacturing a part using said powder and a resulting part.

The invention provides a method for detecting whether a wet process is healthy or not. The method comprises the steps that S1, a clean blank wafer is provided; s2, carrying out a wet process on the front surface of the wafer, wherein a solvent of the wet process contains a sulfur element; s3, performing wet processing on the back surface of the wafer, wherein a solvent for wet processing does not contain sulfur element; s4, performing defect scanning on the front surface of the wafer to obtain a first scanning result; s5, judging whether aggregation defects exist in the first scanning result or not; if yes, the wet process is not healthy, and if not, the wet process is healthy. According to the method and the device, the presence or absence of the sulfur element residue is judged by judging the presence or absence of the aggregated defect on the front surface of the wafer, so that the aim of detecting whether the wet process is healthy or not is fulfilled, the unhealthy wet process can be optimized, and the performance and the reliability of the device are improved.

The invention relates to a method for evaluating the influence of hydrogen on stress corrosion fracture of pipeline steel in an acid environment, which comprises the following steps: (1) respectively carrying out slow strain rate tensile tests in the acid environment and a nitrogen environment, and determining the damage degree of the acid environment on the mechanical property of a pipeline steel sample; (2) carrying out fast and slow scanning anodic polarization curve test, hydrogen permeation curve test and hydrogen filling-slow stretching test on the pipeline steel sample, and determining the damage degree of hydrogen separated out by cathodic reaction on the mechanical property of the pipeline steel sample; and (3) determining the influence degree and contribution rate proportion of hydrogen to the stress corrosion fracture of the pipeline steel in the acid environment. According to the method, the stress corrosion performance of the sulfur-resistant pipeline steel can be accurately and quickly evaluated, the proportion and contribution rate of hydrogen-induced stress corrosion sensitivity in the stress corrosion sensitivity of the pipeline steel in the acid environment are analyzed, and the influence degree of hydrogen on stress corrosion fracture of the pipeline steel in the acid environment is quantitatively represented.