4817results about "Additives" patented technology

The invention discloses environment-friendly shield tail sealing grease for a high-water-pressure shield tunnel and a preparation method. The shield tail sealing grease is prepared from the following materials in parts by weight: 240 to 305 parts of base oil, 25 to 140 parts of a viscosity index modifier, 40 to 140 parts of a thickening agent, 510 to 640 parts of a filling agent, 30 to 55 parts of a reinforcing agent, 10 to 35 parts of calcium-based lubricating grease and 8 to 25 parts of a composite modified additive. A mixture of recycled vegetable oil and C5 petroleum resin is used as base oil, plant fiber is used as a reinforcing agent, a mixture of polyisobutene, polymerized rosin, succinimide and polyisoprene is used as a viscosity index modifier, a mixture of polyisobutene, alginic acid and sodium polyacrylate is used as a thickening agent, and an organic lubricating material and a calcium filler are used as reinforcing agents. Calcium-based lubricating grease is added, and thymol, zinc borate and zinc dialkyl dithiophosphate form a composite modified additive. The environment-friendly shield tail sealing grease for the high-water-pressure shield tunnel is formed by adopting a preparation process of drying, filtering, heat preservation, constant temperature and speed-controlled physical kneading.

This disclosure relates to the use of di(alkyl substituted phenyl)amine antioxidants as additives in lubricant compositions having good oxidation properties in engine crankcase applications, especially in compression ignited engine and or spark ignited engine applications, where the antioxidant comprises from 0 to 10 mass% mono-C9-alkyl substituted diphenyl amine, and 90 to 100 mass% di-C9-alkyl substituted phenyl amines based upon the weight of the mono- and di-C9-alkyl substituted phenyl amines, preferably where tri-C9-alkyl substituted phenyl amines are minimized and ortho substituted di-C9-alkyl substituted phenyl amines are minimized.

The invention relates to a bis-polyisobutylene alcohol amine compound and compositions thereof. The invention also is directed to a new process for making the bis-polyisobutylene alcohol amine by reacting a polyisobutylene epoxide with a polyamine, optionally in the presence of a catalyst, a protic solvent initiator and / or a diluent. In addition, the invention further relates to the many uses of the bis-polyisobutylene alcohol amine including but not limited to its use in lubricants, surfactants, emulsifiers, resins, and the like.

The invention relates to the technical field of lubricating oil, in particular to graphene composite rolling oil and a preparation method and application thereof. The rolling oil comprises base oil, branched oleic acid modified graphene containing quaternary ammonium salt, an anti-wear reagent at extreme pressure, an antioxidant, an anti-rust agent and a defoaming agent. Wherein the quaternary ammonium salt branched oleic acid is prepared through a thiol-ene click reaction and a quaternization reaction, and the dispersity, the interface adsorption strength and the high-temperature stability of graphene in a lubricating oil system can be remarkably improved. The product provided by the invention is suitable for rolling lubrication under severe working conditions such as high temperature and high load, and has a wide industrial application prospect.

Disclosed herein are solid-liquid bi-phase lubricating devices that can include a cuboidal shaped stick with at-least one cylindrical or cuboidal shaped hollow core running through entire or partial length of the stick. The cuboidal shaped stick can include a solid polymer-based composite while the inner space is filled with a semi-fluid grease lubricant. The solid polymer-based composite can include one or more polymers, filler materials, corrosion inhibitors, plasticizers, and additives. The grease lubricant can include lithium, lithium-complex, aluminum-complex, calcium-sulphonate complex, bentone-thickened grease, and mixtures thereof and have an NLGI consistency grade≥1. The lubricating devices can be used for friction reduction of mechanical components involving two or more contacting surfaces in relative motion, such as a steel wheel flange-rail contact interface of transit and freight rail transport systems.

The invention discloses a preparation method of modified self-extinguishing insulating oil with flame-retardant and self-repairing functions. Wherein the insulating liquid is mixed oil of mineral oil and palm oil-based modified natural ester, and the inherent high flash point characteristic of the natural ester improves the fireproof safety of the insulating oil. The modified hexagonal boron nitride (h-BN), the magnesium hydroxide nano material and the microcapsule repairing agent are added into the insulating oil, and the h-BN can capture free electrons in the oil, so that the formation and expansion of electric arcs are inhibited, and the breakdown voltage is improved. Magnesium hydroxide is heated to decompose and absorb heat, the fault temperature is reduced, and therefore the arc self-extinguishing effect is achieved. Under the action of a high electric field and a high temperature, the capsule wall of the microcapsule repairing agent is broken, meanwhile, the repairing material is released, a chemical reaction is carried out, and the insulating property of the insulating oil is repaired. The modified insulating oil prepared by the invention has high insulating strength and high flame retardance, and also has a performance self-repairing function, so that the service life of the insulating oil is prolonged.

This invention relates to a lubricating oil composition comprising: at least 50 mass % or more of one or more base oils; detergent; and 0.01 to 20 mass % of a functionalized polymer comprising a partially or fully saturated olefin homopolymer or copolymer backbone and at least one functional group, having: i) an Mn of 10,000 g / mol or more (GPC-PS) of the polymer prior to functionalization, ii) where in the functional group is derived from an acylating agent and a compound containing amino and / or hydroxyl groups, and iii) optionally, wherein the homopolymer or copolymer backbone is derived from monomers selected from the group consisting of C2 to C30 (such as linear) alpha olefins and C4 to C20 conjugated dienes; where PIBSA-PAM having an Mn of 1,600 g / mol or more (GPC-PS) is absent or substantially absent from the lubricating oil composition, or, if present, is present in an amount such that the weight ratio of the functionalized polymer (B) to the high molecular weight PIBSA-PAM is at least 0.25:1.

To provide a novel lubricant agent additive and a novel lubricant agent composition that can reduce friction of a sliding part.SOLUTION: A lubricant agent additive comprises a polymer containing an olefin compound as a monomer unit or a modified polymer obtained by modifying a hydrogenated polymer with maleic acid or maleic anhydride. A lubricant agent composition comprises: a base oil; and a polymer containing an olefin compound as a monomer unit or a modified polymer obtained by modifying a hydrogenated polymer with maleic acid or maleic anhydride.SELECTED DRAWING: None

The instant disclosure generally relates to lubricating compositions having an oil of lubricating viscosity, an ashless phosphorus-containing antiwear agent an alkaline earth metal detergent, an ashless antioxidant, and an ashless dispersant where the lubricating compositions are substantially free of zinc and methods of lubricating an engine with such lubricating compositions. The instant lubricating compositions are useful as alternative lubricating compositions the reduce and / or eliminate zinc to achieve a desired performance goal of the lubricating composition.

The invention relates to the technical field of petroleum drilling fluids, in particular to a lubricant additive and a preparation method thereof, a lubricant, a water-based drilling fluid and a preparation method thereof, the lubricant additive comprises the following raw materials: 6 parts of taurine, 30-60 parts of 1-bromohexadecane, 8.5-15 parts of potassium hydroxide, 0.5-0.9 part of potassium iodide, 30-60 parts of thionyl chloride, 2-4 parts of N, N-dimethylformamide, 7-17 parts of ammonia water and 30 parts of trichloromethane. The lubricant additive takes sulfonic acid amine as an active adsorption group, and can be stably adsorbed on a drill stem, a sleeve and a mud cake. Meanwhile, two C16 flexible chains are arranged, a compact lubricating film can be formed, and friction resistance is efficiently reduced.

The present invention relates to the field of corrosion prevention materials. Disclosed are anticorrosive oil and an anticorrosive material, and preparation methods therefor and the use thereof. The anticorrosive oil contains a monoalkoxy titanate, a dihydroxypropyl octadecanoate, an organosilicon defoaming agent, an antioxidant, modified nano silicon dioxide, nano titanium dioxide, graphene and aluminum tripolyphosphate, wherein the hydroxyl content of the modified nano silicon dioxide is 0.1-0.5 / nm2, and the particle size of the modified nano silicon dioxide satisfies: calculated on the basis that the particle size interval width is 5 nm, the range of particle size having the maximum proportion is 10-15 nm, and the proportion thereof is 45-55 wt%. There are no gaps between the layers of an anticorrosive material formed by means of the anticorrosive oil of the present invention, and the anticorrosive material has good sealing and good corrosion resistance, impact resistance and ultraviolet aging resistance, and can provide long-acting corrosion prevention for ocean steel piles.

A lubricating oil composition is described. The composition includes a major amount of a base oil of lubricating viscosity and a polyphosphate-based dispersion. The dispersion includes an ammonium polyphosphate and a dispersing agent.

The invention discloses a preparation method of a modified lubricating oil additive containing graphene-silicon dioxide, which comprises the following steps: preparing an RGO / SiO2 nano composite material additive with SiO2 grafted on graphene by a hydrothermal method, and adding oleic acid (OA) to participate in a hydrothermal reaction to prepare an OA-RGO / SiO2 nano composite material additive with SiO2 and OA grafted on graphene; according to the preparation method, the morphology size of the lubricating oil additive is optimized, and the tribological performance and dispersion stability of the lubricating oil additive are improved; the microstructure of the composite material is observed through an SEM scanning electron microscope, it is found that a sheet layer on the surface of the composite material added with oleic acid is thinner and wrinkled, the particle size of nano particles is smaller, the nano particles are wrapped by the sheet layer more tightly, and the nano particle diameter of the OA-RGO / SiO2 additive is reduced by 18.42% compared with that of an RGO / SiO2 additive; in a contact angle test, the nano additive in which oleic acid participates in a hydrothermal reaction can further reduce the surface energy of the nano additive, and the contact angle is greatly reduced.

Provided is a lubricating oil composition containing a base oil (A), a phosphorous acid ester (B) having at least one sulfur atom-containing group having 2 to 20 carbon atoms, the sulfur atom-containing group having at least one -(S)x- group (x is an integer of 1 or more) between two adjacent carbon atoms in a structure of an alkyl group, a thiadiazole-based compound (C), and a benzotriazole-based compound (D), wherein a content of the component (C) is 0.01 mass% or more and less than 0.60 mass% based on the total amount of the lubricating oil composition, and a content of the component (D) is 0.02 mass% or more and less than 0.20 mass% based on the total amount of the lubricating oil composition.

A lubricating composition includes an oil of lubricating viscosity, a phenolic antioxidant, a succinimide dispersant which is at least substantially free of boron, a detergent comprising an alkaline earth metal salicylate and a sulfurized organic compound.

This invention relates to a diesel engine lubricating oil composition comprising or resulting from the admixing of: (i) base oil, (ii) a functionalized polymer, (iii) an overbased magnesium based detergent, and (iv) one or more, optionally borated, higher and / or lower molecular weight PIBSA-PAM dispersant. The composition has a total sulfated ash of less than or equal to 0.9 wt. %, a kinematic viscosity at 100° C. of 5 to 20 cSt, a total phosphorous level of less than or equal to 0.120 wt. %, and a total sulfur level of less than or equal to 0.35 wt. % and provides a Detroit DD-13 scuffing test result of at least 31 hours. Also provided are a method of making the composition, a method of lubricating a diesel engine, a method of improving wear performance and engine cleanliness and reducing emissions of a diesel engine, and a diesel engine oil additive concentrate composition.

A lubricating grease for electric vehicle applications includes thickener 6% by weight (wt. %) to 12 wt. %, lubricating oil 57 wt. % to 92.98 wt. %, and surface-active ester 1 wt. % to 10 wt. %. The lubricating grease also includes additives including friction reducer and modifier 0.1 wt. % to 5 wt. %, anti-wear agent 0.1 wt. % to 5 wt. %, and a balance of extreme pressure agent, oxidation inhibitor, and corrosion inhibitor.

The present invention provides a soluble cold rolling oil composition in which oil particles of approximately 0.1 μm or less are dispersed in water, and which has rolling properties (particularly anti-seizure properties) equal to or better than those of water-insoluble rolling oils and emulsion-type rolling oils, while enabling the gloss of products to be made uniform and enabling an improvement in unit consumption compared to emulsion-type rolling oils; and a cold rolling method using the composition. [Solution] A cold rolling oil composition containing (A) a base oil, (B) a specific fatty acid, (C) a specific sulfur-based extreme pressure agent, (D) a specific water-soluble polymer, and (E) a specific amine, and a cold rolling method using the same.

The invention provides a composite additive based on 2, 6-butylated hydroxytoluene, phosphate fire-resistant oil and application, the composite additive is a mixture of 2, 6-butylated hydroxytoluene and Revonox 501, the addition amount of 2, 6-butylated hydroxytoluene is 0.01%-0.10%, the addition amount of Revonox 501 is 0.0020%-0.0050%, the addition amount of 2, 6-butylated hydroxytoluene is 0.01%-0.10%, the addition amount of 2, 6-butylated hydroxytoluene is 0.0020%-0.0050%, and the addition amount of 2, 6-butylated hydroxytoluene is 0.01%-0.10%. After the phosphate fire-resistant oil is added with the composite additive, the comprehensive performance of the phosphate fire-resistant oil in the operation process can be improved, and the defects that after new phosphate fire-resistant oil is loaded into a system, the action flexibility of a steam turbine assembly is reduced and a servo valve of a speed regulating system is corroded and jammed due to the phenomena that the acid value is increased, the resistivity is reduced, oil sludge is generated and the like in the use process are overcome; and the operation safety of a turbine set of a power plant is influenced.

A liquid composition for providing enhanced lubrication and wear protection, particularly under high-performance and / or extreme-pressure conditions. The composition comprises components that are either solubilized, liquified, or sub-micronized, and are formulated to result in a stable, color-tunable composition that can be stored or implemented over extended periods of time without separation of solid components from the liquid. A composition can either be a lubricant in which the solubilized, liquified, or sub-micronized components are comprised within a base oil, or an additive composition in which the components are formulated to be later added to a base oil. Suitable base oils are industrial, automotive, or open gear oils such as those used in the oil and gas industry, sugar mills, or in rock crushers; rock drill, pneumatic, and air tool oils; anti-seize compounds; cutting, gun, engine, air compressor, or bearing oils; slideway lubricants; and oven, kiln, foundry, metalworking, metalforming, or aerospace lubricants.

This disclosure relates to the use of di(alkyl substituted phenyl)amine antioxidants as additives in lubricant compositions having good oxidation properties in engine crankcase applications, especially in compression ignited engine and or spark ignited engine applications, where the antioxidant comprises from 0 to 10 mass% mono-C9-alkyl substituted diphenyl amine, and 90 to 100 mass% di-C9-alkyl substituted phenyl amines based upon the weight of the mono- and di-C9-alkyl substituted phenyl amines, preferably where tri-C9-alkyl substituted phenyl amines are minimized and ortho substituted di-C9-alkyl substituted phenyl amines are minimized.

This invention relates to a method of reducing abnormal combustion events in a hydrogen fueled internal combustion engine (HICE) during operation of the engine. The method includes the steps of: a) providing to the HICE a lubricating oil composition including or resulting from the admixing of: i) a base oil having a KV100 of less than or equal to 12 cSt and included at greater than 40 wt.% of the composition and comprising a Group I base oil, a Group II base oil, or combinations thereof; ii) at least one optionally borated polyisobutylene succinimide (PIBSA-PAM) dispersant at from 0.25 wt.% to 12.0 wt.% of the composition, wherein the optionally borated PIBSA-PAM dispersant is selected from the group consisting of lower molecular weight PIB SA-PAM dispersant (Mn less than 1600 g / mol), higher molecular weight PIBSA-PAM dispersant (Mn 1600 g / mol or more), and combinations thereof; iii) at least one overbased metal containing detergent with a Total Base Number (KOH / g) greater than or equal to 9 and less than or equal to 500 and included at a treat level to deliver between 100 to 5000 ppm by weight of total metal and between 0.15 wt. % to 8.0 wt. % of total soap to the composition; and iv) the lubricating oil composition having a total sulfated ash of less than or equal to 2.5 wt.%, a total phosphorous level of less than or equal to 0.120 wt.%, and a SAE viscosity grade of 25W-X, 20W-X, 15W-X, 10W-X, 5W-X or 0W-X, where X represents any one of 8, 12, 16, 20, 30, 40, 50 or 60; and b) providing a fuel comprising hydrogen to the hydrogen fueled internal combustion engine; and c) combusting the fuel in the hydrogen fueled internal combustion engine. Also provided are lubricating oil compositions for use in a HICE to reduce the propensity for abnormal combustion events.

The invention belongs to the technical field of insulating oil, and provides a slow-release antioxidant as well as a preparation method and application thereof, the preparation method comprises the following steps: (1) mixing octadecyl trimethyl ammonium bromide, 2, 6-butylated hydroxytoluene, tetraethoxysilane, water and ammonia water, and reacting to obtain the antioxidant; and (2) in a protective atmosphere, mixing the antioxidant, ethanol, water and gamma-mercaptopropyltriethoxysilane, and carrying out a reaction so as to obtain the slow-release antioxidant. The slow-release antioxidant suitable for the synthetic ester insulating oil is prepared through a physical coating means and oleophylic modification, has excellent solubility, can effectively inhibit the increase of the acid value of the synthetic ester insulating oil, delays the oxidation process of the synthetic ester insulating oil, and remarkably prolongs the service life of the insulating oil. Meanwhile, through a slow release mechanism, the antioxidant can prolong the antioxidant effect of the antioxidant, improve the antioxidant stability in long-time operation and meet the higher antioxidant requirement of high-performance equipment such as a transformer for the insulating oil.

The present invention relates to a method for synthesizing graphene, and more particularly, to a method for synthesizing graphene by flash Joule heating (FJH). Such methods may be used to synthesize disordered graphene in large volumes, including low-defect disordered graphene. Such methods may further be used in the synthesis of composite materials and 2D materials.

The invention provides lithium-based lubricating grease and a preparation method thereof. Based on the total weight of the lubricating grease, the lithium-based lubricating grease comprises 0.1-5% of a tetraphenyl ethylene derivative, 0.1-5% of an oxidation and corrosion inhibitor, 0.1-5% of an anti-rust agent, 3-30% of a lithium-based thickening agent and a main amount of lubricating base oil, and the structure of the tetraphenyl ethylene derivative is as shown in a formula (I): # imgabs0. The lithium-based lubricating grease has excellent oxidation resistance, and can be used as a lubricating grease additive. Meanwhile, the consumption of the antioxidant can be predicted through the fluorescence intensity, and the antioxidant also has good extreme pressure anti-wear property, mechanical stability, colloid stability, high dropping point, corrosion resistance and the like.

To provide a lubricant composition having high metal corrosion resistance and capable of being suitably used for lubrication of an internal combustion engine using a fuel containing ammonia.SOLUTION: A lubricant composition used for lubrication of a marine engine using a fuel containing ammonia comprises a base oil (A), an amide-based compound (B), a metal deactivator (C), an organic zinc dithiophosphate (D), and a calcium-based detergent (E), wherein a content of the component (C) is less than 0.30 mass% based on the total amount of the lubricant composition, a content of the component (E) in terms of calcium atoms is 5,000 mass ppm or more based on the total amount of the lubricant composition, a base number of the lubricant composition is 10.0 or more, and a sulfated ash content of the lubricant composition is more than 1.10 mass%.SELECTED DRAWING: None

The invention discloses a modified hexagonal boron nitride nanosheet, a modified hexagonal boron nitride grinding fluid and a preparation method of the modified hexagonal boron nitride nanosheet, the modified hexagonal boron nitride nanosheet is a hydroxylated h-BN nanosheet prepared through an electrolytic method, and the modified hexagonal boron nitride grinding fluid comprises the following components in percentage by mass: 60-80% of deionized water; 5-15% of a surfactant II; 5-15% of a modified hexagonal boron nitride nanosheet; 5-15% of a grinding aid; and a pH regulator II. H2O2 is used as a mild oxidizing agent, and hydroxyl can be introduced under the condition that the basic structure of h-BN is not damaged; the electrolysis process not only promotes decomposition of H2O2 to generate active hydroxyl, but also contributes to stripping of h-BN; more uniform hydroxyl distribution can be generated on the h-BN surface through the electrolytic method; compared with a ball milling method and an electrolytic method, the hydroxylation and stripping processes can be completed within a shorter time, mechanical damage in the ball milling process is avoided, the integrity of the h-BN nanosheet is kept, and expanded production is easy.

Systems and methods for heating feedstock, thermal decomposition of feedstock, and chemically activated chemical reaction of feedstock by indirectly heating the feedstock with a volume of joule heated electrically conductive powder that heats the feedstock, wherein the feedstock can be gas, liquid, or solid. The embodiments disclosed herein further relate to systems and methods for joule heating induced pyrolysis or thermal decomposition of feedstock, including methane or other hydrocarbons to produce, for example, hydrogen and / or various carbon materials that are collected.

The invention provides an ash-free antirust agent and a preparation method thereof. The preparation method comprises the following steps: in a non-polar solvent, mixing dinonyl naphthalene sulfonic acid and dodecenylsuccinic acid to obtain a mixed acid A; the preparation method comprises the following steps: mixing polyethylene polyamine and mixed acid A according to a molar ratio of (0.5-2.0): 1, and adding deionized water and methanol to react until the pH value of the solution is neutral; and adding methyl methacrylate and base oil into the reacted system, heating and distilling, and then carrying out reduced pressure distillation until no obvious distillate is generated, thereby obtaining the ash-free antirust agent. The invention also provides the ash-free antirust agent prepared by the method. The ashless antirust agent integrates the advantages of the dinonyl naphthalene sulfonic acid group and the dodecenyl succinic acid group on the molecular level, the antirust property is better, and the ashless antirust agent and the anti-wear reagent at extreme pressure have a very good synergistic effect.