18803 results about "Anode" patented technology

The invention relates to the technical field of anode carbon block roasting, and discloses an energy-saving control system of an anode carbon block roasting furnace, which comprises a data acquisition module, an energy-saving analysis module, a digital twin modeling module, a control execution module and a feedback optimization module, when the combustion state of the roasting furnace is monitored in real time, a multi-layer monitoring framework is constructed to dynamically track the change trend of temperature, flue gas oxygen content and pressure parameters, continuous comparison is performed based on a preset energy-saving reference interval, and when the parameters deviate from an optimization interval, a digital twinborn model is immediately triggered to intervene in analysis, so that the real-time monitoring of the combustion state of the roasting furnace is realized. Prejudgment identification of potential risks of combustion efficiency reduction and abnormal heat loss is achieved, hidden energy loss caused by imbalance of the air-fuel ratio is avoided, the non-planned shutdown frequency of equipment is reduced, and the continuous energy efficiency management and control stability of the production process is guaranteed.

The present disclosure provides a display substrate and a method of manufacturing the same, a display panel, and a display apparatus. The display substrate includes a base substrate, pixel units are arranged in an array on the base substrate, each pixel unit includes an anode, a light-emitting functional layer and a cathode, a pixel definition layer is provided, and has a plurality of openings, and each opening exposes a portion of an anode; the light-emitting functional layer is located in the opening; at least a portion of two opposite ends of the anode along a first direction is warped in a direction toward the cathode, an orthographic projection of the warped portion of the anode on the base substrate does not overlap with that of the cathode on the base substrate, and a hollow region is provided at a position of the cathode at least corresponding to the warped portion.

The invention provides a preparation method of a porous carbon-silicon composite negative electrode material of a lithium battery. The preparation method comprises the following steps: constructing a multi-stage template system; carrying out carbon precursor impregnation and gradient temperature carbonization on the multistage template system; removing the template to form a gradient porous carbon carrier; carrying out gradient temperature zone silane deposition; and plasma-assisted carbon coating and nitrogen doping are carried out. According to the method, a silicon dioxide sphere hard template is combined with cetyltrimethylammonium bromide and a block copolymer soft template to form a porous carbon carrier with a micropore-mesopore-macropore three-stage structure, and gradient distribution of silicon in porous carbon is realized by utilizing a three-temperature-zone fluidized bed reactor and a pulse type deposition technology, so that the silicon-based porous carbon composite material is obtained. The problem of volume expansion of the silicon material is effectively relieved and the material cycling stability is improved. The porous carbon-silicon composite negative electrode material prepared by the invention has high specific surface area, excellent ion transmission channel and good structural stability, and can be applied to a high-energy-density lithium ion battery.

The invention discloses an asphalt-based hard carbon material as well as a pre-oxidation preparation method and application thereof. Belongs to the technical field of asphalt-based hard carbon materials. The pre-oxidation preparation method comprises the following steps: carrying out primary pre-oxidation treatment on asphalt at 250-400 DEG C in air flow of 50-500mL / min; crushing the obtained primary pre-oxidized asphalt, and then carrying out secondary pre-oxidation treatment at 250-400 DEG C in air flow of 50-500mL / min to obtain secondary pre-oxidized asphalt; and carrying out carbonization treatment on the secondary pre-oxidized asphalt. According to the method, the asphalt can be kept in a solid-phase state to be subjected to efficient and thorough oxidation cross-linking reaction, the production cost is reduced, the obtained asphalt-based hard carbon material has high first coulombic efficiency and high capacity, and powerful support is provided for commercial application of sodium-ion battery negative electrode materials and rapid development of an energy storage technology.

The invention discloses a high-speed multi-photon detection system and method. The system comprises a detector and a signal processing circuit, wherein the detector is composed of a window plated with a photoelectric cathode, a micro-channel plate stack and an anode; a plurality of incident photons are converted into a plurality of photoelectrons by the photoelectric cathode, and the photoelectrons are converted into electron cloud by the micro-channel plate stack; the incident electron cloud is divided into multiple paths by three layers of staggered metal strip electrodes of the anode, and charge collection is carried out to obtain charge short pulses of each layer of electrode; the signal processing circuit converts the charge short pulses transmitted by the three layers of electrodes into digital pulse signals, obtains the centroid coordinates of the electron cloud from the digital pulse signals as the abscissa value, the ordinate value and the verification value of the incident photon position, combines the abscissa value, the ordinate value and the verification value based on the screening condition to obtain the target two-dimensional coordinates, and finally obtains the target two-dimensional coordinates. And transmitting to a terminal for imaging display. According to the invention, a plurality of synchronous photons can be detected, the overall counting rate of the detector is greatly improved, and the detection efficiency is improved.

The utility model discloses an electrolytic bath bipolar plate with micropore flow channels and an electrolytic bath, a micropore flow channel network is arranged on the side surface of an anode of a plate body, and the micropore flow channel network comprises a plurality of groups of micropore flow channel units which are arranged at intervals along the width direction of the plate body; each micropore flow channel unit comprises a main flow channel arranged in the length direction of the plate body and a plurality of first-stage branch flow channels arranged in the length direction of the main flow channel at intervals, a plurality of short branch flow channels are arranged on the two sides of each first-stage branch flow channel at intervals, and a jet hole is formed in the top of each short branch flow channel. The jet flow holes are formed in the direction perpendicular to the side surface of the anode, the length of the short branch runner is smaller than that of the first-stage branch runner, and the short branch runner is perpendicular to the first-stage branch runner. And the microporous flow channel network adopts a structure of combining tree fractal and T-shaped nodes, so that the mass transfer uniformity of water flow in the microporous flow channels can be improved, and the water-membrane contact efficiency is improved, thereby ensuring the hydrogen production efficiency of the bipolar plate.

The invention relates to a modified current collector for a cathode-free metal battery and a preparation method and application thereof.The preparation method comprises the steps that an in-situ modification reaction is conducted on the surface of a copper current collector to obtain a current collector coated with a copper oxide nanometer material, and then selenium is introduced to the surface of the current collector coated with the copper oxide nanometer material through a partial in-situ substitution reaction to obtain the modified current collector coated with the copper oxide nanometer material. The preparation method comprises the following steps: preparing a copper selenide and copper oxide composite modified current collector, performing in-situ lithiation reaction through electrochemical deposition, and partially converting to generate corresponding lithiates, thereby obtaining the modified current collector for the non-anode metal battery. According to the invention, the functional artificial interface layer with lithium affinity, high stability and high ionic conductivity is constructed on the surface of the copper-based current collector in situ, so that the key problems of uneven metal deposition and unstable SEI layer on the surface of the negative electrode current collector in the current research of the metal secondary battery without the negative electrode are solved, the formation of dendritic crystals and the occurrence of side reactions are inhibited, and the service life of the metal secondary battery is prolonged. Therefore, the coulombic efficiency, the safety and the cycle life of the battery are improved.

The invention relates to the technical field of batteries, in particular to a silicon-carbon negative electrode material, a preparation method thereof and a lithium ion battery. The invention provides a silicon-carbon negative electrode material. The silicon-carbon negative electrode material comprises silicon nanoparticles, a porous carbon skeleton, an amorphous carbon layer and a carbon material array structure, pores of the porous carbon skeleton are filled with the silicon nanoparticles; the amorphous carbon layer is coated on the surface of the porous carbon skeleton; the carbon material array structure vertically grows on the surface of the amorphous carbon layer; the carbon material array structure comprises a carbon nanotube array and / or a graphene array. According to the silicon-carbon negative electrode material disclosed by the invention, the compressive strength and the conductivity of the silicon-carbon negative electrode material are improved by vertically growing the carbon nanotube array and / or the graphene array on the surface; therefore, the cycle performance and the rate capability are improved, and the cycle expansion rate is reduced.

Embodiments described herein relate to electrochemical cells with multiple separators, and methods of producing the same. A method of producing an electrochemical cell can include disposing an anode material onto an anode current collector, disposing a first separator on the anode material, disposing a cathode material onto a cathode current collector, disposing a second separator onto the cathode material, and disposing the first separator on the second separator to form the electrochemical cell. The anode material and / or the cathode material can be a semi-solid electrode material including an active material, a conductive material, and a volume of liquid electrolyte. In some embodiments, less than about 10% by volume of the liquid electrolyte evaporates during the forming of the electrochemical cell. In some embodiments, the method can further include wetting the first separator and / or the second separator with an electrolyte solution prior to coupling the first separator to the second separator.

The invention discloses a Schottky diode and a manufacturing method thereof, the Schottky diode comprises a substrate, an epitaxial layer, a cathode layer, a plurality of first ion implantation regions, a plurality of first grooves, a second barrier metal layer and an anode layer, the plurality of first ion implantation regions and the plurality of first grooves are arranged in a main junction region, a first ion implantation region is arranged at the bottom of the first groove, a PN junction is formed between the first ion implantation region and the epitaxial layer, a second ion implantation region is arranged at the bottom of the first groove, a PN junction is formed between the second ion implantation region and the epitaxial layer, and a first barrier metal layer is arranged on the side wall of the first groove; the second barrier metal layer is arranged on one side, far away from the substrate, of the epitaxial layer, is positioned in the main junction region and is connected with the first ion implantation region and the first barrier metal layer; the anode layer is disposed on the second barrier metal layer. Through the above design, the reverse leakage current of the Schottky diode can be greatly reduced, and the forward conduction voltage drop of the Schottky diode can be reduced.

The invention discloses a digital twin drive life prolonging system and method in a lithium battery aging process, the system comprises a sensor detection module, an AI control module and a regulation and control module, the sensor detection module detects pressure, temperature, gas components, SEI film conditions and voltage data between a conductive layer and an anode, and inputs the data into the AI control module; the AI control module performs electrochemical-thermodynamic-mechanics multi-physics field coupling modeling by applying a digital twinborn technology, performs data analysis and processing in combination with cross-working-condition model migration, screens out an optimal regulation and control scheme according to a mirage optimization algorithm, sends an instruction to the regulation and control module, and controls the regulation and control module according to the instruction of the AI control module. Parameters in the energy storage cabin are adjusted, the SEI film state is maintained, and lithium dendrite precipitation is controlled, so that the service life of the lithium battery is prolonged; according to the method, the digital twinborn model is utilized to identify battery capacity attenuation inflection points, trigger lithium supplement or charge strategy optimization and other regulation measures, irreversible damage is avoided, and the replacement frequency is reduced.

Embodiments described herein relate to electrochemical cells with multiple separators, and methods of producing the same. A method of producing an electrochemical cell can include disposing an anode material onto an anode current collector, disposing a first separator on the anode material, disposing a cathode material onto a cathode current collector, disposing a second separator onto the cathode material, and disposing the first separator on the second separator to form the electrochemical cell. The anode material and / or the cathode material can be a semi-solid electrode material including an active material, a conductive material, and a volume of liquid electrolyte. In some embodiments, less than about 10% by volume of the liquid electrolyte evaporates during the forming of the electrochemical cell. In some embodiments, the method can further include wetting the first separator and / or the second separator with an electrolyte solution prior to coupling the first separator to the second separator.

The utility model discloses a mandarin fish domestication feeding device which comprises a feeding pipeline and a bait temporary storage tank arranged at the upper end of the feeding pipeline, a feeding hopper is arranged at the upper end of the bait temporary storage tank, and the feeding pipeline comprises a vertical pipe with the upper end in butt joint with the bait temporary storage tank and a horizontal discharging pipe in butt joint with the bottom of the vertical pipe. One end of the horizontal discharge pipe is connected with a high-pressure water source or air source; the vertical pipe is of a multi-section telescopic rod structure. A cathode ring piece and an anode ring piece are arranged at the two ends of the vertical pipe, and the cathode ring piece and the anode ring piece are connected with a pulse generator used for outputting pulse signals and a pulse power amplifier used for controlling output voltage through wires. The fish feeding device can achieve feeding at different depths, can feed live fish, dead fish and feed according to different proportions, is simple and convenient to operate, greatly reduces the workload of manual feeding, and can be widely applied to the field of bait feeding.

The present invention relates to a system and a treatment method for treating high-phosphorus wastewater and resourcefully utilizing phosphorus elements. The system includes a bipolar membrane electrodialysis device, a phosphorus precipitator, and a membrane treatment device. Inside the bipolar membrane electrodialysis device, there are successively arranged a cathode, a first bipolar membrane, a main cation exchange membrane, a main anion exchange membrane, a second bipolar membrane, and an anode. Between the first bipolar membrane and the main cation exchange membrane is an alkali chamber, between the main cation exchange membrane and the main anion exchange membrane is a wastewater chamber, between the main anion exchange membrane and the second bipolar membrane is an acid chamber, the outside of the first bipolar membrane is a cathode chamber, and the outside of the second bipolar membrane is an anode chamber; the high-phosphorus wastewater is input into the wastewater chamber, the acid chamber is provided with a phosphoric acid recovery pipe, and the alkali chamber and the wastewater chamber are respectively connected to the phosphorus precipitator through an alkali liquid pipe and a first water production pipe; the phosphorus precipitator is provided with a precipitant inlet for inputting a calcium precipitant or a magnesium precipitant, the concentrated water outlet of the membrane treatment device is connected to the wastewater chamber, and the produced water of the membrane treatment device is reused as reclaimed water.

The invention relates to the technical field of batteries, in particular to a copper foil and a preparation method thereof, a current collector, a pole piece and an energy storage device. A connection degree gamma exists between the surface density of the copper foil and the size and arrangement of the through holes, the formula of the connection degree gamma is # imgabs0 #, and the value range of gamma is 1 + / -0.1; the copper foil is prepared through an electrolytic method, and an insulating acid-resistant coating is dispensed on the surface of a cathode of the electrolytic method to form an insulating acid-resistant layer; according to the electrolytic method, an active layer is formed on the surface of an anode by coating a mixed active substance solution and sintering, an inert substance is coated on the surface of the active layer opposite to a point coating position of a cathode to form an inert layer, and the range of the inert layer is smaller than 70% of the area of a pore region. The porous copper foil prepared by the method has a porous structure, the pore size distribution is more uniform, the size is consistent, meanwhile, the parts except the pores are dense copper layers, and the mechanical property of the material is good.

The embodiment of the invention provides an electrostatic precipitator polar plate system ash removal device and a control method thereof, and belongs to the technical field of electrostatic precipitation. The device comprises: a main frame for mounting each working module; the ash removal module comprises a polar plate rolling brush device and a polar line straight brush device; wherein the polar plate rolling brush device is mounted at the front end of the main frame and used for cleaning the surface of an anode plate in an electric precipitator polar plate system; the polar line straight brushing device is installed at the rear end of the upper surface of the main frame and used for cleaning the cathode line surface in the electric precipitator polar plate system. The adsorption walking modules are mounted at four corners of the main frame and are used for adsorbing the device on the surface of the anode plate through magnetic attraction force and driving the device to move; and the thickness measuring device is mounted at the tail end of the main frame and used for detecting the thickness of residual dust on the surface of the anode plate to judge whether reinforced cleaning is needed. According to the scheme, automatic dust removal of the electric dust remover polar plate system is achieved, the manual intervention frequency is effectively reduced, and the dust removal effect and operation safety are improved.

The invention belongs to the technical field of sewage treatment, and particularly relates to an anaerobic ammonia oxidation-photoelectric denitrification deep nitrogen removal method. The method comprises the following steps: firstly, adopting a double-chamber reactor; introducing part of sewage into the cathode chamber, carrying out Anammox reaction under a dark state condition to remove ammonia nitrogen and part of nitrite nitrogen, and synchronously generating nitrate nitrogen; turning on a light source to irradiate the anode chamber, exciting photo-induced electrons by a photosensitizer, transmitting the photo-induced electrons to the cathode chamber through an external circuit, and driving the sulfur autotrophic denitrification sludge to reduce residual nitrite nitrogen and nitrate nitrogen generated by Anammox; the total nitrogen removal rate is close to 100%. According to the invention, photo-induced electrons are used as the only denitrification electron donor, so that the addition of a carbon source / sulfide is thoroughly avoided, and the risk of secondary pollution is eliminated. The method is suitable for green low-carbon deep treatment of sludge digestion liquid and pharmaceutical wastewater high-ammonia-nitrogen low-carbon-nitrogen-ratio sewage.

The invention provides coal-based porous carbon for preparing a silicon-carbon negative electrode material as well as a preparation method and application of the coal-based porous carbon, coal-based porous graphite is used as a matrix carbon material, polymer resin is used as a rigid bonding and coating material, heterogeneous elements such as B, N and P are used as doping materials, a carbon nanotube is used as a flexible conductive buffer material, and the materials are dispersed in a solvent to form slurry; through atomization granulation and high-temperature carbonization, heterogeneous element doped resin hard carbon is bridged with carbon nanotubes to construct a three-dimensional rigid-flexible conductive network to cooperatively coat the surface of the porous coal-based graphite, and doped heterogeneous elements are utilized to induce chemical-physical auxiliary activation to perform micro-mesoporous precise regulation and control pore forming on an inner core and a shell. The prepared novel coal-based porous carbon is high in porous framework particle strength and reasonable in pore distribution and has a three-dimensional rigid-flexible conductive network core-shell structure. The invention aims to solve the problems of unreasonable pore distribution of porous carbon, poor matrix strength and the like in the preparation process of a novel vapor deposition silicon-carbon negative electrode material.

The invention discloses a modeling and optimization control method for a gas supply system of a proton exchange membrane fuel cell, and belongs to the technical field of hydrogen energy power. The method comprises the following steps: establishing a nonlinear state space model of a proton exchange membrane fuel cell gas supply system; determining the optimal oxygen excess ratio of the system under different load currents through experiments, and fitting the optimal oxygen excess ratio into a reference function about the load currents; based on the nonlinear state space model, a model prediction control problem with tracking of the optimal oxygen excess ratio and minimization of the cathode and anode pressure difference as control targets is constructed and expressed as a constrained quadratic programming problem; and decomposing and iteratively solving the quadratic programming problem by adopting an alternating direction multiplier method to obtain the optimal control input of the current control period and act on the system. The method effectively solves the problem that traditional model predictive control is difficult to deploy in real time in a vehicle-mounted controller due to large calculated amount, so that efficient and accurate cooperative control of the proton exchange membrane fuel cell gas supply system is realized.

The invention discloses a component gradient iridium tantalum coating anode and a preparation method thereof, the component gradient iridium tantalum coating anode comprises a titanium-based bottom layer, a middle layer and a surface active layer structure with component gradient, and the middle layer and the active layer are both prepared through a thermal decomposition method. And the intermediate layer is prepared on the titanium substrate and is composed of TiO2 / Ta2O5 mixed oxide. The surface active layer is prepared on the outer side of the middle layer and comprises a plurality of layers of IrO2 / Ta2O5 oxide coatings with different iridium-tantalum proportions. Compared with a traditional uniform coating anode, the prepared component gradient iridium tantalum coating anode can relieve the stress concentration phenomenon and reduce coating cracking, the service life of the anode is remarkably prolonged, and the catalytic activity of the anode is remarkably improved; the modified carbon nano tube is added into the active layer precursor solution, so that the conductivity change caused by component gradient is improved, and the cell voltage of the component gradient iridium tantalum coating anode is effectively reduced; and moreover, the iridium content is lower, and the preparation cost of the electrode is reduced.

The invention discloses a solid-state capacitor and a preparation method thereof, and the preparation method comprises the following steps: (1) core package winding: interposing electrolytic paper between an anode foil and a cathode foil, and winding to form a core package; (2) a repairing step: immersing the core package into a formation liquid for repairing treatment; (3) a drying step: carrying out drying treatment on the core package in the step (2); (4) an impregnation step: immersing the core package in the step (3) into a first impregnation liquid for impregnation treatment; performing drying; immersing into a second impregnation liquid for impregnation treatment, and drying; (5) a polymerization step: immersing the core cladding in the step (4) into an oxidation liquid for polymerization; and (6) assembling, girdling and aging treatment.

The invention belongs to the technical field of zinc battery electrolyte, and discloses application of pyridine hydrochloride as an electrolyte additive in stabilizing a zinc negative electrode and realizing four-electron transfer of a zinc-iodine secondary battery. The hydrochloride containing the pyridine structure is used as an electrolyte additive, molecules of the pyridine structure are adsorbed on the surface of the zinc negative electrode to form a shielding layer, the deposition / stripping reversibility of the zinc negative electrode is improved, stabilization of the zinc negative electrode can be achieved, and the problems of zinc dendritic crystal, corrosion and hydrogen evolution are solved. Meanwhile, molecules with pyridine structures can activate and stabilize I- / I0 / I < + > four-electron redox reaction, inhibit I < + > hydrolysis side reaction and improve the energy density and cycling stability of the zinc-iodine battery. The problem of poor electrochemical deposition / stripping reversibility of a zinc negative electrode and the problem of poor stability of positive valence I < + > species of an iodine positive electrode of a four-electron transfer reaction are solved. The electrolyte containing the additive is low in cost, simple in method, easy to produce and high in practical value.

A LED circuit with a sequence function includes a load component, a capacitive component, a current load, and a voltage processor. The load component provides a resistance value. The capacitive component is connected to the load component in series at anode. The capacitive component provides a capacitance value, and generates an inner voltage at the node. The current load is connected in parallel to the load component and the capacitive component to provide a current path. The voltage processor receives the inner voltage and a threshold voltage, and compares the inner voltage with the threshold voltage to generate a comparison signal. The LED circuit counts time to acquire a time value from a starting time when the voltage processor starts to generate the comparison signal to a time when a level of the comparison signal changes, and uses the time value for sequencing.

The invention relates to the technical field of fuel cells, in particular to a method and system for accurately controlling the hydrogen stoichiometric ratio of a fuel cell, and the method comprises the steps: firstly, obtaining a quantitative anode health state value through a fusion calculation model by collecting load current, anode inlet and outlet pressure, temperature, high-frequency resistance and other multi-source signals in real time; a feed-forward model based on a load current change rate predicts sudden change of hydrogen demand, and an optimal hydrogen flow instruction is jointly generated in combination with output of a PID controller which adaptively adjusts parameters according to a health state value. According to the method, the integrated diagnosis parameter, namely the anode health state value, is created, so that the internal state of the fuel cell can be accurately perceived and prospectively judged. Through deep fusion of multi-source heterogeneous information such as high-frequency resistance, anode pressure difference, current and temperature, a comprehensive index capable of comprehensively and quantitatively reflecting anode water content, gas concentration and runner smoothness is generated.

In one aspect, non-invasive methods are described in which combinations of certain battery parameter values are used to identify whether metal plating (e.g., lithium plating) has occurred during charging of a battery. In response to the detection of metal plating and / or conditions associated with metal plating, one or more characteristics of a charge process may be adjusted or adapted to maintain battery parameter values within a specified range. In some cases, after detection of metal plating, a battery charge process may be adjusted or adapted to remove metal plating from a battery's anode by a discharge pulse.

Embodiments described herein relate to electrochemical cells with multiple separators, and methods of producing the same. A method of producing an electrochemical cell can include disposing an anode material onto an anode current collector, disposing a first separator on the anode material, disposing a cathode material onto a cathode current collector, disposing a second separator onto the cathode material, and disposing the first separator on the second separator to form the electrochemical cell. The anode material and / or the cathode material can be a semi-solid electrode material including an active material, a conductive material, and a volume of liquid electrolyte. In some embodiments, less than about 10% by volume of the liquid electrolyte evaporates during the forming of the electrochemical cell. In some embodiments, the method can further include wetting the first separator and / or the second separator with an electrolyte solution prior to coupling the first separator to the second separator.

The invention discloses a gas-phase silicon-carbon negative electrode material preparation system and method, and belongs to the technical field of silicon-carbon negative electrode materials. According to the preparation system disclosed by the invention, the solid raw material supply device, the fluidized bed reactor, the vapor deposition rotary furnace, the product post-processing device, the heat recycling device and the gas raw material supply system are arranged, so that the problems of small production scale, high production cost and low production efficiency of vapor deposition equipment in preparation of the vapor silicon-carbon negative electrode material are solved; and after engineering amplification of the technology, vapor deposition uniformity is reduced, a filter is frequently blocked, and high-temperature sealing is difficult to realize.

An electrode stack can include a plurality of anode assemblies, each anode assembly including at least one anode layer attached to an anode tab; a plurality of cathode assemblies, each cathode assembly including at least one cathode layer attached to a cathode tab; a plurality of separators; an anode feedthrough bridge arranged to engage each anode tab of each of the plurality of anode assemblies; a cathode feedthrough bridge arranged to engage each cathode tab of each of the plurality of cathode assemblies; an anode feedthrough terminal coupled to the anode feedthrough bridge; and a cathode feedthrough terminal coupled to the cathode feedthrough bridge, wherein the plurality of anode assemblies and the plurality of cathode assemblies are alternately arranged and separated by the plurality of separators to form an electrode stack. A battery is also presented.

The invention provides embedded metal fullerene and a preparation method thereof. The preparation method comprises the following steps: mixing a metal source and graphite powder, and filling a hollow graphite rod with the mixture to prepare an anode; the electrode is installed at the anode end of an electric arc furnace, and on-line activation is conducted through anode and cathode short-circuit current under the inert atmosphere; then carrying out arc discharge under specific air pressure and current, and collecting generated carbon ash; performing ultrasonic extraction by using an organic solvent to obtain a fullerene crude extracting solution; and finally, performing multi-stage separation and purification by high performance liquid chromatography, and performing primary and fine separation by sequentially adopting preparative and semi-preparative chromatographic columns to obtain a high-purity product. According to the method, a complete technical path capable of efficiently and controllably preparing the ultra-high-purity embedded metal fullerene is formed through a synthesis process integrating online activation and accurate atmosphere regulation and control and a multi-stage gradient chromatography purification strategy, and a solid foundation is laid for application of atomic-scale accurate materials in the frontier fields of quantum devices and the like.

The present application relates to a display panel, an electronic device and a display panel manufacturing method. The display panel includes a planarization layer, a sub-anode layer, a pixel define layer, an electroluminescent layer and a cathode layer. The sub-anode layer is configured to control light emission conditions of sub-pixels, and is above the planarization layer. The sub-anode layer has a plurality of separate sub-anodes. The sub-anode has a via hole penetrating therethrough. In the above structure, water vapor can be evaporated outwards through via holes on the sub anodes, so as to avoid the water vapor from being blocked between the planarization layer and the sub anode layer, and further avoid the situation existing in the sub anode layer in which the water vapor rises upwards and forms a protrusion and / or an opening. With the above configuration, it is beneficial to ensure the display effect of the display panel.