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560 results about "Aromatic amine" patented technology

An aromatic amine is an organic compound consisting of an aromatic ring attached to an amine. It is a broad class of compounds that encompasses anilines, but also many more complex aromatic rings and many amine substituents beyond NH₂. Such compounds occur widely.

Imine covalent organic polymer, preparation method thereof, negative electrode material and potassium ion battery

The invention provides an imine covalent organic polymer and a preparation method thereof, a negative electrode material and a potassium ion battery. The preparation method comprises the following steps: carrying out first mixing on raw materials including a carbonyl-containing first organic compound, an amino-containing second organic compound and a dispersion liquid to obtain a mixed liquid; carrying out in-situ polymerization reaction on the mixed solution to obtain an imine covalent organic polymer; wherein the first organic compound is nitro-substituted or non-substituted pyrene-4, 5, 9, 10-tetraketone; the second organic compound is selected from any one or more of C6-C12 aromatic amine compounds, C6-C12 heteroaromatic amine compounds and amino-substituted C4-C6 cyclic compounds, and the number of amino groups in each molecule of the second organic compound is greater than or equal to 2. The covalent organic polymer obtained by the preparation method can solve the problem that the structure is easily stacked and is easily dissolved in electrolyte to be damaged when the covalent organic polymer is used as a negative electrode material.
Owner:SHANGHAI XUANYI NEW ENERGY DEV CO LTD

Heat dissipation type anticorrosive paint and preparation method thereof

The invention discloses a heat dissipation type anti-corrosion coating and a preparation method thereof, and belongs to the technical field of anti-corrosion coatings. The heat dissipation type anticorrosive paint comprises a component A and a component B, wherein the component A comprises the following components in parts by mass: 100 parts of heat-conducting water-borne epoxy resin, 4-6 parts of graphene, 0.3-0.5 part of an antioxidant, 0.2-0.4 part of a defoaming agent, 0.2-0.4 part of a flatting agent and 10 parts of first deionized water; the component B comprises the following components in parts by mass: 10-20 parts of a curing agent, 40-60 parts of a toughening agent, 4-6 parts of functionalized boron nitride microspheres and 30-50 parts of second deionized water; the heat-conducting water-borne epoxy resin is 1, 5-naphthalene diphenol modified water-borne epoxy resin; the curing agent is an aromatic amine curing agent; the toughening agent is obtained by carrying out copolymerization on acrylamide, N-(4-aminophenyl) acrylamide, 1, 3, 5-triacryloyl-s-triazine and 3-dimethylamino allyl phosphoric acid; the functionalized boron nitride microspheres are boron nitride microspheres modified by 4-aminobenzoic acid.
Owner:QINGDAO AUTO RADIATOR

Organic compound, composition, electronic device, and display panel

The invention discloses an organic compound, a composition, an electronic device and a display panel. The organic compound has a structure as shown in formula (1): (1); the organic compound provided by the invention is an arylamine compound taking dibenzofuran or dibenzothiophene substituted by a heterocyclic group containing a nitrogen atom, an oxygen atom or a sulfur atom as a core structure, and can have a relatively high refractive index; when the organic compound provided by the invention is used in a covering layer of an electronic device, the refractive index of the covering layer can be effectively improved, so that the luminous efficiency of the electronic device is improved, and the electronic device with excellent performance can be realized.
Owner:GUANGZHOU CHINARAY OPTOELECTRONICS MATERIALS LTD

Process for reducing aromatic imine with neoimine reductase (IRED)

The present invention relates to a process for producing a chiral aromatic amine, said process comprising the steps of: a) providing an aromatic imine, and b) contacting said aromatic imine from step a) with an imine reductase, thereby stereoselectively reducing said aromatic imine to a chiral aromatic amine with said imine reductase; and to novel imine reductases capable of catalytic reactions.
Owner:F HOFFMANN LA ROCHE & CO AG

Waste polyurethane material recovery method and polyurethane product preparation method

The invention discloses a waste polyurethane material recovery method and a preparation method of a polyurethane product, and belongs to the technical field of waste polyurethane material recovery and reutilization. The recovery method comprises the following steps: a powder preparation stage: crushing a waste polyurethane material by using crushing equipment to obtain polyurethane powder; a premixed liquid preparation stage: mixing polyurethane powder with a degradation agent, a catalyst and a cosolvent in proportion, and uniformly mixing through stirring equipment to obtain a premixed liquid with a certain powder content; in the degradation stage, equipment with a mechanical shearing and extruding function is used for grinding, extruding and shearing the premixed liquid, the reaction process is carried out within a set temperature range, and degradation mixed liquid of the polyurethane material is obtained after the reaction is completed. In the preparation method of the polyurethane product, a part of or all of the polyol raw material adopts a degradation mixed solution. According to the method, the degradation process is low in reagent consumption, low in temperature and short in time, does not need gas protection, and does not generate toxic substances such as aromatic amine, and the obtained high-performance heterogeneous polyhydric alcohol can be directly used for preparing polyurethane products without any post-treatment process.
Owner:QINGDAO UNIV OF SCI & TECH

Arylamine compound and luminescent device

The invention belongs to the technical field of organic electroluminescence, and discloses an arylamine compound and a luminescent device. The arylamine compound has a structural general formula as shown in a formula (1) or a formula (2), wherein a ring A in the formula (1) is selected from one of formulas (1-1)-(1-4); the ring A in the formula (1) is selected from one of formulas (2-1)-(2-2); and any two adjacent * represent condensation sites of the ring A and naphthyl in the formula (1) and the formula (2). The arylamine compound provided by the invention has the advantages of low driving voltage, high luminous efficiency, long device life and the like, and can be used as a main body material in preparation of light-emitting devices.
Owner:GUANGDONG AGLAIA OPTOELECTRONICS MATERIALS

Epoxy resin vacuum infusion system and preparation method and application thereof

PendingCN120648170APolymer scienceFirming agent
The invention relates to the technical field of composite material preparation, and discloses a vacuum infusion epoxy resin system which comprises the following components in parts by weight: 50-80 parts of epoxy resin, 10-30 parts of a curing agent, 1-5 parts of an accelerant, 5-15 parts of a flexibilizer, 10-20 parts of filler, 1-3 parts of a coupling agent, 5-10 parts of a diluent, 0.1-1 part of a defoaming agent, 0.5-2 parts of an antioxidant and 0.5-2 parts of a light stabilizer. Low-temperature rapid curing is achieved through the synergistic effect of the modified aromatic amine curing agent and the accelerant, the carboxyl-terminated nitrile rubber toughening agent and the filler form a synergistic toughening system to improve the mechanical property, and the hydrogenated bisphenol A epoxy resin is matched with the light stabilizer and the antioxidant to enhance the weather resistance and the high temperature resistance. The system can be used for preparing composite materials in the fields of wind power generation blades, ships, aerospace and the like, fiber reinforced materials are infiltrated by adopting a vacuum infusion forming process and then are cured and formed, and the problems that an existing resin system is long in curing time and insufficient in mechanical property and weather resistance are solved.
Owner:MIANYANG HIGH-TECH ZONE FULIN MOULD & PLASTIC PROD CO LTD

Sulfonic acid-functionalized covalent organic frameworks / nafion proton exchange materials, methods of making, and uses thereof

The application discloses a kind of sulfonic acid group covalent organic framework / Nafion composite material for proton conduction and preparation method and application thereof, belong to fuel cell technical field.The application first utilizes double sulfonic acid group organic aromatic amine ligand and aldehyde group ligand to construct a kind of sulfonic acid functional two-dimensional covalent organic framework material COF-(SO3H)2 by condensation reaction.COF-(SO3H)2 is compounded with Nafion polymer to prepare proton exchange membrane, and the proton exchange membrane material has excellent proton conduction, and the proton conductivity is 1.338*10 ‑1 S·cm ‑1 (80ºC).The proton exchange membrane material of the application is prepared by solvothermal process and casting method, and the preparation method is simple and easy to operate, which provides a new choice for proton conduction material in fuel cell, and expands the application value of covalent organic framework material.
Owner:ZHONGYUAN ENGINEERING COLLEGE

Preparation method of melatonin and mehedroline indole derivative and compound

The invention belongs to the field of organic synthetic chemistry, and relates to a preparation method of melatonin and meerythrine indole derivatives and compounds. Specifically, the indole derivative is efficiently synthesized by taking arylamine and carboxylic acid as raw materials through a one-pot two-step reaction in the presence of catalysis of ferric chloride hexahydrate (FeCl3. 6H2O), a ligand, a diazotization reagent, an additive and a solvent under the conditions of visible light irradiation, inert atmosphere and room temperature. According to the method, visible light induced iron-based LMCT catalysis and iron lewis acid catalysis functions are integrated, and efficient integration of diazotization, decarboxylation, free radical coupling and cyclization reaction is achieved. The method has the advantages that raw materials are cheap and easy to obtain, reaction conditions are mild, substrate applicability is wide, functional group compatibility is good, operation is easy, convenient and safe, and environment friendliness is achieved, gram-level scale preparation can be achieved, and a green and efficient synthesis path is provided for indole compounds with biological activity such as melatonin and meerythrine.
Owner:DALIAN UNIV OF TECH

An aromatic organic compound and an organic electroluminescent device comprising the same.

This invention relates to an aromatic amine organic compound and an organic electroluminescent device containing the same, belonging to the field of semiconductor materials technology. The structure of the compound provided by this invention is shown in general formula (1): When the hole transport material or electron blocking layer material of the organic electroluminescent device is prepared by using the aromatic amine compound of this invention, the device voltage can be reduced and the device life can be extended at the same time, especially the device high temperature life is significantly improved.
Owner:JIANGSU SUNERA TECH CO LTD

Liquid spray head and one-component adhesive

To provide a liquid spray head that has a low environmental impact, is acid-resistant, and is highly reliable. [Solution] A liquid spray head that sprays liquid from a nozzle comprises a first member, a second member, and a cured product of a one-component adhesive that adheres the first member and the second member, wherein the one-component adhesive comprises a bisphenol-free epoxy resin, a curing agent containing an aromatic amine polymer, and an alkylphenol, wherein the alkylphenol is (a) an alkylphenol having at least one ethyl group, or (b) an alkylphenol having 1 to 3 carbon atoms in the alkyl group and at least one methyl group and one isopropyl group.
Owner:SEIKO EPSON CORP

An organic electron acceptor containing a carbazole side chain and its application

The present invention discloses an organic electron acceptor containing a carbazole side chain and its application in solar cells. The organic electron acceptor containing a carbazole side chain has a structure shown in the following formula: #imgabs0# wherein R1 and R2 are independently a linear or branched alkyl group containing 1-18 carbon atoms, and A is an electron-withdrawing functional group. The present invention uses a non-fully fused ring structure based on trithiophene as the central conjugated skeleton of the organic electron acceptor, introduces a carbazole group as a side chain, prevents excessive elevation of the molecular HOMO energy level, and inhibits the internal rotation between the trithiophene rings connected by single bonds through its rigid large steric effect, thereby ensuring the planarity of the acceptor molecule, regulating the stacking between molecules, and simultaneously inhibiting the aromatic amine group from inducing the molecular skeleton to form a quinone structure, thereby improving the molecule's resistance to photooxidation.
Owner:ZHEJIANG UNIV

Active aldehyde substance inhibitor based on AI design and application thereof

The invention discloses an active aldehyde substance inhibitor based on AI design and application thereof. The inhibitor comprises a compound represented by a general formula (I) or a derivative thereof, wherein the definitions of all groups are described in the specification. The method is based on an autonomously built AI technical platform, the alkalinity of aromatic amine, imine reaction transition state activation energy delta G and chemical reaction enthalpy change delta H are calculated and predicted, then wet experiments are combined for repeated iterative optimization, and finally the compound or the derivative of the compound is obtained. The compounds or the derivatives of the compounds can efficiently capture active aldehyde substances (RASP, reactive aldehyde substances), and can be used as active aldehyde substance capture agents for treating and / or preventing various diseases caused by the active aldehyde substances.
Owner:SHENZHEN NEWROSETTA BIOSCIENCES CO LTD

Insulation sealing coating adhesive

The embodiment of the invention relates to the technical field of insulating adhesives, and discloses an insulating sealing coating adhesive which comprises 60-80 parts of a modified styrene-butadiene-styrene block copolymer, 0.3-1 part of a ketimine curing agent, 2-8 parts of an aromatic amine curing agent, 3-8 parts of methyl silicone oil and 12-26 parts of petroleum ether, wherein the modified styrene-butadiene-styrene block copolymer is obtained by epoxidation of a styrene-butadiene-styrene block copolymer (SBS), the molecular weight of the styrene-butadiene-styrene block copolymer is 7000-11000, the substance amount fraction of a PB end (polybutadiene chain segment) is 70-85%, and the ratio of a branched chain structure to a straight chain structure in the PB end is 1: 2-1: 3. The insulation sealing coating adhesive has the characteristics of high reliability and uniform coating in multiple axial directions, especially in the vertical direction (namely the z-axis direction) through the structural characteristics of the insulation sealing coating adhesive and the compounding of the insulation sealing coating adhesive and a multi-element curing agent, is convenient to spray and is beneficial to application to precise components.
Owner:JOINTRUST MATERIALS (HUIZHOU) CO LTD

Liquid spray head and two-part adhesive

To provide a liquid spray head having a cured adhesive product that has a low environmental impact, is fast-curing, and acid-resistant. [Solution] The liquid spray head is a liquid spray head that sprays liquid from a nozzle and comprises a first member, a second member, and a cured product of a two-component mixed adhesive that adheres the first member and the second member. The two-component mixed adhesive comprises liquid A, which contains a main component including an epoxy resin that does not contain bisphenol; liquid B, which contains at least one of 2,5-bis(aminomethyl)bicyclo[2.2.1]heptane and 2,6-bis(aminomethyl)bicyclo[2.2.1]heptane and an alkylphenol; and a polymer of an aromatic amine contained in liquid A or liquid B. The alkylphenol is (a) an alkylphenol having at least one ethyl group, or (b) an alkylphenol having 1 to 3 carbon atoms in the alkyl group and at least one methyl group and one isopropyl group.
Owner:SEIKO EPSON CORP

Nonmetal antiknock agent as well as preparation method and application thereof

The invention relates to the technical field of fuel additives, in particular to a non-metal antiknock agent and a preparation method and application thereof, aims to provide the non-metal antiknock agent and the preparation method and application thereof, and solves the core problem that a traditional non-metal antiknock agent is low in efficiency. In order to solve the technical problems, the technical scheme adopted by the invention is as follows: the non-metal antiknock agent comprises the following components in percentage by mass: 55-75% of straight-chain or branched-chain fatty amine, 10-25% of aromatic amine, 5-15% of polysubstituted fatty amine and 5-15% of an electron donor, the electron donor adopts a hydrated electron base solution. The gasoline antiknock agent is environment-friendly and efficient, does not depend on a noble metal catalyst, does not need high temperature and high pressure, not only has the excellent effect of a metal antiknock agent, but also is pollution-free, and can greatly improve the gasoline quality under the condition of extremely low addition amount.
Owner:AMO (NANJING) ENVIRONMENTAL PROTECTION TECHNOLOGY CO LTD

Vehicle composition for inorganic fine particle dispersion, inorganic fine particle-dispersed slurry composition and method for producing inorganic fine particle-dispersed sheet

The present invention aims to provide a vehicle composition for inorganic fine particle dispersion which has excellent decomposability at low temperature and enables degreasing in a short time, an inorganic fine particle-dispersed slurry composition containing the vehicle composition for inorganic fine particle dispersion, and a method for producing an inorganic fine particle-dispersed sheet with the inorganic fine particle-dispersed slurry composition. The present invention relates to a vehicle composition for inorganic fine particle dispersion, containing a binder resin, an organic solvent, and an organic compound having a boiling point at normal pressure of 200° C. or higher and lower than 400° C., the binder resin containing a (meth)acrylic resin, the organic compound containing at least one selected from a phenol compound, an aromatic amine compound, a quinone compound, and a nitro compound, the amount of the organic compound being 1 to 100 parts by weight relative to 100 parts by weight of the binder resin.
Owner:SEKISUI CHEMICAL CO LTD

Biphenyl dinaphthalene substituted arylamine compound and application thereof

The invention relates to the technical field of organic light-emitting display, in particular to a biphenyl-naphthalene substituted arylamine compound and application, and provides a compound shown in a formula (I) which can be used for hole transport materials. The compound has a parent structure of biphenyl and naphthalene substituted arylamine, is high in bond energy between atoms, has good thermal stability, is beneficial to solid-state accumulation between molecules, is high in hole transition capability, and can effectively reduce the voltage of a device and prolong the service life of the material when being used as a hole transport material. The invention also provides an organic electroluminescent device and a display device containing the compound shown in the formula (I).
Owner:YANTAI XIANHUA CHEM TECH CO LTD +1

Polyamide-based products

Compositions and products formed thereof are based on glass fiber-reinforced polyamide admixed with at least one secondary aromatic amine, at least one phosphinic acid derivative and bis(2,4-di-t-butylphenyl)pentaerythritol diphosphate in amounts to improve ageing behavior in the form of improved preservation of the elongation at break and impact toughness, improved color preservation or improved color stability, and simultaneously improved UV stability after thermal ageing by comparison with products based on glass fiber-reinforced polyamide with such a mixture.
Owner:ENVALIOR DEUTSCHLAND GMBH

Aromatic amine epoxy resin curing agent, its design method and insulating epoxy resin and its preparation method

The application discloses a kind of aromatic amine epoxy resin curing agent and its design method and insulating epoxy resin and its preparation method, belong to insulating technical field.At least two benzene ring structures are designed, and the benzene ring structures are connected by functional bridge bond;An amino functional group is respectively arranged at the two ends of the designed structure;High electron-withdrawing substituent group is not arranged at the ortho position of the designed amino functional group;Get aromatic amine epoxy resin curing agent;Functional bridge bond is arranged at the 1,4 or 1,3 substitution site of benzene ring structure.Multiple aromatic diamines are used as the curing agent component of epoxy resin, rigid aromatic structure is introduced into the epoxy main chain to enhance its thermal stability and improve the glass transition temperature;Functional bridge bond is introduced between benzene rings as breaking benzene ring conjugated structure, to improve electrical performance.Can prepare high-temperature stability and high-resistance high-voltage direct-current insulating epoxy resin.Help to solve the electrical performance of key insulating parts in DC GIS / GIL under the action of high temperature gradient and high electric field.
Owner:XI AN JIAOTONG UNIV

Environment-friendly biodegradable lubricating oil for hydraulic retarder and preparation method of environment-friendly biodegradable lubricating oil

The invention belongs to the technical field of lubricating oil, and particularly relates to environment-friendly biodegradable lubricating oil for a hydraulic retarder and a preparation method of the environment-friendly biodegradable lubricating oil. The environment-friendly biodegradable lubricating oil for the hydraulic retarder is prepared from the following components in parts by mass: 80 to 90 parts of base oil, 1 to 3 parts of a cleaning agent, 1 to 3 parts of a dispersing agent, 1 to 2 parts of a viscosity index improver, 0.5 to 2 parts of an anti-wear agent, 0.3 to 1.5 parts of an antioxidant, 0.1 to 0.5 part of an anti-foaming agent and 0.1 to 0.3 part of a pour point depressant, the antioxidant comprises hindered phenolic ester, aromatic amine and zinc thiophosphate in a mass ratio of (3-6): (2-5): 1. The environment-friendly biodegradable lubricating oil for the hydraulic retarder, provided by the invention, is biodegradable, and has excellent high-temperature resistance, oxidation resistance and low-temperature resistance and longer oil change period.
Owner:JINFENG HONGRUN TECH (GUANGDONG) CO LTD

Light-emitting element

ActiveDE112012007388B4CarbazoleHost material
Light-emitting element comprising: a first electrode (103); a light-emitting layer (703) over the first electrode (103), the light-emitting layer (703) comprising a guest material and a host material; and a second electrode (108) above the light-emitting layer (703), where the maximum of the emission spectrum of the host material overlaps the absorption band at the longest wavelength side (the side of lowest energy) in the absorption spectrum of the guest material, wherein the difference between the energy value of the maximum of the emission spectrum of the host material and the energy value of the maximum of the absorption band on the lowest energy side in the absorption spectrum of the guest material, said maximum having an absorption wavelength corresponding to a direct transition from the singlet ground state to the lowest excited triplet state of the guest material, is 0.2 eV or less, wherein the maximum of the absorption wavelength of the absorption band on the longest wavelength side lies in a range from 490 nm to 530 nm, and wherein the host material is a material mixture of a heterocyclic compound and an aromatic amine compound or carbazole compound.
Owner:SEMICON ENERGY LAB CO LTD

Solvents for container application of oilfield products

PendingUS20250333638A1Cleaning apparatusDrilling compositionOrganic sulphur compoundCellulose
A water-soluble container including a treatment chemical is provided. The treatment chemical may be, for example, an organic sulfur compound, an imidazoline, a carboxylic acid, a fatty acid amine condensate, a substituted fatty acid ester, a substituted aromatic amine, a phosphoric acid ester, a quaternary ammonium compound, a compound having multiple positive charges, or any combination of these chemicals. The water-soluble container may include, for example, cellulose, polyvinyl alcohol, gelatin, or any combination of these materials.
Owner:CHAMPIONX LLC

Composite cleaning agent for automobile paint surface maintenance based on nano dry cleaning technology and preparation method of composite cleaning agent

The invention discloses a composite cleaning agent for automobile paint maintenance based on a nanometer dry cleaning technology and a preparation method thereof, and belongs to automobile cleaning supplies. The composite cleaning agent comprises 8-12% of nano oxide, 15-22% of a surfactant, 12-18% of a natural maintenance component, 10-15% of a functional additive and the balance of a solvent carrier. According to the principle, nano silicon dioxide forms a three-dimensional network structure through a sol-gel method, and forms a compact hydrophobic layer on the paint surface under the synergistic effect of the nano silicon dioxide and polyhydroxy arylamine modified silicone oil. Quaternary ammonium salt groups in the modified silicone oil and metal ions on the paint surface generate electrostatic interaction, and the wiping force is reduced by 60% in cooperation with the ball effect of the nano silicon dioxide. The citric acid and the tea saponin form a composite chelating agent, the removal rate of inorganic stains such as rust and bird droppings reaches 98%, and meanwhile corrosion to aluminum parts is avoided.
Owner:CHEMEIJIE (BEIJING) TECHNOLOGY CO LTD

High-temperature-resistant water-based polyimide sizing agent for carbon fibers, modified carbon fibers, resin-based composite material of modified carbon fibers, preparation method and application of resin-based composite material

The invention discloses a high-temperature-resistant water-based polyimide sizing agent for carbon fibers, modified carbon fibers, a resin-based composite material of the modified carbon fibers, a preparation method and application of the resin-based composite material, and belongs to the technical field of advanced composite materials. The sizing agent disclosed by the invention is prepared by carrying out condensation polymerization on aromatic dianhydride and monofunctional aromatic amine to generate polyamide acid and then carrying out an ionizing salt formation process. The sizing agent has excellent storage stability and thermal stability, can effectively improve the wettability of the carbon fiber surface, and significantly improves the interface bonding performance of the carbon fiber reinforced polyimide composite material. The sizing agent provided by the invention can remarkably improve the room-temperature and high-temperature interface bonding strength of the carbon fiber reinforced polyimide composite material, and is suitable for the fields of aerospace, high-end equipment manufacturing and the like.
Owner:SICHUAN UNIV

Preparation method of 9-aryl xanthene compound

The invention relates to the technical field of organic synthesis, in particular to a preparation method of a 9-aryl xanthene compound. The preparation method of the 9-aryl xanthene compound comprises the following steps: adding a xanthene compound, an aromatic amine compound and a nitrogen-doped carbon material into an organic solvent, and reacting in an oxygen atmosphere; the 9-aryl xanthene compound is novel in structure and can be applied to the fields of medicines, agricultural chemicals, material science and the like, and the preparation method has the advantages of mild reaction conditions, simplicity and safety in operation, high raw material economy, wide substrate applicability and functional group compatibility, good chemical and regioselectivity and the like; a new way is provided for the construction of a novel xanthene derivative.
Owner:YANCHENG INST OF TECH

Synthesis method and reaction system of arylamine compound

The application discloses a synthesis method and a reaction system of an aromatic amine compound. The synthesis method of the aromatic amine ionic compound comprises the following steps: in a continuous flow reactor, carrying out a nucleophilic substitution reaction on water, an ionic compound A and a nitrogen source Y to obtain the aromatic amine ionic compound. The preparation method has the characteristics of short reaction time, simple and safe operation and no amplification effect.
Owner:SHANGHAI SYNTHEALL PHARM CO LTD +2

Preparation method and application of diselenide arylamine compound

The invention discloses a preparation method and application of a double-selenium arylamine compound. The preparation method comprises the following steps: mixing a compound shown as a formula I, a compound shown as a formula II, a copper catalyst, an oxidizing agent and a solvent for reaction to obtain a compound shown as a formula III. The bis-selenium arylamine compound is prepared from the compound shown in the formula I and the compound shown in the formula II as raw materials through a one-step method, synthesis steps are simple, the raw materials are non-toxic, low in price and easy to obtain, and the synthesis method has the advantages of being good in functional group compatibility, high in atom economy and high in yield.
Owner:WUYI UNIV

Super-hydrophobic coating and preparation method thereof

The invention belongs to the technical field of functional coatings, and particularly relates to a super-hydrophobic coating and a preparation method thereof. The preparation method comprises the following steps: pretreating a base material, placing the base material in an aqueous solution containing a zinc source and at least one electroplating additive, and carrying out electro-deposition to form a zinc coating on the surface of the base material; electroplating it in a first solution comprising a zinc source and an electrolyte salt; transferring into a second solution containing zinc source and alkali source precursors, and growing on the zinc plating layer by a hydrothermal method to form a ZnO nano-structure array layer; the preparation method comprises the following steps: reacting a trifluoromethyl-containing acylating agent with a hydrazine compound in an organic solvent, adding phenolic hydroxyl-containing aromatic amine or a salt thereof and alkali, and reacting under a reflux condition to obtain a fluorine-containing organic ligand; sequentially putting the zeolite imidazate framework material into a first organic solvent containing a zinc source and a second organic solvent containing a fluorine-containing organic ligand and imidazole or a derivative thereof to react, and enabling the fluorine-containing zeolite imidazate framework material to grow on the surface in situ to obtain the super-hydrophobic coating.
Owner:YUNNAN POWER GRID CO LTD ELECTRIC POWER RES INST