The invention relates to pet cat litter and its preparation method, which comprises preparing organic base-material 20- 60%, clay 30-80%, binder 0-10%, water absorber 0-20%, surface adsorption substance0- 5%, crushing organic base-material to 30 screen mesh bulkload, processing clay to powder finer than 200 screen mesh, picking organic base material and clay proportionally to making cat litter base body, mixing and stirring the remaining material to making mixed covering material, placing cat litter base body in high-velocity rotating vibration machine, rotating making hydrosphere seeping to the surface of base body, then adding mixed covering material, vibrating slightly for mixing, then sifting and drying, sifting out powder. The inventive cat litter has good deodorant effect, good conglobation property after using, and waste cat litter can combust in favor of environment protection.