2271 results about "Ionic liquid" patented technology

The invention relates to the technical field of fibers, and discloses an antistatic warm-keeping fiber and a preparation method thereof. The preparation method comprises the following steps: carrying out graft modification on a far infrared material graphene oxide through functionalized POSS, introducing the modified graphene oxide and an ionic liquid into polypropylene, carrying out melt grafting to prepare an antistatic polypropylene master batch, introducing the master batch into polypropylene slices for spinning, and carrying out a synergistic antistatic effect of an inorganic antistatic agent graphene and an organic antistatic agent ionic liquid to prepare a composite material. The prepared fiber has antistatic performance and far infrared heating performance, and meanwhile, the POSS structure with excellent thermal stability is introduced, so that the heat resistance of the fiber is further improved.

The invention relates to a foam material, in particular to a polyimide / ionic liquid composite foam material and a preparation method thereof. The polyimide (PI) polymer with a rigid molecular structure and high temperature resistance is successfully synthesized, meanwhile, high-compatibility ionic liquid (ILs) molecules are introduced into adjacent PI molecular chains, the polyimide / ionic liquid composite foam material is formed through supercritical foaming, the foaming capacity is remarkably improved, and the polyimide / ionic liquid composite foam material has excellent performance.

The invention discloses an electrolytic adhesive, an electrolytic cotton adhesive tape and a preparation method of the electrolytic adhesive. The electrolytic cotton adhesive tape comprises the following components in parts by weight: 5-10 parts of 1, 1 '-ferrocene diformyl chloride, 10-15 parts of acrylic acid beta-cyclodextrin ester, 3-8 parts of polyethylene glycol diglycidyl ether, 10-20 parts of ionic liquid, 1.5-3 parts of a cross-linking agent, 10-15 parts of tackifying resin and 0.5-1.5 parts of an initiator, and a polymer matrix comprises an acrylic acid-hydroxypropyl acrylate copolymer and acrylic acid-2-ethylhexyl ester. Comprising an adhesive layer and an adhesive tape base layer, the adhesive layer is prepared from the electrolytic adhesive, and the adhesive tape base layer is prepared from acrylic foam; the obtained electrolytic cotton adhesive tape has high initial adhesion and viscosity strength after power-on and power-off re-adhesion.

The invention belongs to the technical field of batteries, and particularly relates to a negative electrode material, a secondary battery and electric equipment. The second coating layer with the porous carbon material in the negative electrode material provides a sufficient buffer space for volume expansion of silicon, so that cracks and pulverization of the negative electrode material are effectively reduced, and the structural integrity of the negative electrode material is further ensured. And meanwhile, the solid electrolyte arranged in the second coating layer can maintain the smoothness of an ion transmission path in the silicon expansion process, so that the rate capability and the quick charge performance of the battery are ensured. Besides, a third coating layer (SEI film) formed by the ionic liquid has good ionic conductivity, and dynamic covalent bonds existing in some ionic liquids can be fractured and recombined under the action of external stress, so that a self-repairing function is realized. Therefore, when cracks are generated on the surface of the negative electrode material due to volume expansion, the third coating layer can quickly repair the cracks, prevent electrolyte permeation and lithium dendrite growth and inhibit side reactions.

Disclosed are an ionic liquid-based perfluorinated high-voltage-resistant lithium battery electrolyte and a preparation method therefor. The high-voltage-resistant electrolyte is composed of an imidazolyl ionic liquid, a lithium salt, and an electrolyte additive. The ionic liquid-based electrolyte has relatively reversible and stable lithium stripping / deposition performance, exhibits good compatibility with a lithium metal / graphite negative electrode, and can also form a highly fluorinated stable electrode-electrolyte interface (CEI / SEI layer), thus improving the compatibility of the ionic liquid electrolyte with a high-voltage lithium cobaltate positive electrode, and effectively inhibiting dendrite formation and oxidation dissolution of the electrolyte, thereby achieving extremely high cycle stability and Coulombic efficiency of a lithium battery under high voltage conditions.

The invention provides a perovskite absorption layer and a preparation method thereof, and a polyion liquid-ion liquid synergistically modified perovskite solar cell, belongs to the technical field of solar cells, and aims to solve the problems of bulk phase and interface defects of the perovskite solar cell. The preparation method of the perovskite absorption layer comprises the following steps: dispersing and dissolving a perovskite precursor, polyionic liquid and ionic liquid into an organic solvent to prepare a perovskite precursor solution; and spin-coating the perovskite precursor solution to form a film, and annealing to obtain the perovskite absorption layer. According to the invention, polyionic liquid (PIL) and ionic liquid (IL) are preferably and synergistically added into a single-junction or multi-junction photovoltaic cell containing perovskite junctions, so that dual passivation of bulk phase and interface defects is realized; and the film uniformity and the photoelectric efficiency are improved.

The invention relates to the technical field of molecular simulation, and discloses a molecular simulation analysis method of a functionalized covalent organic framework confinement ionic liquid microstructure, and the method specifically comprises the following steps: converting force field files of COF and anions and cations of ionic liquid into coordinate files by using a Python tool; the anions and the cations are confined to a pore channel formed by COF stacking to form a composite membrane, and the whole system is placed in a simulation box; data and input files are generated according to the potential file, and LAMMPS software is used for conducting molecular dynamics simulation on a set simulation box; the two-dimensional density, cation orientation and the like of the ionic liquid are analyzed through a Python post-treatment molecular dynamics track, and meanwhile the porosity and the free volume of the COF are calculated. According to the method, a regulation and control mechanism of the COF confinement ionic liquid can be obtained, and a theoretical basis is provided for design and preparation of a COF confinement ionic liquid membrane material.

The invention discloses a copper wire tinning method for tinned copper stranded wire production, which relates to the technical field of metal surface treatment, and comprises the following steps: releasing a copper wire to an ionic liquid electrophoresis tank, applying an electric field to strip surface oxides, and then carrying out three-stage countercurrent rinsing to generate a clean copper wire; putting the clean copper wire into a composite plating tank, monitoring the tin liquid viscosity and the copper wire linear speed in real time, calculating the magnetic field gradient, and controlling tin crystal oriented growth according to the magnetic field gradient to generate an oriented crystallization tinned copper wire; the surface temperature of the directionally crystallized tinned copper wire is monitored in real time and compared with a preset temperature threshold value, a temperature permission trigger signal is generated, the annular array spray gun is triggered to work according to the temperature permission trigger signal, and a densified tinned copper wire is generated; and the densified tinned copper wire is scanned through a micro-focus CT scanner, a gap three-dimensional point cloud picture is generated, the gap size and the normal angle of the gap three-dimensional point cloud picture are analyzed, the optimal spraying parameters are recognized, and the passivation film tinned copper wire is generated.

The application discloses a kind of full-color organic ion gel based on anion-induced phase separation strategy of high ionic conductivity, stretchability and long phosphorescence lifetime and application thereof, which comprises: introducing anions in a polymer ion solution containing a large number of hydroxyl groups, inducing molecular chain rearrangement by freeze-thaw and low-temperature drying, and constructing an ion liquid enrichment zone and a polymer enrichment zone, wherein the highly solvated ion liquid enrichment zone is a soft phase, which bears elastic deformation and ion transport function, and the polymer enrichment zone is a hard phase, which bears mechanical load and induces phosphorescence emission.The application solves the problems of poor mechanical properties, non-stretchability and short phosphorescence lifetime of existing phosphorescent materials, and synergistically improves the mechanical properties and phosphorescent properties of ion gel.The prepared ion gel has excellent environmental tolerance, recyclability and responsiveness;using its multicolor phosphorescent display and responsive electrical signals, it can be used to construct soft robots and information encryption devices with dual-channel information interaction.

The invention relates to the field of preparation of lubricating materials, in particular to a preparation method of composite phase change lubricating gel based on temperature-friction force synergistic response. The lubricating gel adopts a sandwich layered structure; the bottom layer is a porous ceramic layer formed by micro-arc oxidation, is filled with a disulfide bond dynamic network polymer and is anchored on a metal substrate; the middle layer comprises a microencapsulated phase change material which is dispersed in a polyurethane network containing dynamic disulfide bonds and is wetted with ionic liquid; the surface layer is an epoxy resin coating rich in boron nitride nanosheets, and a rapid heat conduction channel is constructed. Compared with the prior art, the lubricating state can be automatically adjusted in the friction process without external energy input, and the method has the advantages of being sensitive in multi-field coupling response, capable of achieving automatic antifriction protection, high in extreme working condition adaptability and the like.

The invention provides a phosphorus-based ionic liquid flame-retardant polymer solid electrolyte and a preparation method and application thereof, belongs to the technical field of polymer solid electrolyte materials, and relates to a phosphorus-containing group flame-retardant ionic liquid polymer electrolyte and a preparation method thereof. The invention aims to overcome the problems that the polymer electrolyte in the prior art is poor in safety and the battery performance needs to be further improved, and provides the ionic liquid polymer electrolyte with the flame-retardant characteristic, the polymer electrolyte can greatly improve the safety performance of the battery while improving the battery performance, and the service life of the battery is prolonged. The phosphate group-containing ionic liquid has the advantages that the phosphate group-containing ionic liquid can be used as a polymer matrix of a polymer solid electrolyte, so that enough mechanical strength is ensured, phosphate radicals play a flame-retardant effect in a reaction process, a combustion reaction can be interrupted, and the safety performance of a battery can be greatly improved while the performance of the battery is improved.

The invention discloses a compound environment-friendly corrosion inhibitor as well as a preparation method and application thereof. The choline ionic liquid comprises choline ionic liquid and amino acid, the choline ionic liquid is choline cations; the amino acid is one or more of cysteine and tryptophan. The compound environment-friendly corrosion inhibitor has high corrosion inhibition efficiency, and the compound structure of the compound environment-friendly corrosion inhibitor further improves the protection performance of the compound environment-friendly corrosion inhibitor through a dual adsorption mechanism of the synergistic effect of physical adsorption and chemical adsorption on the metal surface. According to the compound environment-friendly corrosion inhibitor, a full-green ionic liquid corrosion inhibition system is constructed, the environment-friendly requirement is met, and a metal protection solution can be provided for industrial acid pickling and other strong acid working conditions. Not only is the progress of a corrosion inhibition technology promoted, but also more economic and environment-friendly anti-corrosion application can be provided for actual industrial scenes.

The invention discloses an application of an ionic liquid in extraction of trioxymethylene, in the process of generating trioxymethylene by acid-catalyzed condensation of a formaldehyde aqueous solution, the ionic liquid is added as an extraction agent to extract and separate the trioxymethylene generated by reaction, and the ionic liquid is methyl tributyl phosphonium bis (trifluoromethanesulfonyl) imide salt; when the ionic liquid is used for extracting trioxymethylene, a ternary azeotropic system of trioxymethylene, water and methylene glycol can be broken, the ionic liquid and trioxymethylene are subjected to nonpolar Van der Waals' force interaction so as to realize extraction, and methylene glycol and water are left in a water phase through hydrogen-bond interaction, so that high-purity trioxymethylene with the purity of more than or equal to 99.5 wt.% is obtained.

The invention discloses a method for recovering rare earth and valuable metal from waste rare earth alloy by using ionic liquid, and belongs to the technical field of non-ferrous metal metallurgy. Comprising the following steps that (1) recycled waste rare earth alloy is smashed, and waste rare earth alloy powder is obtained; (2) the waste rare earth alloy powder is put into ionic liquid to be subjected to a leaching reaction, solid-liquid separation is conducted after leaching is completed, and solid rare earth salt and filtrate are obtained; and (3) the filtrate serves as electrolyte, an electrolytic deposition system is constructed for electrodeposition, and valuable metal is obtained. The recovery method also has the advantages of simple process, environmental friendliness, high purity of the regenerated electrolyte and stable performance, and has great popularization and application prospects.

The application discloses a kind of full solid-state battery and its preparation method and application, it is related to solid-state battery technical field.The edge of positive active layer is attached with solidified insulating glue, so as to use the solidified insulating glue to fill the size difference between the positive active layer and the negative active layer, and the end of the positive active layer and the negative active layer is flush, the insulating glue plays a supporting role under extrusion, avoids the problems such as collapse and short circuit caused by the size difference between the positive active layer and the negative active layer;The insulating glue at the edge can be bonded with the negative electrode under high pressure, and when the positive electrode is charged and discharged, the cycle performance difference caused by the volume change of the positive electrode during charging and discharging can be effectively alleviated, and the cycle of the battery is improved;It can also effectively avoid the occurrence of problems such as the edge of the positive electrode dropping material.By setting electrolyte film between the positive active layer and the negative active layer, the impedance between the electrolyte film and the electrode sheet is reduced by using the ionic liquid treatment layer on the electrolyte film, and the battery performance is improved.

The invention relates to the technical field of adhesives, and discloses an imidazolium ionic liquid and a preparation method and application thereof, the preparation method comprises the following steps: reacting omega-bromoalcohol with 1-(methoxymethyl) imidazole in acetonitrile, and washing with methyl tert-butyl ether to obtain a target ionic liquid precursor; and dissolving the product in acetonitrile, adding 4-trifluoromethyl phenyl isocyanate, and washing with methyl tert-butyl ether after the reaction is finished, thereby obtaining the target imidazolium ionic liquid. The imidazolium ionic liquid disclosed by the invention is applied to a PVB (Polyvinyl Butyral) adhesive, and the PVB adhesive shows excellent adhesion strength in a macroscopic adhesion performance test on the basis of multiple interactions, and particularly has excellent adhesion strength on aluminum. The obtained adhesive can be universally adapted to various substrates such as metal substrates and macromolecule substrates, and finally high-strength and high-durability intelligent adhesion performance is achieved.

According to the cell fixing liquid, phenol oxidase is used for catalyzing phenol to be oxidized into a quinone structure, the quinone structure reacts with protein amido to form light covalent immobilization, cell immobilization is achieved, a stable hydration environment and membrane protection are provided through the ionic liquid solvent choline dihydrogen phosphate, a phosphate-free buffer system is provided, and cell immobilization is achieved. Therefore, a novel cell fixing liquid is obtained, the cell structure integrity required by cell imaging analysis is effectively reserved, meanwhile, cell staining fluorescence signal interference is avoided, and therefore the accuracy of cell counting and cell imaging analysis is ensured.

The invention belongs to the technical field of conductive microsphere preparation, and particularly relates to a preparation method and application of conductive microspheres with convex particles on the surfaces. The preparation method comprises the following steps: acidizing resin microspheres by using imidazole disulfate ionic liquid, and combining the acidized resin microspheres with aminated activated carbon through chemical bonds to obtain microspheres with convex particles on the surfaces; and sequentially carrying out stannous chloride sensitization, palladium chloride activation and chemical nickel plating on the microspheres with the convex particles on the surfaces to obtain the conductive microspheres with the convex particles on the surfaces. The conductive microspheres with the raised particles on the surfaces can generate more and more effective local contact points in the crimping process, so that the connection resistance is obviously reduced, and the excellent conductive performance is realized.

The invention discloses conductive lubricating grease and a preparation method thereof, and belongs to the technical field of lubricating grease materials, the conductive lubricating grease comprises the following components by mass: 50-80 parts of base oil, 5-15 parts of a thickening agent, 3-10 parts of an additive, 5-20 parts of an oil soluble ionic liquid, and 1-10 parts of nanoscale conductive solid particles; the oil-soluble ionic liquid is prepared from trioctylamine, bromohexadecane and sodium di-tert-butyl phosphate. According to the conductive lubricating grease provided by the invention, the oil-soluble ionic liquid and the nanoscale conductive solid particles synergistically conduct electricity, so that the conductive lubricating grease has a tunnel conductive effect and excellent conductivity; besides, due to synergistic conduction of the oil-soluble ionic liquid and the nanoscale conductive solid particles, the addition amount of the conductive solid particles can be reduced, the anti-attrition effect of the conductive lubricating grease is further improved, meanwhile, the nanoscale conductive solid particles have a good anti-attrition effect, the solid size and the oil film thickness are both in nanoscale sizes, and the conductive lubricating grease has a good anti-attrition effect. Therefore, the conductive lubricating grease is excellent in overall anti-wear effect.

The invention discloses a polymer solid electrolyte, which is composed of the following components: a polymer substrate; a lithium salt; the composite filler is IL (at) ZIF-67 formed by compounding ZIF-67 and an ionic liquid; and a solvent. The ionic liquid is used as a plasticizer, and the EmimTFSI can effectively weaken the intermolecular acting force between polymer chains and increase the free volume and movement ability of the polymer chains. ZIF-67 has abundant Lewis acid sites (Co < + >), and the sites can form weak coordination with LiTFSI, so that the ionic conductivity is further improved. The introduction of the composite filler is beneficial to improving the interface stability of the polymer electrolyte and the lithium metal negative electrode and inhibiting the growth of lithium dendrites, so that the cycle life of the battery is prolonged. The polymer solid electrolyte membrane prepared on the basis of the preparation method is applied to a solid-state lithium-sulfur battery, and the cycling stability, the rate capability and the coulombic efficiency of the battery can be remarkably improved.

The invention provides a bionic ionic gel humidity sensing material as well as a preparation method and application thereof. The bionic ionic gel humidity sensing material is prepared from the following raw materials in parts by mass: 50 to 55 parts of acrylic acid, 20 to 25 parts of acrylamide and 20 to 25 parts of conductive ionic liquid, the coating also comprises a cross-linking agent and a photoinitiator; wherein the dosage of the cross-linking agent is 0.1 wt%-1wt% of the sum of the dosage of the acrylic acid and the dosage of the acrylamide; the dosage of the photoinitiator is 0.1 wt%-0.5 wt% of the sum of the dosage of the acrylic acid and the dosage of the acrylamide. The ionic gel with a bionic structure is formed by synergistically proportioning double monomers (acrylic acid / acrylamide) and the conductive ionic liquid and combining a specific cross-linking system, and the ionic gel is sensitive to humidity change response and remarkable in signal strength. The device is suitable for being applied to the fields of respiration monitoring and non-contact switches.

The invention discloses a fluorinated COF enhanced PVDF-HFP composite gel polymer electrolyte. The fluorinated COF enhanced PVDF-HFP composite gel polymer electrolyte is prepared from the following raw materials: polyvinylidene fluoride-co-hexafluoropropylene, a fluorinated covalent organic framework containing an ether oxygen bond and a carbon-carbon unsaturated double bond, bis (trifluoromethylsulfonyl) imide anion ionic liquid and fluorine-containing imide lithium salt, the fluorinated covalent organic framework containing the ether-oxygen bond and the carbon-carbon unsaturated double bond is prepared by carrying out condensation reaction on a perfluorophenylene-containing module and the ether-oxygen bond-containing aromatic module. According to the electrolyte, PVDF-HFP is used as a polymer matrix, bis (trifluoromethylsulfonyl) imidogen ionic liquid is used as a functional phase and a plasticizer, imide lithium salt is used as a lithium ion source, fluorinated COF containing ether oxygen bonds and olefinic bonds is introduced, and the electrolyte has high ionic conductivity, high lithium ion transference number, excellent mechanical property and interface stability; the method is especially suitable for a high-safety lithium metal battery system.

The application belongs to the technical field of etching liquid, and particularly relates to an anti-crystallization copper etching liquid and a preparation method and application thereof. The copper etching liquid is obtained by mixing hydrogen peroxide, inorganic acid, organic acid, fluorine compound, hydrogen peroxide stabilizer, organic sulfonic acid sodium salt, pyrazine polycarboxylic acid, amino acid ionic liquid and water. The components in the copper etching liquid jointly act, so that the phase stability of the copper etching liquid is significantly improved, the copper etching liquid can avoid crystallization in long-time work, and is suitable for industrial application.

The invention provides an azacyclo-ionic liquid solvent as well as a preparation method and application thereof. The azacyclo-ionic liquid solvent comprises azacyclo-ionic liquid and an organic solvent, the structure of the azacyclo ionic liquid is [M] [Y], [M] is an imidazole cation, and [Y] is an azacyclo anion and comprises any one of [Y1], [Y2], [Y3] or [Y4]. The azacyclo ionic liquid solvent provided by the invention realizes directional regulation and control on the phase change behavior of the solvent after CO2 is absorbed by regulating the structures and polarities of the imidazole cations and the organic solvent, so that homogeneous-phase or phase-change ionic liquid solvents meeting different requirements are obtained, and absorbents adaptive to different scenes are obtained; guidance is provided for directional design of the carbon capture functional ionic liquid solvent, and the workload in solvent design is effectively reduced.

The invention belongs to the technical field of energetic plasticizer preparation, and particularly discloses a method for preparing N-butyl nitroxyethyl nitramine through ionic liquid nitration. The method comprises the following steps: mixing an ionic liquid nitrating agent with butyl ethanolamine to obtain a mixed solution; and mixing the mixed solution with a catalyst and acetic anhydride, reacting, and carrying out post-treatment to obtain the N-butyl nitroxyethyl nitramine. According to the method, the ionic liquid with stable properties is adopted as the nitrating agent, the reaction is mild when the ionic liquid is mixed with the butylethanolamine, violent heat release caused when fuming nitric acid is in contact with the butylethanolamine is effectively avoided, and the ionic liquid precursor can be recycled through simple extraction after the reaction.

The invention belongs to the technical field of composite material manufacturing, and discloses a structural battery integrated composite board and a forming method and application thereof. According to the composite board, carbon fiber reinforced materials are adopted as positive and negative electrodes, glass fiber materials are adopted as a diaphragm and an insulating layer, epoxy resin-based solid-state structure electrolyte is adopted as a bonding packaging medium, and a curing agent, ionic liquid, electrolyte lithium salt, nano ceramic particles and other auxiliaries of specific types and proportions are introduced into epoxy resin; the multifunctional modification of the resin matrix is realized. And meanwhile, doping and surface grafting modification are performed on the electrode material, so that the energy density and the mechanical strength of the battery are improved. And further constructing a low-temperature formed metal or carbon-based circuit layer on the outer surface of the structural battery to form an integrated complex comprising the circuit board, the structural battery and the bearing structure. The composite board satisfies dielectric insulation and reliability, realizes integrated energy supply and signal processing, and is widely applied to weight and volume sensitive fields such as aerospace and new energy automobiles.

The invention discloses a preparation method and application of a catalyst based on pyridine ionic liquid, and belongs to the technical field of catalyst preparation. According to the invention, a hydrolysis reaction of a silane coupling agent is utilized to prepare a silicon oxide nanotube containing a pyridine unit, and then a quaternization reaction is carried out to obtain the catalyst based on the pyridine ionic liquid. The catalyst has a high specific surface area and a rich pore channel structure, exposure of active sites and contact of the active sites and reactants are facilitated, and the catalytic rate is increased. Meanwhile, the silicon oxide nanotube contains hydroxyl, and can cooperate with a pyridine ionic liquid site to catalyze a carbon dioxide cycloaddition reaction. The obtained catalyst can catalyze the reaction of carbon dioxide and an epoxy compound to prepare cyclic carbonate under solvent-free and metal-free conditions, and the catalyst is easy to recover and simple in product purification, and has a good application prospect.

The invention discloses a protective base film for a polaroid and a preparation method of the protective base film, and belongs to the technical field of optical display equipment protective films. The protective base film comprises an antistatic PET base material layer and a self-adhesive layer, the antistatic PET base material layer is prepared by blending optical-grade PET slices and antistatic master batches, the master batches are prepared by taking ionic liquid dihydric alcohol as a comonomer, and the base film is endowed with lasting and stable intrinsic antistatic performance; the self-adhesive layer is formed by melting and blending a polyurethane acrylate prepolymer, a modified montmorillonite filler, other matrix materials and auxiliaries according to a specific ratio and carrying out an online UV curing process. Through innovative material design and an integrated forming process, the prepared protective base film has excellent optical transparency, lasting antistatic property, appropriate bonding strength, clean stripping property and outstanding damp-heat aging resistance, the comprehensive performance is remarkably superior to that of a traditional gluing protective film, and the production process is more environment-friendly and efficient.

A conductive epoxy composition is disclosed comprising an epoxy resin, a low-viscosity hydrocarbon diluent, silver, and graphene. The one-part formulation provides enhanced electrical conductivity, mechanical strength, and process stability. The epoxy resin may include resorcinol diglycidyl ether, diglycidyl ether of Bisphenol A, or Bisphenol F. The hydrocarbon diluent may include glycidyl-ether-family resins having defined carbon-chain characteristics and molecular weights. Silver may be present in particulate, flake, nanoparticle, or coated forms at about 55-90 wt. %, while graphene may be present at 0.03-0.3 wt. % with dimensions of 1-10 μm and surface areas of 400-2,000 m2 / g. Optional additives include solvents, ionic liquids, latent curing agents, and strength enhancers to optimize curing and adhesion.

The invention belongs to the technical field of chemical synthesis, and discloses a method for synthesizing cyclic carbonate through urea alcoholysis under photo-thermal synergistic catalysis. Uniformly mixing the mixed solution of methanol and ionic liquid, zinc salt and other metal salts, and reacting; and after the reaction is finished, centrifugally separating a product, washing, drying, and calcining to obtain the zinc-based homojunction photo-thermal catalyst. The method comprises the following steps: mixing urea, dihydric alcohol and a zinc-based homojunction photo-thermal catalyst, and reacting for 1-6 hours under the conditions that the light intensity is 1-150 mW / cm, the temperature is 130-160 DEG C and the pressure is 5-30 kPa to obtain the cyclic carbonate. The catalyst used in the method effectively overcomes the limitations of low target product synthesis efficiency and high reaction energy barrier in single thermocatalysis, and the yield of the synthesized cyclic carbonate can reach up to 84.1%. Through light energy excitation coupling thermocatalysis, the harshness of reaction conditions is significantly reduced, and efficient synthesis of cyclic carbonate under mild conditions is realized.