The present invention discloses a
nitrogen isotope determination method for
nitrogen in a gas sample, and relates to the technical field of
isotope analysis, the method comprises: instrument performance pretreatment: before sample determination, determining that an instrument is in a stable working state by checking the vacuum degree, detecting the interference peak, tuning an
ion source, and testing the stability and
linearity of reference gas; according to the method, a glass sample
bottle is adopted to collect a gas sample, and before collection, a bidirectional
inert gas replacement-vacuumizing
coupling sampling process is adopted to treat the sample
bottle. Residual air in the sample
bottle and air attached to the bottle wall are effectively removed, and the sample
pollution risk is remarkably reduced; the CO2 adsorption trap adopts a gradient filling structure and is matched with a constant-temperature heating sleeve, so that the
contact time of CO2 and an adsorption material is prolonged, meanwhile, the influence of adsorption heat release on the adsorption efficiency is avoided, and the CO2 removal rate is improved.