The invention relates to the technical field of
electrochemistry, and discloses a liquid-phase electro-
catalysis in-situ
cell for X-
ray absorption spectrum testing, the liquid-phase electro-
catalysis in-situ
cell is characterized in that a
copper working electrode wire, a fixed window and an
insertion window are arranged on an
electrolytic cell cavity, a
cell body top cover is fixedly arranged on the
electrolytic cell cavity, the fixed window is located at one side of the
electrolytic cell cavity, and the
insertion window is located at the other side of the electrolytic
cell cavity. The
insertion window is positioned on the other side of the electrolytic tank cavity; the
liquid layer thickness adjusting
assembly is fixedly mounted in the insertion window; the
working electrode fixing
assembly is fixedly installed in the fixing window. The cavity of the electrolytic tank is of an integrated structure, the light-transmitting tube adopts a 45-degree unfilled corner and an adjustable
liquid layer design, rapid switching of transmission and
fluorescence modes is supported, screws or
adhesive tape fixation is avoided, the integrated cavity shortens the
electrode replacement time to be less than 1 minute, the
test efficiency is remarkably improved, the liquid leakage risk is reduced, a
corrosion-resistant material is matched with an acid / alkaline
electrolyte, and the service life of the electrolytic tank is prolonged. The
modular structure can be expanded to different reaction systems, and is convenient to modify to adapt to other
synchrotron radiation testing technologies.