1831 results about "High concentration" patented technology

The invention provides a method for selecting a high-concentration VOCs adsorbent at different temperatures and application, and belongs to the technical field of waste gas governing. According to the method, through testing pore structure parameters of a model adsorption material with concentrated pore size distribution, a static adsorption isotherm and a dynamic penetration curve for VOCs at different temperatures, a high-concentration VOCs adsorbent is obtained; a linear relation equation of the critical aperture and the critical pressure is established through linear fitting, then a correlation equation of the critical aperture, the temperature and the partial pressure is established, and the appropriate aperture distribution range and the model selection standard of the high-concentration VOCs adsorbent at different temperatures are determined by combining dynamic adsorption results. According to the method, the ternary matching relation equation of the VOCs partial pressure, the temperature and the critical aperture is constructed, accurate type selection of the high-concentration VOCs adsorbent at different temperatures is achieved, the pore volume utilization rate and the adsorption capacity can be improved, meanwhile, desorption energy consumption and the VOCs pyrolysis risk are reduced, and a theoretical basis is provided for adsorbent type selection and technical optimization.

The invention belongs to the technical field of back contact photovoltaic cells, and particularly relates to a back contact photovoltaic cell with high-concentration co-doped regions and a manufacturing method and application thereof.The back contact photovoltaic cell with the high-concentration co-doped regions is characterized in that N-type doped regions and P-type doped regions which are alternately distributed are arranged on the backlight face of an intrinsic amorphous silicon layer, and the high-concentration co-doped regions are arranged between the N-type doped regions and the P-type doped regions; a doping source of the co-doped region comprises doping source phosphorus of the N-type doped region and doping source boron of the P-type doped region, the co-doped region, the doping source of the N-type doped region and the doping source of the P-type doped region form a specific concentration gradient structure, and the specific concentration gradient structure meets the condition that the doping concentration of phosphorus contained in the co-doped region is greater than that of phosphorus contained in the N-type doped region; the doping concentration of boron contained in the co-doped region is greater than the doping concentration of boron in the P-type doped region. The carrier transport and collection efficiency is optimized, the fill factor and open-circuit voltage are improved, the cell conversion efficiency and stability are improved, the preparation process is simple, and multiple times of opening etching are not needed.

The invention relates to the technical field of image data processing, in particular to a water-soluble fertilizer dissolution rate visual measurement method and system, and the method comprises the steps: obtaining a sequence image of a dissolution process; performing multi-scale frequency domain analysis on the image, and calculating a scale convergence index by using the deviation between a local phase and a weighted average phase; a spectral sharpness factor is calculated according to the ratio of the high-frequency energy response to the low-frequency energy response; fusing the scale convergence index and the spectral sharpness factor to obtain a solid boundary probability; segmenting the particle region based on the probability and converting the particle region into physical mass, and differentiating a mass change sequence to obtain a dissolution rate. By fusing the phase consistency and the frequency domain energy distribution characteristics, the physical entity edge and the optical refraction halo are effectively distinguished, the refraction interference problem during high-concentration dissolution is solved, and the dissolution rate measurement accuracy is improved.

The invention discloses a tracing method and system for atmospheric pollution in a chemical industry park, and relates to the technical field of tracing of atmospheric pollution. The method comprises the following steps: determining at least one first pollution source according to an enterprise-pollutant-raw material incidence matrix and at least one pollutant in the chemical industry park; and according to the real-time pollutant concentration data and a Gaussian diffusion model simulation result, screening out an enterprise with a relatively high fitting degree with the real-time pollutant concentration data, and according to a screening result, determining at least one second pollution source. And determining at least one third pollution source according to the position of the at least one pollution source. And determining at least one fourth pollution source in the high-concentration change area. And determining a pollution traceability result. According to the invention, multi-source data are fused to trace the air pollution, the comprehensiveness and timeliness of the data are ensured, and the accuracy of pollution traceability can be improved.

The invention discloses a molecular film type automotive nitrogen and oxygen separation device which comprises a turbocharger, a nitrogen and oxygen separator, a gas inlet valve, a gas outlet valve, a negative pressure pump and an electric control throttling valve. The turbocharger is driven by a turbine in an automobile turbocharger, so that the air is compressed to be conveyed to two paths of the nitrogen and oxygen separation device, the nitrogen and oxygen separation device can separate oxygen from the air, the air with high oxygen content is output, and the air is supplied to an engine for use through the gas outlet valve. The two paths of the nitrogen and oxygen separation device work alternately, when the temperature of the two paths of the nitrogen and oxygen separation device is too high to influence oxygen production efficiency, a main air inlet pipeline is opened to provide air normally by controlling the opening degree of the electric control throttling valve, and thus the phenomena of gas circuit plugging and engine stalling are avoided. According to the automotive nitrogen and oxygen separation device, the two branch paths work alternately, high concentration oxygen can be supplied to the engine continuously so that fuel can burn and act, and the burning utilization rate of the fuel is improved.

The invention discloses a multi-network anti-freezing hydrogel electrolyte, a preparation method thereof and application of the multi-network anti-freezing hydrogel electrolyte in an electrochemical device. The hydrogel is prepared by using polyvinyl alcohol (PVA) and polyacrylamide (PAM) to form a basic network skeleton, introducing phytic acid, ethylene glycol and lithium / zinc bimetal salt (Li2SO4 / ZnSO4), and carrying out thermal initiation polymerization and freeze thawing. The hydrogel prepared by the invention has a multiple physical cross-linked network formed by polymer molecular chain entanglement, hydrogen-bond interaction among functional groups and metal coordinate bonds constructed between phosphate groups and divalent metal ions, so that the hydrogel electrolyte has excellent mechanical properties. Due to introduction of ethylene glycol, formation of ice crystals is effectively inhibited, and the hydrogel is endowed with excellent anti-freezing performance; the high-concentration Li < + > and Zn < 2 + > ensure the high ionic conductivity. The supercapacitor assembled by using the hydrogel electrolyte shows relatively high specific capacitance and good capacitance retention rate under bending and freezing conditions, and has good electrochemical properties and safety performance.

The invention discloses a method for detecting the concentration of vanadium ions in an electrolyte of an all-vanadium redox flow battery, and relates to the technical field of batteries. The method for detecting the concentration of vanadium ions in the electrolyte of the all-vanadium redox flow battery comprises the following steps: preparing trivalent and tetravalent vanadium ion reference solutions and trivalent and tetravalent vanadium ion standard solutions with different concentrations; performing baseline correction by using a high-concentration reference solution, setting an absorbance difference value between a corresponding reference cell and a sample cell as 0, and obtaining a trivalent vanadium ion standard curve and a tetravalent vanadium ion standard curve by using standard solutions with different concentration gradients; and detecting the absorbance difference value of the electrolyte stock solution to be detected, and substituting the absorbance difference value into the corresponding standard curve to calculate the vanadium ion concentration. According to the present invention, the detection can be performed without diluting the electrolyte stock solution during the detection, the interference of the adjacent valence vanadium ions is not easily generated, and the detection result is accurate.

The embodiment of the invention provides a composite substrate and a preparation method of the composite substrate, relates to the technical field of semiconductor devices, and is used for solving the technical problem of relatively high bonding interface resistance of a composite substrate formed by bonding a 3C-SiC substrate and a 4H-SiC substrate in related technologies. The composite substrate comprises a 3C-SiC layer and a 4H-SiC layer, the 4H-SiC layer comprises a first surface, and the 3C-SiC layer comprises a second surface; the first surface and / or the second surface comprises a high-concentration doped layer with N-type conductivity, and a bonding interface of the 3C-SiC layer and the 4H-SiC layer is a contact surface between the high-concentration doped layer and the second surface, between the high-concentration doped layer and the first surface or between the high-concentration doped layer and the two high-concentration doped layers. The interface energy band is adjusted through the energy band bending effect of the high-concentration doping layer, the barrier width and height of the bonding interface are reduced, electrons penetrate through the barrier through a tunneling mechanism, the migration efficiency of the electrons on the heterojunction interface is improved, and the interface resistance is reduced.

The invention discloses a preparation method and application of samarium-doped lanthanum ferrite nanofibers, and the preparation method is a design thought based on synergistic interaction of'defect engineering 'and'morphology control': samarium (Sm) ions with a specific proportion are creatively introduced to the A site of LaFeO3, and lattice distortion is induced by utilizing radius mismatch between the samarium (Sm) ions and lanthanum (La) ions; therefore, high-concentration gas-sensitive active sites (oxygen vacancies) are generated in the intrinsic structure of the material; and the material is constructed into a one-dimensional nanofiber network with a high specific surface area through an electrostatic spinning technology, so that the exposure efficiency of active sites is maximized.

The invention provides a TBC cell P region structure, a TBC cell and a preparation method thereof, and a photovoltaic module, and relates to the technical field of solar cells, the TBC cell P region structure comprises a first tunneling oxide layer, a first boron-doped polycrystalline silicon layer, a second tunneling oxide layer and a second boron-doped polycrystalline silicon layer which are sequentially laminated on the back surface of a silicon substrate; wherein the doping concentration of the second boron-doped polycrystalline silicon layer is higher than that of the first boron-doped polycrystalline silicon layer. In the invention, the bottom layer is doped with i-poly at a relatively low concentration, so that boron accumulation on the interface is inhibited, the BRL (boron-rich layer) concentration is reduced, and a low Auger composite interface is obtained; and then a thin tunneling layer is deposited again, and a second polycrystalline silicon layer is doped with a high concentration, so that auger recombination is reduced, passivation and contact performance is improved, opening voltage is improved, filling factors are improved, and the conversion efficiency of the cell is improved finally.

The invention belongs to the technical field of water quality parameter inversion, and particularly relates to a machine learning-based suspended matter concentration remote sensing inversion method and system, and the method comprises the steps: collecting a satellite remote sensing image and synchronous actual measurement suspended matter concentration data, and obtaining a space gridding water body remote sensing reflectivity matrix through radiometric calibration, atmospheric correction and water body mask. Reconstructing and denoising through wavelet decomposition, and normalizing and standardizing the spectrum to obtain a spectrum numerical sequence; multi-scale waveband combination and differential features are constructed based on the sequence, and sensitive features are screened out by using XGBoost. A physical constraint term is constructed in combination with sensitive characteristics and a water body radiation transmission rule, and an intermediate inversion result is obtained through numerical iteration. And performing deviation compensation on an intermediate result by using a deep learning residual error, and finally performing spatial smoothing, consistency verification and high-concentration saturation optimization to obtain a high-precision and spatially continuous suspended matter concentration spatial distribution result. According to the method, efficient feature mining and physical mechanism deep fusion are realized, and the explanatory and generalization ability of the model is greatly improved.

The invention belongs to the technical field of biological medicines, and particularly discloses a bionic nano-vesicle for regulating and controlling neutrophil phenotype in combination with ultrasound, and a preparation method and application of the bionic nano-vesicle. The bionic nano-vesicle provided by the invention can be broken under the action of high-concentration glutathione existing in a tumor tissue microenvironment to release the sound-sensitive agent and functional siRNA, and under the action of US irradiation, the sound-sensitive agent is activated to generate a large amount of ROS, promote tumor cell DNA breakage, generate a large amount of double-stranded DNA, activate APC and promote IFN-beta release, so that the tumor tissue microenvironment is inhibited. The released functional siRNA can promote the N2-type neutrophile granulocyte to become N1-type neutrophile granulocyte, and the released functional siRNA can prevent the N1-type neutrophile granulocyte from being reversed to the N2-type neutrophile granulocyte again, so that the regulation and control on the phenotype of the neutrophile granulocyte are realized; under catalysis of CAT rich in the thylakoid membrane, H2O2 overexpressed by tumor tissue is decomposed into oxygen, the tumor hypoxia microenvironment can be relieved, and the tumor treatment effect can be improved.

The invention belongs to the technical field of intelligent fragrance control, and discloses an intelligent fragrance control system and method based on olfaction perception self-adaption, multi-dimensional data such as exhaled gas fragrance residue and skin electroreaction are captured in real time through a multi-mode olfaction fatigue monitoring unit, and 1-5 olfaction fatigue levels are accurately judged in combination with an LSTM-attention model; and then the dynamic release control unit is matched with a layering strategy, for example, short-time pulse stimulation is started in light fatigue, fragrant cross-modulation switching and concentration zeroing are triggered in heavy fatigue, and local high-concentration pseudo fatigue is avoided synchronously through a distributed space probe. By means of the design, fragrance release is always matched with the real-time olfaction state of a user, the problem that the fragrance cannot be effectively perceived after continuous exposure is thoroughly solved, it is ensured that the user can stably perceive the fragrance in different use periods, and the use experience is remarkably improved; and a complete logic chain with multi-mode monitoring, double-target sensing and cooperative control is constructed.

A semiconductor device includes a chip that has a main surface, a high concentration region of a first conductivity type that is formed in a surface layer portion of the main surface on an inner portion side of the chip, and a low concentration region of the first conductivity type that is formed in the surface layer portion of the main surface on a peripheral edge portion side of the chip, and has an impurity concentration lower than an impurity concentration of the high concentration region.

The invention provides application of high-concentration colloidal gold in preparation of an influenza virus detection test strip, and relates to the technical field of immunodetection. The detection test strip provided by the invention is composed of a sample pad, a combination pad, a nitrocellulose membrane, a water absorption pad and a bottom plate, and in the preparation process of the detection test strip, high-concentration colloidal gold with the OD value of 100 is adopted for respectively marking an influenza A virus monoclonal antibody 1, an influenza B virus monoclonal antibody 1 and a chicken IgY antibody; optimized colloidal gold labeled reconstitution fluid is mixed and then sprayed on the combination pad, and meanwhile, a corresponding capture antibody and a goat anti-chicken IgY antibody are respectively sprayed on the nitrocellulose membrane to form a detection line and a quality control line. Through the synergistic effect of the high-concentration colloidal gold mark, the optimized sample pad / combination pad treating fluid and the special sample diluent, the detection sensitivity is remarkably improved, the false negative rate is effectively reduced, and rapid, high-sensitivity and high-specificity field detection on influenza A and B viruses is realized.

The invention relates to the technical field of environment monitoring, and discloses a real-time detection method and system for concentration and components of air particulate matters. According to the method, signal fragments are intercepted from continuous detection flow of an air sample in a segmented mode to serve as analysis elements, a de-noising characteristic signal set is generated through background field stripping, and background field parameters are recorded. And positioning a high-concentration characteristic peak cluster in the de-noised signal to mark a key detection window, and constructing a corresponding dynamic detection task sequence. And calling a special analysis thread to carry out collaborative analysis on the de-noised characteristic signal set to obtain a hierarchical judgment result. And the result is coupled and compared with background field parameters, and if conflicts exist, the dynamic detection task sequence is recombined in real time. And updating and executing a control strategy for a subsequent detection flow according to the recombined sequence, thereby forming a self-adaptive closed-loop detection process. According to the invention, the accuracy, depth and adaptive capacity of real-time analysis of pollution components in a complex environment are improved.

The invention relates to a silicon single crystal drawing method capable of reducing the resistivity range of a whole silicon single crystal rod, which belongs to the technical field of wafer processing and comprises the following operation steps of: 1, completely melting a solid silicon material and a doping agent into liquid in a crucible a; and 2, slowly lowering the crucible position in the crucible b to realize that a part of liquid at the bottom of the crucible is slowly solidified into a solid from the bottommost part. And 3, after the crucible in the crucible c is slowly lowered and stopped, seeding, shouldering and equal-diameter operation are carried out. And 4, carrying out an equal-diameter growth stage in the d crucible. And 5, continuously growing the single crystal rod in the e crucible. And 6, finishing silicon single crystal drawing in the crucible f through an ending process. An initial state of'high-concentration melt + low-concentration solid 'is constructed before crystal pulling, and real-time and dynamic dilution compensation is performed on the concentration of a dopant of a main melt, so that the inherent defect of resistivity axial non-uniformity caused by a segregation effect in a traditional Czochralski method is effectively overcome.

The invention provides a micro-disk structure semiconductor laser and a preparation method, and belongs to the technical field of semiconductor lasers. The high-concentration Zn-doped p-GaAs multi-quantum-well multi-quantum-well light-emitting diode comprises a SiO2 barrier layer, an n-GaAs substrate with the thickness of 100 microns, an n-GaAs contact layer with the thickness of 100 nm, a Si-doped n-AlGaInP limiting layer with the thickness of 200 nm, an n-AlGaInP waveguide layer with the thickness of 400 nm, a first GaInP / AlGaInP multi-quantum-well layer, a GaAs barrier layer, a second GaInP / AlGaInP multi-quantum-well layer, an undoped p-AlGaAs waveguide layer with the thickness of 150 nm, a Zn-doped p-AlGaInP limiting layer with the thickness of 200 nm and a high-concentration Zn-doped p-GaAs contact layer with the thickness of 100 nm. By controlling the thickness and the doping concentration of each layer, efficient limitation and injection of carriers are realized; due to the design of the double multi-quantum well layer and the barrier layer, the device can realize stable lasing in two wavebands of 808nm and 650nm; the undoped waveguide layer effectively reduces the optical loss, prolongs the photon lifetime, and improves the laser output efficiency. And the quantum efficiency and the temperature stability of the device are improved.

The invention relates to the technical field of detection kits, in particular to a blood coagulation reaction linked lupus anticoagulant fluorescence detection kit and application thereof, the kit contains a screening-confirmation integrated reagent, a calibration product, a quality control product and an anticoagulation interference inhibitor; the integrated reagent is divided into a reagent A and a reagent B, the reagent A contains a buffer solution, recombinant snake venom thrombin, composite phospholipid, a fluorescent substrate and other components, and the reagent B contains prothrombin, calcium ions, high-concentration composite phospholipid and other components; the composite phospholipid system is formed according to a specific proportion and modifies beta2-glycoprotein I, the fluorescence enhancement-stabilization system is formed by matching a Schiff base compound with a stabilizer, the calibrator is a series of lupus anticoagulant standard substances, and the quality control substance comprises simulants with different concentrations and negative control. The anti-interference capability is high, and the influence of anti-coagulant drugs and enzyme source fluctuation is reduced; the signal amplification effect is obvious, the detection sensitivity is high and the reagent stability is good; the operation is simple and convenient, screening and confirmation are integrally completed, and a conventional fluorescence detector is adapted.

The invention relates to a preparation method of a biomass-based degradable dust suppressant and a spraying device. The biomass-based degradable dust suppressant is prepared from the following components in percentage by weight: 0.78% of a biological matrix, 20.7% of a salting-out salt solution and the balance of an acetic acid solution diluted by deionized water, the method comprises the following specific steps: adding biological matrix powder into an acetic acid solution; the salting-out salt solution powder is poured into a biological matrix acetic acid solution, magnetic stirring is conducted for 30 min under the conditions that the rotating speed is 200 r / min and the temperature is 30 DEG C, and then ultrasonic treatment is conducted for 10 min for full reaction; a salting-out method and a dust suppression technology are combined, high-concentration salt solutions such as sodium citrate and sodium sulfate are selected, physical and chemical effects between salt ions and biomass material molecules are utilized, and the limitation of a traditional cross-linking mode is broken through the synergistic effect of salting-out auxiliary precipitation and weak ion cross-linking net forming; according to the present invention, the long-acting and safe dust suppression agent can be simply and conveniently prepared, the dust suppression efficiency can be effectively improved, and the dust suppression cost can be effectively reduced.

The invention discloses a method suitable for extracting extracellular small vesicles in fresh water pearl shell tissue waste liquid, which comprises the following operation steps: (1) solid-liquid separation: slaughtering pearl shells, and filling slaughtering waste liquid into a waste liquid crude extraction device; (2) waste liquid crude extraction: performing multi-stage gradient filtration and gravity settling on the slaughtering waste liquid by using a waste liquid crude extraction device to obtain clarified waste liquid; (3) removing impurities: removing impurities for the first time and removing impurities for the second time; (4) concentration of the extracellular vesicles: concentrating the extracellular vesicles by using an ultra-speed centrifuge to obtain a high-concentration extracellular vesicle solution; and (5) preservation of extracellular vesicles: according to the final volume of the high-concentration extracellular vesicle solution obtained in the step (4), carrying out sample standardization through protein concentration, sub-packaging the sample, and carrying out long-term preservation in a low-temperature environment. The particle sizes of the extracted vesicles are concentrated, high-purity and complete extracellular small vesicles can be obtained, and the method is suitable for biomedical research and product development.

The invention relates to the technical field of radiation environment monitoring, and discloses a dose calculation method and system based on radiation environment monitoring data. The method comprises the following steps: acquiring radiation source data, calculating initial radiation field distribution based on the data, obtaining an initial dose deposition value of each space point in a monitoring area, analyzing interaction among particles, and determining an energy redistribution coefficient of each space point; adjusting the initial dose deposition value point by point by using the coefficient to obtain corrected three-dimensional dose concentration field data, calculating a gradient vector between spatial points, and generating an optimized gradient distribution diagram; extracting a boundary point set with gradient change exceeding a threshold value, constructing a contour surface grid to form a three-dimensional contour surface structure, obtaining a time sequence radiation source data iteration updating coefficient, and obtaining a concentration field time sequence evolution sequence; the high-concentration area is identified and marked based on the sequence, the high-concentration area and the three-dimensional contour surface structure are fused, a visual distribution model reflecting the dose concentration is generated, and the accuracy of radiation dose calculation is improved.

The invention relates to the technical field of lasers, and discloses a corona-based creeping spark discharge strong pre-ionization pulse gas laser which comprises a main frame chamber, a pre-ionization device is fixedly mounted at the top of an inner cavity of the main frame chamber, a cathode electrode is arranged at the top of the inner cavity of the main frame chamber, and a connecting copper sheet is fixedly mounted on the lateral upper portion of the inner wall of the main frame chamber. A flow guide plate is fixedly installed on the connecting copper sheet, and an anode electrode is fixedly installed at the top end of the flow guide plate. A corona-based creeping spark discharge strong pre-ionization pulse gas laser is characterized in that a pre-ionization area can be formed on a pre-ionization device and structures on the pre-ionization device, electrons in the pre-ionization area move in an accelerated manner under the action of electric field force, and in the movement process, the electrons in the pre-ionization area are separated from the pre-ionization device. And the electrons and other gas particles are subjected to inelastic collision and ionization or excitation, so that high-concentration and uniform initial electrons are generated, a micro-discharge channel is formed, and continuous seed electrons are provided for a core discharge region of the micro-discharge channel.

A MEMS gas sensor and a preparation method therefor, comprising an insulating substrate (1), a heating electrode (403), an insulating layer (105) and a testing unit, which are overlappingly disposed. The testing unit comprises a testing electrode, a sensing unit (2), and a selective separation membrane (3); the sensing unit (2) has a nanowire array structure formed by multiple nanowires disposed at intervals, and the selective separation membrane (3) covers the surface of the sensing unit and a recessed portion; the nanowires comprise a first metal and a second metal, the first metal being Pd, and the second metal being at least one selected from Ni, Cu, Ag, Au and Ir; the selective separation membrane (3) comprises an inner separation membrane (301) and an outer separation membrane (302) which are stacked in sequence; the inner separation membrane (301) comprises polytetrafluoroethylene, and the outer separation membrane (302) is a mixed matrix membrane having a covalent organic framework material as a filler and a polymer of intrinsic microporosity as a matrix. The MEMS gas sensor possesses excellent sensitivity for low-concentration gas monitoring, and tolerance stability for high-concentration gas, as well as excellent anti-interference performance and response speed.

The invention discloses iron oxide nanoparticles capable of responding to particle size change in a tumor microenvironment and a preparation method of the iron oxide nanoparticles, and belongs to the technical field of biomedical nano materials. The nano-particle comprises an iron oxide nano-crystal core with the particle size of 3-5nm and a tumor microenvironment response layer coating the surface of the iron oxide nano-crystal core. The response layer contains groups, such as disulfide bonds, enzyme digestion peptide fragments and the like, which can respond to acidic pH, high-concentration reduced glutathione or matrix metalloproteinase and other tumor characteristic stimuli to generate structural changes. In a tumor microenvironment, the hydration particle size of the nanoparticles can be directionally and controllably converted from 3-20 nm to 20-100 nm (or reversely). The preparation method mainly comprises two steps of preparing the core by a thermal decomposition method and modifying the surface response layer. The technical problems of insufficient tumor targeted enrichment capacity, limited imaging contrast and difficulty in balancing permeation and retention caused by fixed particle size of the existing iron oxide nanoparticles are solved, and the accuracy and efficiency of tumor diagnosis and treatment can be remarkably improved.

A method for separating and purifying 4MP1 from a mixture containing 4MTP2 and 1-Hexene comprises the following steps: continuously introducing a solution in which 4MTP2, 1-Hexene and 4MP1 with any concentration are dissolved into a simulated moving bed chromatography system as a raw material solution, collecting a high-purity 4MP1 solution from raffinate of the simulated moving bed chromatography system by adopting a metal organic framework material as a stationary phase, and separating the high-purity 4MP1 solution from the raffinate of the simulated moving bed chromatography system. The extraction liquid is a solution containing impurities 4MTP2 and 1-Hexene. The invention provides a brand new method for separating 4MP1 from 4MTP2 and 1-Hexene, and a complete separation scheme is provided for the prior art; in the separation of high-concentration 4MP1, the relative purity of the separated and purified 4MP1 can reach gt; the recovery rate is gt; and in the separation of low-concentration 4MP1, the rectification level is also exceeded, and the method is more suitable for 4MP1 thermosensitive substances.

The invention discloses a modular tumor microenvironment response polypeptide and a preparation method and application thereof. The modular tumor microenvironment response polypeptide is composed of the following functional modules: a targeting and chemotactic module used for targeting tumor cell surface p32 protein and tumor lymphatic vessels and promoting tumor tissue penetration and enrichment; the microenvironment double-response module is used for being cut by MMP-2 / 9 enzyme and broken by high-concentration glutathione GSH in a tumor microenvironment to trigger self-assembly; the self-assembly driving module is used for exposing after the microenvironment responds to activation and driving short peptides to be self-assembled to form a nano structure; a killing module: a pro-apoptotic peptide PAD used for targeting a mitochondrial membrane and inducing tumor cell apoptosis; and the stability optimization module is used for enhancing the degradation resistance of the oligopeptide. By integrating targeted delivery, enzyme digestion response, acid-sensitive release and stabilizing structures, the problems of insufficient targeting property, inaccurate release, poor stability, diagnosis-treatment splitting and the like of the anti-tumor drug and the developing agent are solved.

The invention discloses synchronous test paper for Fe < 3 + > and Fe < 2 + > as well as a preparation method and application of the synchronous test paper, and effectively solves the problem that high-concentration Fe < 3 + > and Fe < 2 + > in a boiler chemical cleaning solution are difficult to rapidly, accurately and simultaneously detect. The detection test paper is provided with isolated first and second color developing regions, provides an independent space for Fe < 3 + > and total iron detection, and is anti-interference and accurate. A potassium thiocyanate-hydrochloric acid color developing agent is specially used for measuring Fe < 3 + > in the first color developing area, a phenanthroline-ascorbic acid color developing agent is used for measuring total iron in the second color developing area, and the concentration of Fe < 2 + > is calculated in a combined mode. A standard colorimetric card is matched, color blocks accurately correspond to the concentration range (0-5000 mg / L), the common iron ion concentration is covered, and a comparison basis is provided for detection. During detection, information can be rapidly and visually obtained by comparing the color of the color developing area with the color chart, operation is easy and convenient, complex equipment and professionals are not needed, and field requirements are met. And the scheme is resistant to interference of high-concentration and complex components, and the result is real and reliable.

The invention provides a TBC battery, a preparation method thereof and a photovoltaic module, and relates to the technical field of solar cells, and the front surface structure of the TBC battery comprises an N + front surface field layer, a front phosphorosilicate glass layer, a passive film layer and an antireflection film layer which are sequentially stacked on the front surface of a silicon substrate; wherein the N + front surface field layer is a high-concentration N-type region formed by doping phosphorus atoms on the front surface through phosphorus diffusion. An N + front surface field (FSF) is added on the front surface of the cell, phosphorus atoms are doped on the front surface through phosphorus diffusion to form an N + region, an N-N + high-low junction is formed with an N-type silicon substrate, minority carriers are repelled, and the field passivation effect is improved.

The invention discloses a membrane separation and concentration system for treating solid waste incineration fly ash, relates to the technical field of membrane separation, and aims to solve the technical problem that a concentrated solution is difficult to form a high-concentration state due to reduction of membrane flux caused by thickening of a filter cake layer. An annular filter membrane is installed on the rotating frame, a concentration chamber is formed in an inner cavity of the annular filter membrane, a supporting pipe body is arranged in the concentration chamber, a liquid inlet channel is arranged in an inner cavity of the supporting pipe body, and a plurality of gathering plates and collecting assemblies are further arranged in the concentration chamber. The device has the advantages that a stable filter cake layer formed on the surface of the membrane during static filtration is broken, membrane hole blockage caused by continuous deposition of impurities is avoided, a concentrated solution can be in full contact with a new filter hole area, which does not participate in preliminary filtration, of the annular filter membrane, the filter area of the filter membrane is utilized to the maximum extent, and the filter efficiency and the concentration multiple are improved.