The invention provides an
oxide solid electrolyte material and a preparation method and application thereof, and relates to the technical field of
electrolyte material preparation, the preparation method comprises the following steps: 1) preparing pure-phase
lithium borate from BLiO2, Li2O and B4Li2O7 according to a certain proportion under a certain condition; 2) mixing
lithium borate with a
zirconium source, a
lithium source and a
doping agent according to a certain proportion, and carrying out ball milling or wet ball milling /
drying; 3) then tabletting, carrying out primary high-temperature
solid-phase
sintering, crushing and the like; and 4) finally, mixing and ball-milling the doped and modified LZBO and a
coating agent, tabletting, and then carrying out secondary high-temperature
solid-phase
sintering, crushing and the like to obtain the LZBO material. Aiming at the defects of the traditional high-temperature solid-
phase synthesis method, by innovating
raw material combination and process steps, the
reaction temperature is reduced, the product purity and the production efficiency are improved, and
energy conservation and emission reduction are realized. According to the invention, the
ionic conductivity, the compaction density, the battery rate, the cycle performance and the like are improved, and the application range is widened.