3472results about "Process control/regulation" patented technology

Disclosed herein are cell processing systems, devices, and methods thereof. A system for cell processing may comprise a plurality of instruments each independently configured to perform one or more cell processing operations upon a cartridge, and a robot capable of moving the cartridge between each of the plurality of instruments.

Disclosed herein are cell processing systems, devices, and methods thereof. A system for cell processing may comprise a plurality of instruments each independently configured to perform one or more cell processing operations upon a cartridge, and a robot capable of moving the cartridge between each of the plurality of instruments.

Disclosed herein are cell processing systems, devices, and methods thereof. A system for cell processing may comprise a plurality of instruments each independently configured to perform one or more cell processing operations upon a cartridge, and a robot capable of moving the cartridge between each of the plurality of instruments.

Disclosed herein are cell processing systems, devices, and methods thereof. A system for cell processing may comprise a plurality of instruments each independently configured to perform one or more cell processing operations upon a cartridge, and a robot capable of moving the cartridge between each of the plurality of instruments.

The invention discloses an intelligent control type expansion coating preparation reaction kettle device which comprises a reaction kettle body, the interior of the reaction kettle body is divided into a plurality of independent stirring cabins through partition plates, each stirring cabin is internally provided with an independent stirring assembly, a feeding assembly and an observation assembly, and each stirring assembly comprises a stirring shaft, stirring blades and a driver; the stirring blade is provided with a semiconductor chilling plate and a heating element, and the feeding assembly comprises a plurality of feeding channels connected with the stirring cabin, is provided with a flow meter, an electromagnetic valve and a dynamic adjusting module, and is used for independently controlling the feeding amount and the feeding speed of each cabin; the control system comprises a multi-channel data acquisition module, a learning module and a coordination control module, the multi-channel data acquisition module is provided with a sensor network for monitoring the temperature, the pressure and the material state of each stirring cabin in real time for each stirring cabin, and the control system performs coordination control on the stirring cabins according to preset parameters or autonomous learning results. And the stirring speed, temperature and feeding strategy of each cabin are dynamically adjusted.

The invention provides a sulfamic acid continuous crystallization production device and process, the sulfamic acid continuous crystallization production device comprises a filter box and a production box, the production box is fixedly connected to the upper surface of the filter box through bolts, the top end of the production box is provided with a feeding pipe, the middle part of the interior of the production box is provided with a partition plate, and the middle part of the partition plate is provided with a conveying pipe; a discharging pipe, a production reaction module and a filtering and cleaning module are arranged between the production box and the filtering box. According to the sulfamic acid continuous crystallization production device and the sulfamic acid continuous crystallization production process, in the sulfamic acid continuous crystallization production process, when sulfamic acid crystals are filtered out from mother liquor through the filter cartridge, purified water is sprayed into the filter cartridge through the spray head; and the sulfamic acid crystals can be quickly and uniformly washed to remove impurities through the filter cartridge which continuously shakes in a reciprocating manner in the rotating process, so that the continuous crystallization production efficiency of the sulfamic acid can be effectively improved.

The invention provides a flexible preparation system and method for sustainable aviation fuel, and the system comprises a green power supply module which is used for outputting fluctuating green electric energy; the process execution device is connected with the green power supply module and comprises five process modules, namely an air carbon capture module, a co-electrolysis module, a Fischer-Tropsch synthesis module, a hydrogen production module and a hydrogenation refining module; the data acquisition module is used for acquiring the temperature, the pressure, the liquid level, the raw material input flow and / or the product output flow of each process module in the process execution device; and the decision control module is used for predicting the future power supply condition of the green electricity based on the historical weather data of the green electricity location, adjusting the distribution of the power in each process module according to the future power supply condition, and adjusting the temperature, pressure and / or raw material input flow in each process module. According to the invention, the cost, the reliability, the operation and maintenance performance, the product quality and the green power utilization rate can be substantially improved at the same time, and the flexible and stable operation of the system under the green power condition is realized.

The invention relates to a multi-section quench trickle bed reaction system and reaction method for liquid phase hydrogenation of aldehyde and ketone, the system comprises a multi-section quench liquid phase hydrogenation reactor filled with at least two sections of catalyst bed layers, a product circulating liquid inlet is arranged above each section of catalyst bed layer and is used for introducing a product circulating liquid into the corresponding catalyst bed layer; the adiabatic temperature rise of each section of the catalyst bed layer of the reactor is independently controlled by controlling the flow and the temperature of the circulating quenching liquid of each section of the catalyst bed layer; the method can effectively reduce the adiabatic temperature rise of the catalyst bed layer, prolong the service life of the catalyst, reduce the occurrence of side reactions, improve the product quality and yield, reduce the circulation volume of the liquid-phase product, and reduce the energy consumption. And a better hydrogenation effect can be realized by adopting a single trickle bed reactor, so that the equipment investment is reduced.

The invention relates to the technical field of temperature control, in particular to an enzyme reaction kettle self-adaptive temperature control system and method, and the system comprises a temperature detection module, a temperature control module, a heat conduction oil flow control module and an automatic regulation and control module; temperature data of a reaction kettle are collected in real time through a temperature detection module, a temperature control module adjusts parameters based on a PID algorithm and fuzzy logic to generate a control instruction, and a heat conduction oil flow control module adjusts flow by combining double-closed-loop cascade control with a feedforward compensation algorithm, so that thermal inertia lag is shortened. And the automatic regulation and control module generates optimized process parameters based on a reaction kinetic model and a genetic algorithm, and dynamically adjusts a temperature set value. The control method comprises the steps of temperature data acquisition, PID control instruction generation, conduction oil flow coordinated regulation, process parameter optimization and the like. The problems that in the prior art, temperature control precision is insufficient, conduction oil flow control is not accurate enough, and technological parameters cannot be automatically regulated and controlled are solved.

Disclosed is an apparatus for generating a product passport, the apparatus comprising: one or more computing node(s) and one or more computer-readable media having thereon computer-executable instructions that are structured such that, when executed by the one or more computing node(s), cause the apparatus to perform the following steps:receiving a request to provide a first decentral identifier associated with at least one first physical entity of a product supply chain and / or a recycling product chain;in response to the request, providing the first decentral identifier associated with the at least one first physical entity of the product supply chain and / or the recycling product chain;generating a product passport including the first decentral identifier and data related to the at least one first physical entity of the product supply chain and / or the recycling product chain;providing the product passport for access by a data consuming service under control of a data providing service associated with a data owner.

The invention provides a wind-solar hydrogen production and ammonia synthesis system and a configuration method thereof, electronic equipment and a storage medium. The wind and light hydrogen production and ammonia synthesis system comprises a wind and light hydrogen production subsystem, an ammonia synthesis subsystem and a coordination controller which are relatively independent, the ammonia synthesis subsystem comprises a hydrogen storage tank, the hydrogen storage tank is connected with the wind and light hydrogen production subsystem, and the configuration method of the wind and light hydrogen production and ammonia synthesis system can be executed by the coordination controller. The configuration method of the wind-solar hydrogen production ammonia synthesis system comprises the following steps: firstly, determining capacity configuration parameters of a wind-solar hydrogen production subsystem by taking the minimum leveling hydrogen production cost as a target; and determining the capacity configuration parameters of the ammonia synthesis subsystem based on the capacity configuration parameters of the wind-solar hydrogen production subsystem by taking the maximization of the wind-solar absorption rate, the minimization of the total cost of the system and the minimization of the operation cost of the system as targets. The wind and light hydrogen production subsystem and the ammonia synthesis subsystem are subjected to two-stage decoupling type system configuration, and stable operation of the ammonia synthesis process is ensured while efficient utilization of green electricity is achieved.

The invention belongs to the technical field of micro-reaction, and particularly relates to a micro-mixer and a method for continuously preparing nano cooling liquid. Comprising a reaction cavity in which a plurality of reaction flow channels are arranged, all the reaction flow channels are used for preparing nano cooling liquid and are vertically arranged in the reaction cavity in a three-dimensional spiral shape, and each reaction flow channel is internally provided with a plurality of disturbance structures and a plurality of distributors which are arranged in the reaction cavity and located above all the reaction flow channels, each distributor is connected with the inlets of all the reaction flow channels, the collectors are arranged at the outlets of all the reaction flow channels, and pressure regulating structures are arranged in the collectors. According to the invention, the distributor is adopted to enable the reaction fluid to flow into the corresponding reaction flow channel, the three-dimensional spiral flow channel design in the reaction cavity is folded in space, so that the overall size of the microreactor is not too large, and a disturbance structure is arranged in each reaction flow channel, so that the mixing efficiency can be further improved; the production rate of the microreactor is improved, and blockage in a flow channel is avoided.

The invention discloses a continuous synthesis and purification method of hexafluoropropylene oxide, which comprises the following steps: introducing hexafluoropropylene, oxygen and a fluorine-containing solvent into a supergravity reactor to carry out oxidation reaction at the reaction temperature of 100-200 DEG C under the reaction pressure of 1.0-2.5 Mpa for 10-120 seconds, and after the reaction is finished, overflowing and leading out reaction liquid to obtain the hexafluoropropylene oxide. And purifying to obtain the hexafluoropropylene oxide. According to the method, the problems of mass transfer and heat transfer can be effectively solved by using the supergravity reactor, the reaction selectivity is remarkably improved, meanwhile, the productivity is effectively improved, and the supergravity reactor is combined with extractive distillation treatment, so that the conversion rate of the hexafluoropropylene reaches 79% or above, the selectivity of the hexafluoropropylene oxide is 85% or above, and the purity of the hexafluoropropylene oxide after extractive distillation reaches 99%. The invention further discloses a device used in the continuous synthesis and purification method, and cyclic utilization of hexafluoropropylene and the fluorine-containing solvent can be achieved.

The present invention relates to a method and an apparatus for producing nitrile with controlled spray liquid input pressure. According to the manufacturing method, spraying liquid can be atomized, the contact area with ammonia is increased, and the mass transfer efficiency is improved. The present invention relates to a method for producing nitrile, comprising a step (referred to as a reaction step) for producing a nitrile-containing reaction product by subjecting a hydrocarbon raw material to an ammoxidation reaction, and a step (referred to as a cooling step) for cooling the reaction product by spraying a spray liquid onto the reaction product by means of a spraying device, the spraying device comprises a spraying liquid inlet, a first spraying pipe in fluid communication with the spraying liquid inlet, and a plurality of second spraying pipes which are in fluid communication with the first spraying pipe, are perpendicular to the first spraying pipe and extend towards the two sides of the first spraying pipe. The first spraying pipe is communicated with the first spraying pipe through fluid, the second spraying pipe is communicated with the second spraying pipe through fluid, the third spraying pipes are communicated with the second spraying pipe through fluid and extend towards the two sides of the second spraying pipe perpendicular to the second spraying pipe, the nozzles are located at the tail ends of the third spraying pipes and communicated with the third spraying pipes through fluid, and in the cooling step, the spraying liquid input pressure of a spraying liquid inlet is controlled to be 0.06-1.00 MPaG.

The invention discloses a deep learning and automatic control chemical reactor and a resource recovery method, and relates to the technical field of hydrometallurgy, and the deep learning and automatic control chemical reactor comprises a chemical reactor, a motor, a heating device, a monitoring device, a data center and a PLC control system. Based on a PLC control system, a Transform-LSTM time sequence prediction model is integrated, so that real-time monitoring of parameters such as mixed liquid temperature, reaction chamber pressure, mixed liquid viscosity, conductivity and the like in a wet leaching reaction process can be realized; and the heating power of the heating device, the rotating speed of the motor, the raw material adding amount of the feeding port, the mixed material discharging time of the discharging port and the air displacement of the air exhaust port can be automatically and accurately controlled. The problems that stirring efficiency is low, parameter regulation and control are lagged, and manual experience is relied on are solved, through a predictive control strategy, the real-time monitoring and dynamic regulation level is remarkably improved, the wet leaching process is optimized, energy consumption is reduced, the high-grade metal leaching efficiency is improved, and the method is suitable for various wet metallurgy processes.

The embodiment of the invention provides a hydrochloric acid PH control device in a germanium oxide production process and a control method thereof, and belongs to the field of chemical process automatic control. The device comprises an acid liquor storage tank used for storing raw liquor hydrochloric acid and connected to an acid mixing tank through a raw acid feeding control valve; the acid mixing tank is used for mixing an acid solution with a diluent and is connected to the pH regulation reaction tank through a mixed acid feeding control valve; the alkali liquor storage tank is connected to the pH regulation reaction tank through an alkali liquor adding control valve; the pH regulation reaction tank is used for receiving the mixed acid liquor and the alkali liquor and regulating the pH value of a reaction system, and is provided with a pH sensor for detecting the pH value in real time; and the control unit is used for dynamically adjusting the opening degree of each valve by adopting an improved fuzzy self-adaptive PID control algorithm according to a detection result of the pH sensor so as to control the pH value to be within a target range. According to the scheme, the problems of overshoot and lag caused by traditional fixed parameter PID adjustment are solved, and therefore the stability of the pH value of the solution and the consistency of the technology in the germanium oxide production process are guaranteed.

The invention relates to the technical field of automatic control, in particular to a monitoring method and system for synthesizing ceramide based on alpha-hydroxy fatty acid, and the monitoring system for synthesizing ceramide based on alpha-hydroxy fatty acid comprises a raw material feeding module, a reaction control module, a quenching-crystallization joint control module and a data integration module; carrying out dynamic weighing monitoring on the raw materials based on the received synthesis instruction, and starting a reaction kettle according to weighing data; performing multi-dimensional data acquisition in real time according to the set reaction data, and performing dynamic feeding control according to the set reaction data; when the TLC detection substrate reaction is completed, the cooling process and the crystallization process are regulated and controlled in real time according to the reaction data until the end point judgment standard is met; according to a received synthesis completion instruction, product quality data is obtained, a monitoring data packet is generated, the synthesis instruction is marked and then stored, process control is accurately monitored and controlled, and the purity and crystal form of the product are ensured.

Polymers synthesized by solid-phase synthesis are selectively released from a solid support by reversing the bias of spatially addressable electrodes. Change in the current and voltage direction at one or more of the spatially addressable electrodes changes the ionic environment which triggers cleavage of linkers that leads to release of the attached polymers. The spatially addressable electrodes may be implemented as CMOS inverters embedded in an integrated circuit (IC). The IC may contain an array of many thousands of spatially addressable electrodes. Control circuity may independently reverse the bias on any of the individual electrodes in the array. This provides fine-grained control of which polymers are released from the solid support. Examples of polymers that may be synthesized on this type of array include oligonucleotides and peptides.

The invention relates to the technical field of guanidine nitrate preparation, in particular to a method for preparing guanidine nitrate by a continuous dynamic tubular reaction process, which comprises the following steps: uniformly mixing dicyandiamide, target ammonium nitrate and target ammonium carbonate according to a mass ratio of 1: (1-3): (1-0.5); conveying the uniformly mixed material to a feeding section in a dynamic tubular reactor through a first conveying screw rod for mixing treatment, wherein the dynamic tubular reactor further comprises a heating section, a reaction section and a cooling section; sequentially conveying the target mixed material to a heating section for heating melting treatment, a reaction section for synthesis reaction treatment and a cooling section for cooling forming treatment through a second conveying screw rod to obtain an initial product; conveying the initial product into a cooling and crushing device for cooling and slicing to obtain a target guanidine nitrate product. According to the method disclosed by the invention, the mass and heat transfer efficiency can be improved, the online quantity and liquid holdup of the material are reduced, meanwhile, the raw material ratio and the reaction path are optimized, and the safety and the product purity are improved.

The present application relates to a multiphase reactor. The multiphase reactor comprises: a reactor housing in which a reaction cavity is formed, wherein the reactor housing is provided with a second material inlet pipe and first material inlet pipes communicated with the reaction cavity, and the first material inlet pipes are used for conveying a first material to the reaction cavity; a gas distributor located in the reaction cavity, wherein the second material inlet pipe is communicated with the gas distributor, and a second material conveyed by the second material inlet pipe is conveyed to the reaction cavity by means of the gas distributor; and flow guide cylinders located in the reaction cavity, wherein a plurality of ventilation parts are arranged on each flow guide cylinder in the circumferential direction of the reactor housing, and the flow guide cylinders are used for axial drainage and radial cutting in the reaction cavity. The present application solves the technical problems that the reaction efficiency is affected and the material consumption is increased due to uneven distribution of a temperature field and a reaction field in multiphase reactors.

The invention discloses a device for continuously preparing adiponitrile from adipic acid by supergravity, which is characterized in that a specially designed gas-in-liquid mixed feeding mode is firstly adopted, so that liquid of a falling film assembly is uniformly dispersed as far as possible, and meanwhile, by accurately controlling the reaction temperature in the falling film assembly, side reactions are reduced; secondly, the contact mode of gas and liquid of the falling film assembly is changed, the gas-liquid countercurrent contact mode is changed into gas-liquid parallel flow, and the liquid is prevented from being stopped in a pipeline through the gas-liquid parallel flow; and finally, mixing and mass and heat transfer effects of adipic acid and ammonia molecules in the reaction process are enhanced by using a supergravity assembly, so that adipic acid decomposition and coking in a bubbling section of a traditional reactor are effectively slowed down, the reaction efficiency and the product yield are improved, and side reactions are reduced.

The invention relates to the technical field of chemical automation control, and discloses an intelligent closed-loop control system for producing p-dichlorobenzene by a biomass method, which comprises a signal acquisition module, a residence time reconstruction module, a thermal coupling analysis module, a parameter self-adaptive scheduling module and an execution control module. The rheological characteristics of raw materials are monitored by collecting the current of a stirring motor, the liquid level is dynamically increased through a retention time reconstruction module to prolong the retention time of the materials, and a liquid level periodic migration strategy is introduced to prevent scaling of a gas-liquid interface; the thermal coupling analysis module and the parameter self-adaptive scheduling module are used for calculating thermal retardation post factors, temperature control parameters are corrected in real time, the upper limit of cooling output is limited, inner wall supercooling crystallization is prevented, and the problems that the conversion rate is reduced, the heat transfer efficiency is reduced and equipment is hung on the wall due to viscosity fluctuation of biomass raw materials are effectively solved. And the self-adaptive stable control of the reaction process is realized.

The invention relates to the technical field of chemical reaction equipment, in particular to a reaction device for synthesizing high-molecular N-halamine resin, which comprises a viscosity adjusting mechanism, the viscosity adjusting mechanism comprises a detection plate for detecting viscosity, a first permanent magnet is embedded in the detection plate, a second permanent magnet is magnetically adsorbed by the first permanent magnet, and a second permanent magnet is embedded in the second permanent magnet; the top end of the second permanent magnet is provided with a magnetism isolating plate, and the top end of the magnetism isolating plate is fixedly connected with a conducting strip. The viscosity of the resin is fed back by detecting the movement distance of the detection plate, when the viscosity of the resin is increased, the friction force between the resin and the detection plate is also increased, the detection plate moves towards the side away from the connecting spring, and the movement drives the second permanent magnet and the conducting strip to slide on the resistance plate. And through a current monitor in the PLC, the current change of the slide rheostat can be detected, so that the viscosity of the resin is monitored in real time.

The invention discloses a continuous production process of a CO2-based multipolymer, and belongs to the technical field of polycarbonate synthesis. The technological process comprises the following steps: firstly, preparing an auxiliary agent, a solid-state monomer, a liquid-state reaction monomer and any solvent into a mixed solution in a premixer (1); continuously feeding carbon dioxide and the mixed solution into a multi-stage continuous reactor for mixing and heating to initiate a reaction, wherein the total reaction residence time of the materials in the multi-stage continuous reactor is controlled to be 10 minutes to 5 hours; and after the reaction is completed, carrying out post-treatment to complete the continuous production of the CO2-based multipolymer. The process particularly optimizes the effective continuous polymerization of high-molecular and high-viscosity materials of the CO2-based multipolymer. Through accurate control of the multi-stage tubular reactor, appropriate reaction viscosity is realized, further reaction uniformity of materials in the screw extrusion reactor is ensured, and reaction efficiency is improved.

The invention relates to the technical field of chemical rectification equipment, in particular to a method and device for improving rectification purity by adjusting the reflux ratio, and the method comprises the following steps: determining the total reflux position and the total extraction position of a liquid separation module; an initial position is set, and the liquid separation module is deflected to the initial position; collecting distillate and analyzing the purity of the distillate; the obtained purity is compared with the set purity, and the deflection direction of the liquid separation module is determined; the liquid separation module is adjusted to deflect towards the determined deflection direction; the measurement position is obtained until the purity of the distillate reaches the maximum; and performing rectification treatment on the to-be-treated liquid according to the screened measurement position so as to improve the rectification purity of the to-be-treated liquid. Through mutual cooperation of all the units, multi-point adjustment of the swing position of the liquid separation module between total reflux and total extraction can be realized, so that the reflux ratio is accurately controlled, and the rectification purity is improved.

Disclosed herein are cell processing systems, devices, and methods thereof. A system for cell processing may comprise a plurality of instruments each independently configured to perform one or more cell processing operations upon a cartridge, and a robot capable of moving the cartridge between each of the plurality of instruments.

The invention relates to the technical field of pyrolysis gas treatment, in particular to a biomass pyrolysis gas self-heating reforming hydrogen production system which comprises a pyrolysis gas reforming hydrogen production subsystem and a thermochemical self-heating subsystem. Wherein the pyrolysis gas reforming hydrogen production subsystem can realize reforming quality improvement of pyrolysis gas to obtain high-purity hydrogen. On one hand, the thermochemical self-heating subsystem provides energy for the reforming hydrogen production reaction through an exothermic reaction of calcium oxide and carbon dioxide, and continuous and efficient operation of the reforming hydrogen production reaction is achieved; on the other hand, primary separation and quality improvement of the reformed gas can be realized, and the energy of the pyrolysis gas which is difficult to store and transport and has low utilization value is stored in calcium oxide. Through organic coupling of biomass pyrolysis gas reforming hydrogen production and thermochemical heat storage, self-heat-supply upgrading utilization of biomass pyrolysis gas and low-cost preparation of green hydrogen are achieved, and the device has the advantages of being high in energy utilization rate, high in treatment efficiency, convenient to operate and control, high in applicability and the like.

The invention relates to a safety early warning method and system for continuous production of hydrolytic polymaleic anhydride, and the method comprises the steps: L1, in the continuous production process of hydrolytic polymaleic anhydride, obtaining the data information of the temperature of a reaction kettle in real time based on a temperature sensor on the reaction kettle, data information of pressure of the reaction kettle is acquired in real time based on a pressure sensor on the reaction kettle, data information of rotating speed of a stirrer in the reaction kettle is acquired in real time based on a tachometer on the reaction kettle, and data of temperature and pressure of the reaction kettle and data of the rotating speed of the stirrer are fused by adopting an improved multi-modal model level fusion algorithm. And constructing a combined characteristic matrix of the reaction kettle. According to the invention, the operation state of the reaction kettle can be accurately predicted in advance, and safety early warning is carried out, so that the quality of the product is ensured to meet the standard, the whole monitoring process does not need manual participation, the manual error is reduced, and the production efficiency of hydrolytic polymaleic anhydride is improved.

The invention discloses a homogeneous reaction and separation integrated hydrothermal upgrading device for industrial byproduct gypsum, and belongs to the technical field of slurry reaction devices under high temperature and high pressure. The device is characterized in that an elliptical head is arranged on one side of a reaction device barrel, a slurry inlet pipeline and a steam pipeline are arranged on the elliptical head, stirring blades and turbulent flow blades are arranged on the inner wall of the elliptical head, and an inner screw rib type stirring and conveying assembly is fixed in the reaction device barrel; the solid-liquid separation unit is arranged on the other side of the reaction device barrel, and a slurry baffle plate is arranged at the upper end of the joint of the reaction device barrel and the solid-liquid separation unit; one end of the steam heating device is connected with the elliptical head, and the other end is arranged along the axial direction of the reaction device barrel; and the water separation discharging device is arranged on the solid-liquid separation unit. The device provided by the invention not only can ensure that the slurry is rapidly heated and pressurized, but also can keep good homogeneity of the slurry, and can produce partially dehydrated gypsum slurry, so that the economical efficiency of the whole process and the system integration are improved.