11786results about "Chemical industry" patented technology

A recovery treatment apparatus for trichloroethane in sucralose production. The rotation of an output shaft of a motor (7) drives multiple gas suction assemblies (31) to rotate, so that a negative pressure environment is formed, and the transmission of tail gas from the bottom of a water washing tower (1) into a gas guide pipe (2) is accelerated; and at this time, multiple atomizing nozzles (19) spray mist and the mist is sprayed to the tail gas passing through a sieve plate (23), then HCl gas in the tail gas is absorbed when in contact with water, thereby achieving the effect of purifying toxic gas HCl. Along with the rotation of a rotating rod (10), a collar (12) further drives L-shaped connecting rods (14) and turning blocks (15) to turn filter materials, so that collision and displacement occur between the filter materials; and at this time, particulate impurities adsorbed on the surfaces of the filter materials are cleaned under the flow of water vapor, and meanwhile, the vibration generated by dynamically moving filter materials can also cause the adsorbed particulate impurities to be shaken off. Thus, the continuous purification and adsorption effect of filter materials is improved, and the service cycle of filter materials can be prolonged at the same time.

The invention discloses a preparation method and application of a vertically-oriented boron nitride / epoxy resin heat-conducting composite material under a magnetic field, and belongs to the field of composite materials. The invention aims to solve the problems of high cost, complex process and narrow application range of the existing filler directional arrangement method. The method comprises the following steps: 1, preparing a mixed solution of boron nitride and ferroferric oxide; 2, preparing a boron nitride nanosheet solution with ferroferric oxide attached to the surface; (3) preparing BNNS coated Fe3O4; and 4, preparing the vertically-oriented boron nitride / epoxy resin heat-conducting composite material under the magnetic field. The invention relates to application of a vertically-oriented boron nitride / epoxy resin heat-conducting composite material in electronic packaging under a magnetic field. The heat conductivity of the epoxy resin can be effectively improved, the process is simple and reliable, the efficiency is high, the cost is low, the heat conductivity coefficient is high, and the method can be applied to electronic packaging.

The invention relates to the field of electric heating materials, and provides a graphene-based heating coating and a preparation method thereof. The coating is prepared from functionalized graphene, a surface modified bismuth telluride nanobelt, polyaniline, bisphenol A epoxy acrylate, polyurethane acrylate, a dispersing agent, a flatting agent, a silane coupling agent, a defoaming agent and a propylene glycol methyl ether acetate / N-methyl pyrrolidone mixed solvent. The functionalized graphene is obtained by modifying a hyperbranched polyolefin-acryloyl-POSS copolymer, and carrying out ultrasonic stripping, centrifugal separation, gradient washing and vacuum drying; the surface-modified bismuth telluride nanobelt is modified by an amino silane coupling agent, so that the interfacial compatibility is improved. The preparation method comprises the steps of solvent premixing, nanofiller dispersion, ultrasonic homogenization, coupling agent modification, ultraviolet curing and thermocuring. The heating coating provided by the invention has high conductivity, excellent thermal stability and adhesive force, and can be widely applied to heating electric appliances and intelligent temperature control equipment.

The invention discloses a phosphorus oxyfluoride reaction and separation integrated preparation tower, and belongs to the field of industrial equipment for phosphorus oxyfluoride preparation, the preparation tower comprises a tower body, the tower body is provided with a feeding area, a reaction area and a separation area, the feeding area and the separation area are both filled with filler sections of filler, a first feeding port is formed in the bottom of the filler section in the feeding area, and a second feeding port is formed in the bottom of the reaction area. A tubular heat exchanger is arranged in each reaction zone, a threaded pipe is arranged on each tubular heat exchanger, filler is also filled between the threaded pipes, a second feeding hole is formed in the upper part of the reaction zone on the top layer, and polyphosphoric acid and anhydrous hydrogen fluoride are contacted in the reaction zones to form a concentration stepped reaction and a temperature stepped reaction; and the phosphorus oxyfluoride gas generated after the reaction is fractionated through the filler section on the separation area and enters the next process from the top of the tower body. According to the invention, the reaction and separation of phosphorus oxyfluoride production are integrated, the energy consumption of phosphorus oxyfluoride production is reduced, the production cost is reduced, and the reaction yield is improved.

The invention discloses a rectifying tower for producing furanone, and relates to the technical field of rectifying tower condensers. According to the rectifying tower for producing furanone, when steam is condensed, the flowing speed of cooling water can be reduced, the path of the cooling water can be increased, meanwhile, the cooling water between the partition plate assemblies can be stirred in a reciprocating mode, the heat absorption efficiency of the cooling water is higher, the heat absorption effect of the cooling water is better, and then the condensation efficiency and effect are improved; when the flow speed of the steam is too high, the speed of the steam can be limited, and when the flow speed of the steam is relatively low, air extraction operation can be carried out to accelerate the steam in the tower body to thoroughly enter the condenser assembly for condensation operation, so that the condensation efficiency and effect can be improved; a condenser pipe can be knocked and vibrated in a reciprocating manner, so that condensed furanone liquid is prevented from being attached to the inner wall, and the collection effect is better; and before the cooling water enters the heat exchanger, the cooling water can be pre-cooled, so that the subsequent cooling efficiency and effect of the heat exchanger are improved.

The invention relates to the technical field of dielectric material preparation, in particular to a preparation method of a polymer dielectric film. The preparation method comprises the following steps: in an inert atmosphere, mixing a diamine monomer, a dianhydride monomer and an organic solvent, and carrying out condensation polymerization to obtain a precursor solution; wherein one of the diamine monomer and the dianhydride monomer contains benzyl groups; and carrying out imidization reaction and benzyl free radical cross-linking reaction on the precursor solution to obtain the polymer dielectric film. The glass transition temperature (Tg) of the polymer dielectric film prepared by the preparation method is improved, the modified film has excellent breakdown electric field and energy storage density in a high-temperature environment of 250 DEG C, and other complicated and high-technical-content processes are not added on the basis of a process for synthesizing a commercial polymer dielectric film; vacuum environment crosslinking is not needed, environmental protection and energy saving are achieved, the reaction degree is controllable, the surface of the prepared polymer dielectric film is smooth, and the cross section has no obvious defects.

The present disclosure relates to a gas turbine plant which decomposes ammonia and supplies it as fuel to a combustor of the gas turbine. The gas turbine plant supplies sufficient heat to the ammonia in order to thermally decompose the ammonia effectively, and separates the residual ammonia present in the decomposition gas and supplies it to a combustor of the gas turbine.

The invention discloses a stirring device for fine chemical engineering and relates to the technical field of fine chemical engineering, the stirring device comprises a stirring tank and further comprises a stirring device, a feeding pipe is fixedly mounted at the top of the stirring tank, a discharging pipe is fixedly mounted at the bottom of the stirring tank, and a fixing plate is fixedly mounted at the top of the stirring tank; a rotating motor is fixedly installed at the top of the fixing plate, a rotating rod is fixedly installed at the output end of the rotating motor and rotationally penetrates through the top of the inner wall of the stirring tank, and an extrusion rod moves upwards to make contact with a displacement ring A and extrudes the displacement ring A to move upwards; the displacement ring A moves upwards to drive the stirring rod to move upwards to stir materials at different depths in the stirring tank, so that the materials at different depths can be uniformly mixed by stirring the materials at different depths in the stirring tank, uniform distribution of various materials in the stirring tank is ensured, and the mixing quality and efficiency of the materials are improved.

The invention relates to a preparation method of spherical silicon dioxide micropowder with ultralow dielectric loss. The preparation method comprises the following steps: preparing an organic silicon polymer; preparing slurry; performing solid-liquid separation on the synthetic slurry to obtain concentrated slurry, and drying the concentrated slurry to obtain spherical silica powder; carrying out low-temperature heat treatment on the obtained spherical silica powder at 1500-7000 DEG C for h to remove residual organic matters and free water in the powder; then, high-temperature densification is carried out at the temperature of 3000-28000 DEG C for h, and moisture is further removed; adding a modifier into the stirring equipment for surface modification; and after surface modification, drying at 55-300 DEG C for h, and removing modified micromolecular byproducts to obtain the spherical silicon dioxide micro powder with ultralow dielectric loss. The method is simple in production process, short in production period, low in production cost, high in yield and capable of effectively reducing the dielectric loss of the spherical silicon dioxide micro powder.

The invention discloses a high-thermal-conductivity radiation refrigeration coating material and a preparation method thereof, and belongs to the technical field of coating materials. The preparation method of the high-thermal-conductivity radiation refrigeration coating material comprises the following steps: coating the surfaces of SiO2 hollow sphere particles subjected to surface amination with surface hydroxylated hBN nanosheets to obtain hollow SiO2 (at) hBN composite particles; the preparation method comprises the following steps: adding surface hydroxylated hBN micron sheets and hollow SiO2-coated hBN composite particles into a solvent containing a dispersant, uniformly dispersing to obtain a raw material solution, then adding a solution of a polymer substrate into the raw material solution, uniformly dispersing, and coating to obtain the high-thermal-conductivity radiation refrigeration coating material. The high-thermal-conductivity radiation refrigeration coating material prepared by the invention has relatively high thermal conductivity and an excellent radiation refrigeration effect, and is suitable for the field of thermal management of electronic devices.

The invention relates to a deicing super-hydrophobic coating based on MXene, a coating, a preparation method and application of the coating. The coating comprises the following components in percentage by mass: 2%-5% of a super-hydrophobic modified MXene photo-thermal material, 2%-5% of epoxy resin, 0.5%-1.5% of an epoxy resin curing agent, 0.5%-1.5% of PDMS, 0.05%-0.15% of a PDMS curing agent and 80%-90% of a diluent. Wherein the super-hydrophobic modified MXene photo-thermal material is MXene powder treated by fluorine-free long-chain silane, and the super-hydrophobic modified MXene photo-thermal material is a super-hydrophobic modified MXene photo-thermal material. MXene with excellent photo-thermal conversion performance is used as a photo-thermal material, fluorine-free long-chain silane is used for performing low-surface-energy hydrophobic modification on the MXene material, environmental pollution caused by perfluorinated or polyfluorinated organic compounds is avoided, photo-thermal performance and super-hydrophobic performance are integrated, the advantages of a super-hydrophobic coating and a photo-thermal coating are integrated, and the application prospect is wide. The deicing super-hydrophobic coating based on MXene can be used for passive ice prevention and active photo-thermal deicing.

The utility model relates to a blanking pipe dredging device for rosin resin conveying, which comprises a pipe body, a side shell is fixedly sleeved on the peripheral surface of the pipe body, the side shell is filled with heat conducting oil, a heater is fixedly connected to the peripheral side of the side shell, an upper pipe is fixedly arranged at the upper half part of the pipe body in a penetrating manner, and two ends of the upper pipe extend into the side shell. A rotating pipe is arranged in the pipe body, the upper half portion of the rotating pipe extends into the upper pipe, the rotating pipe is rotationally connected with the upper pipe, a driving part is arranged below the rotating pipe, and a heat conduction part is arranged in the rotating pipe. The utility model relates to the technical field of rosin resin conveying. The first water pump works to drive high-temperature heat conduction oil to circularly flow in the rotating pipe and the side shell, the peripheral side of rosin resin in the pipe body is subjected to heat conduction of the heat conduction oil in the side shell, the interior of the rosin resin is subjected to heat conduction of the heat conduction oil in the rotating pipe, and therefore the temperature rising speed of the rosin resin is increased, and the discharging speed is increased.

The invention belongs to the technical field of polymer heat conduction, and particularly relates to a preparation method of a high-heat-conductivity polymer with modified boron nitride as filler, which comprises the following steps: (1) dissolving boron nitride nanosheets into tetrahydrofuran, ultrasonically dispersing uniformly, adding a modifier for reaction, then removing tetrahydrofuran by using a rotary evaporator, transferring into deionized water, and drying to obtain a boron nitride nano-sheet; drying to obtain a modified boron nitride nanosheet; (2) dispersing carbon nanotubes in deionized water, stirring and carrying out ultrasonic treatment, adding the modified boron nitride nanosheets, and then carrying out freeze orientation treatment and freeze drying treatment to obtain a porous foamed composite heat-conducting filler; and (3) carrying out melt blending on the composite heat-conducting filler and polyethylene glycol terephthalate, and carrying out hot press molding to finally prepare the modified high-heat-conductivity polymer. According to the invention, the composite heat-conducting filler improves the interfacial compatibility and dispersity with a polymer matrix, and reduces the interfacial thermal resistance of the composite material, so that the modified polymer has good application in the aspect of heat dissipation of electronic equipment.

The present invention relates to the technical field of solvent purification, and discloses a propylene glycol methyl ether acetate purification control method and a propylene glycol methyl ether acetate purification process, the propylene glycol methyl ether acetate purification control system comprises a rectification device and a rectification control system, the rectification device comprises a rectification tower, a raw material preheater, a condenser, a reflux tank and a reboiler, the rectification control system comprises an environment temperature measuring unit, a tower top temperature measuring unit, a tower bottom temperature measuring unit, a feeding temperature measuring unit and a regulation and control module, the rectification control system is pre-trained with a parameter prediction model, and the parameter prediction model takes the environment temperature, the tower top temperature, the tower bottom temperature and the feeding temperature as input to output regulation and control parameters. The regulation and control parameters comprise the opening degree of a steam valve, the power of a condenser and the opening degree of a return valve, a primary distribution controlled parameter is obtained according to a preset distribution strategy, the primary distribution controlled parameter is specifically the optimized regulation and control parameter, and the tower top temperature is controlled within a preset tower top temperature range according to the primary distribution controlled parameter.

The invention relates to a preparation method of a radiation refrigeration coating with super-hydrophobic performance. According to the method, hydrophobic modified nano-particles and nano-particles with high reflectivity and high emissivity are blended in an adhesive solution, an adhesive is separated out to form a micron-sized aggregate through a non-solvent induced phase separation technology, and meanwhile, various nano-particles are uniformly coated on the surface of the aggregate, so that a stable suspension system is prepared. The radiation refrigeration coating has excellent radiation refrigeration performance, excellent super-hydrophobicity and good durability, the preparation process is simple, the radiation refrigeration coating is suitable for large-scale industrial application of outdoor scenes such as building outer walls, and a new technical solution is provided for developing efficient and lasting radiation refrigeration materials.

The invention discloses a preparation method of a high-dispersion and high-thermal-conductivity filler based on carbon black, and relates to the technical field of carbon black modification, and the preparation method specifically comprises the following steps: treating carbon black in a first acid solution to obtain activated carbon black; treating the single-walled carbon nanotube in a second acid solution to obtain an activated single-walled carbon nanotube; treating the activated single-walled carbon nanotube with a sulfanilamide solution to obtain a functionalized single-walled carbon nanotube; placing the graphene nanosheets in a third acid solution for treatment to obtain activated graphene nanosheets; the preparation method comprises the following steps: mixing amino silane hydrolysate and epoxy silane hydrolysate, adding activated carbon black, functionalized single-walled carbon nanotubes and activated graphene nanosheets, and treating to obtain a pre-modified filler; amino acid and a cross-linking agent are pre-polymerized to obtain an amino acid pre-polymerized solution, and the pre-modified filler is treated by the amino acid pre-polymerized solution to obtain the high-dispersion and high-thermal-conductivity filler. The method disclosed by the invention is simple to operate and low in energy consumption, the prepared filler is good in thermal conductivity and good in dispersity in a polymer matrix, and the thermal conductivity and the mechanical property of a polymer are greatly improved.

The invention belongs to the technical field of carbon-carbon heaters, and particularly relates to a preparation method of a carbon-carbon heater. The preparation method of the carbon-carbon heater comprises the following steps: carrying out first vacuum filtration on a dispersion liquid of short carbon fibers in a mold, adding a mixed liquid of phenolic resin and ethanol into the mold, carrying out second vacuum filtration, demolding, curing and molding, dipping an obtained carbon-carbon heater blank in asphalt or phenolic resin, and carbonizing to obtain the carbon-carbon heater. The obtained carbonized blank is subjected to graphitization treatment, vapor deposition densification and purification treatment, and the carbon-carbon heater is obtained. Through vacuum filtration forming, manual knitting errors can be avoided, the uniformity of the product is better, and the conductivity of the prepared carbon-carbon heater is good. And meanwhile, large-batch production can be realized, the productivity is higher, the labor cost is saved, and time and labor are saved. The preparation method is low in raw material consumption, low in cost and convenient to operate, and the carbon-carbon heater is good in integrity, low in impurity content and good in conductivity and mechanical property.

The present invention provides a silane cross-linked polyethylene insulating material for heating cables and a preparation method thereof, wherein the insulating material is prepared by mixing the following raw materials in parts by weight: 70-100 parts of polyolefin resin; 1.5-2.5 parts of silane cross-linking agent; 0.3-0.6 parts of grafting initiator; 0.2-0.6 parts of first lubricant; 0.1-0.3 parts of first antioxidant; 1.0-2.5 parts of cross-linking catalyst; 0.2-0.5 parts of second lubricant; 0.1-0.3 parts of second antioxidant; 5-15 parts of ethylene-vinyl acetate copolymer; 0.5-2 parts of maleic anhydride grafted polyethylene; 0.1-0.3 parts of ultraviolet absorber; 0.1-0.3 parts of antistatic agent. The preparation method includes mixing, melt blending, extrusion granulation, cross-linking molding and cooling and shaping. The finished product of the present invention has better performance, more stable production and more competitive cost.

The invention provides a preparation device and process of electronic-grade silane. According to the preparation device, a first disproportionation reaction is carried out on the basis of the first reactor, dichlorosilane is rectified and separated to serve as a raw material for a second disproportionation reaction, silane can be obtained on the basis of cheap trichlorosilane and a catalytic reagent, and electronic-grade silane can be obtained on the basis of traditional purification after rectification; based on heat exchange between tower top materials of the rectifying tower I and a tower kettle reboiler of the rectifying tower II, differential pressure thermal coupling integration is realized, condensing equipment and operation steps can be omitted, energy consumption is reduced, and the defects of high preparation cost and high energy consumption of a silane preparation device in the prior art are overcome.

The utility model discloses a shell-and-tube efficient heat exchanger which comprises a heat exchanger body and a first liquid inlet tube, the bottom of the first liquid inlet tube is fixedly installed on the top of a tube box, the first liquid inlet tube comprises a communicating tube, a connecting tube, a pressing block, a filter plate, a connecting block and a clamping mechanism, and the bottom of the communicating tube is fixedly installed on the top of the tube box. The inner wall of the bottom of the connecting pipe and the top of the communicating pipe are slidably mounted, the top of the pressing block and the inner surface of the connecting pipe are fixedly mounted, the top of the pressing block and the interior of the communicating pipe are slidably mounted, the outer surface of the filter plate and the interior of the communicating pipe are clamped, the side face of the top of the connecting block and the outer surface of the connecting pipe are fixedly mounted, and the clamping mechanism is arranged on the surface of the communicating pipe. A clamping mechanism is arranged, a pull rod is transversely pulled, a U-shaped rod and a clamping column are driven to horizontally move and are separated from the interior of a connecting block, then a connecting pipe is moved upwards, the connecting pipe is separated from a communicating pipe, impurities on the surface of a filter plate are cleaned, and the situation that the filter plate is blocked after the impurities are accumulated, and the injection rate of fluid is affected is avoided.

The invention provides a continuous purification method of crude acetonitrile, and belongs to the field of acetonitrile purification. The continuous purification method of the crude acetonitrile comprises the following steps: rectification light component removal, membrane separation impurity removal, adsorption impurity removal and rectification purification. According to the continuous purification method of the crude acetonitrile, continuous purification of the crude acetonitrile can be realized, and meanwhile, the problems that new impurities are introduced by side reactions, the rectification efficiency and the rectification stability are influenced by treated products and the device is influenced by over-high alkalinity of the treated secondary rectification liquid due to the fact that sodium hydroxide and formaldehyde are adopted to treat the rectification liquid are avoided; the acetonitrile product with the purity meeting the requirement is prepared by continuously purifying the crude acetonitrile.

The utility model provides an emission reduction system for producing tetrahydrofuran from 1, 4-butanediol, and relates to the technical field of chemical production equipment. By arranging the 1, 4-butanediol raffinate separation unit, the 1, 4-butanediol raffinate generated in the tetrahydrofuran production unit can directly enter the film evaporator to be separated, the light component 1, 4-butanediol is rapidly evaporated and flows out from the first gas phase outlet, and the light component 1, 4-butanediol is condensed by the gas phase condenser and then returns to the tetrahydrofuran production unit to serve as a raw material to be recycled. And heavy components of tar in the film evaporator flow out from a first liquid phase outlet at the bottom and are discharged and incinerated. The system can further separate the 1, 4-butanediol raffinate generated in the tetrahydrofuran production unit, and recycle the 1, 4-butanediol in the raffinate, so that the material waste of the 1, 4-butanediol is reduced, and the utilization rate of the 1, 4-butanediol raw material is improved. And meanwhile, the 1, 4-butanediol residual liquid discharge incineration treatment amount is greatly reduced, energy conservation and emission reduction are achieved, and the production cost is reduced.

The invention belongs to the technical field of micro-reaction, and particularly relates to a micro-mixer and a method for continuously preparing nano cooling liquid. Comprising a reaction cavity in which a plurality of reaction flow channels are arranged, all the reaction flow channels are used for preparing nano cooling liquid and are vertically arranged in the reaction cavity in a three-dimensional spiral shape, and each reaction flow channel is internally provided with a plurality of disturbance structures and a plurality of distributors which are arranged in the reaction cavity and located above all the reaction flow channels, each distributor is connected with the inlets of all the reaction flow channels, the collectors are arranged at the outlets of all the reaction flow channels, and pressure regulating structures are arranged in the collectors. According to the invention, the distributor is adopted to enable the reaction fluid to flow into the corresponding reaction flow channel, the three-dimensional spiral flow channel design in the reaction cavity is folded in space, so that the overall size of the microreactor is not too large, and a disturbance structure is arranged in each reaction flow channel, so that the mixing efficiency can be further improved; the production rate of the microreactor is improved, and blockage in a flow channel is avoided.

The utility model discloses a polycrystalline reduction starting device and a microwave power supply heating system, and relates to the technical field of polycrystalline silicon, a polycrystalline reduction furnace comprises a reduction furnace base and a bell jar which are detachably connected, the polycrystalline reduction starting device is characterized in that the tail of a microwave energy feedback device is connected with a microwave transmission device, and the microwave transmission device is used for being connected with a microwave emission device; the microwave energy feedback device is installed on the surface of the bell jar and guides microwave energy into the polycrystalline reduction furnace to heat the silicon core. The microwave energy feedback device introduces microwave energy into the reduction furnace to heat the silicon core, so that the resistance value of the silicon core can be reduced, the silicon core can be subsequently subjected to breakdown start with lower voltage, microwave heating can be started at low voltage, the phenomenon of discharge sparking in the reduction furnace is avoided, an insulating part at the bottom of the reduction furnace is prevented from being damaged, and safe operation of equipment can be ensured; and other materials or impurities cannot enter the reduction furnace through microwave heating, so that the environment of the reduction furnace is prevented from being polluted, and the purity of generated polycrystalline silicon is prevented from being reduced.

The invention belongs to the technical field of chemical production, and particularly relates to an efficient energy-saving refining system for producing cyclohexanone through dehydrogenation, which comprises an alcohol tower, a dehydrogenation heat exchanger, a dehydrogenation reactor, an alcohol tower feeding heat exchanger, a dehydrating tower, a light tower I, a light tower II, a ketone tower and an alcohol recovery tower which are connected in sequence, a middle feeding port of the alcohol tower is communicated with a tube pass discharging port of the alcohol tower feeding heat exchanger, a top discharging port of the alcohol tower is communicated with a tube pass feeding port of the dehydrogenation heat exchanger, a bottom discharging port of the alcohol tower is communicated with a middle feeding port of the alcohol recovery tower, and an alcohol ketone drying tower is additionally arranged between the alcohol tower feeding heat exchanger and the dehydration tower. A feed port of the alcohol ketone drying tower is communicated with a shell pass discharge port of the alcohol tower feed heat exchanger, and a liquid phase discharge port of the alcohol ketone drying tower is communicated with an upper feed port of the dehydrating tower. The alcohol tower adopts a process that raw materials directly enter the tower top, tower top reflux is cancelled, steam consumption is reduced, and the purpose of saving energy is achieved.

The invention provides a graphene-boron nitride composite epoxy resin material and a preparation method thereof, the surface of a graphene-boron nitride filler is modified to obtain a filler with magnetic response, the filler is added into epoxy resin, and the filler can be in more sufficient contact and ordered arrangement under the action of an external magnetic field, so that the graphene-boron nitride composite epoxy resin material is obtained. The heat conductivity coefficient of the composite material is effectively improved. Tests show that when the filler accounts for 25%, the heat conductivity coefficient reaches 2.1 (W / mk), and the friction coefficient can be effectively reduced and is reduced by about 30% compared with pure epoxy resin. The research of the invention provides a new thought and method for preparing the epoxy resin-based composite material with high heat-conducting property, expands a new field and direction for the application of epoxy resin in the field of electronic packaging, and has practical significance.

The invention discloses a chemical heat exchanger with energy-saving improved structural design, which comprises a heat exchange tank body, a connecting disc is fixedly mounted at the end part of the heat exchange tank body, a tank cover is arranged on one side, far away from the heat exchange tank body, of the connecting disc, and a processing assembly is arranged on the inner side of the tank cover. When the heat exchanger is used, dirt generated by liquid can adhere to the interior of the heat exchange tank body and needs to be cleaned, at the moment, a waterproof motor is started, a rotating rod fixedly installed at the output end of the waterproof motor starts to rotate, and a limiting ring fixedly installed at the end of the rotating rod drives a reciprocating lead screw to rotate along with the reciprocating lead screw; the rotating reciprocating lead screw drives the sleeve plate arranged on the outer wall of the reciprocating lead screw in a sleeving mode to move in a reciprocating mode, the sleeve plate drives the scraping ring to slide on the outer wall of the heat exchange pipe through the extrusion rod, and due to the fact that the scraping ring is attached to the outer wall of the heat exchange pipe to slide, dirt attached to the outer wall of the heat exchange pipe can be cleaned.

The invention discloses a boiler water energy-saving and emission-reducing agent, and relates to the technical field of boiler energy conservation, and the boiler water energy-saving and emission-reducing agent is prepared from the following components: 1, 3-bis ((trihydroxymethyl) methylamino) propane, sodium lignin sulfonate, caffeine, (3, 6-diamino-9-acridinyl) boric acid, a functional copolymer, sodium glycyrrhizinate, hydroxypropyl beta-cyclodextrin and deionized water. The functional copolymer comprises a structural unit introduced by the following monomers: N-acryloyl morpholine, 3-[N, N-dimethyl-[2-(2-methylpropyl-2-enoyloxy) ethyl] ammonium] propane-1-sulfonic acid inner salt, N-trihydroxymethyl methacrylamide, and 2-[3-(2H-benzotriazole-2-yl)-4-hydroxyphenyl] ethyl 2-methacrylate. The agent has remarkable scale and corrosion inhibition effects, is safe and environment-friendly to use, and has good energy-saving and emission-reducing effects.

The utility model relates to the technical field of shell-and-tube heat exchangers, and particularly discloses a multi-pipe-diameter multi-helix-angle multi-strand winding pipe type heat exchanger. Comprising a shell, a middle core cylinder installed in the shell and a spiral assembly spirally wound on the outer side of the middle core cylinder in the axial direction of the middle core cylinder. The spiral assembly comprises a plurality of spiral winding tube bundle layers which are spirally wound on the outer side of the middle core cylinder in sequence; each spiral winding tube bundle layer comprises a plurality of groups of spiral winding tubes wound on the outer side of the middle core cylinder, and the outer diameters of the spiral winding tubes in each spiral winding tube bundle layer are arranged at equal intervals; one or more fluid media are arranged in the spiral winding pipes on the same layer, and one or more wall thicknesses of the spiral winding pipes are arranged and correspond to the fluid media in a one-to-one mode. The heat exchange requirement and the winding strength requirement can be effectively met, meanwhile, the use efficiency of the material can be improved, and the production and processing cost can be reduced.

The invention discloses preparation of a high-uniformity cerium oxide abrasive material and application of the high-uniformity cerium oxide abrasive material in a chemical mechanical polishing solution. According to a method, cerium nitrate or cerium oxalate is used as a cerium source, a cationic or nonionic surfactant is used as a structure-directing agent, and the high-uniformity cerium oxide abrasive material is prepared in a mixed solvent system formed by water and isopropanol or water and diethylene glycol according to a specific volume ratio. The preparation method comprises the following steps: regulating the particle size and the morphology structure through a solvothermal reaction, carrying out cleaning, drying and high-temperature calcination treatment on a reaction product to obtain sphere-like cerium oxide nano-particles with high particle size concentration ratio, moderate surface roughness and good dispersity, adding cerium oxide powder into deionized water, and carrying out ultrasonic dispersion to obtain the spherical cerium oxide nano-particles. And sequentially adding a dispersing agent and amino acid while stirring, uniformly stirring, fixing the volume, and adding a pH regulator to enable the solution to be weakly acidic, thereby obtaining the chemical mechanical polishing solution. The cerium oxide submicron powder which is different in surface appearance, particle size and distribution uniformity is prepared by adjusting the solvent ratio and other reaction conditions.