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6090 results about "Hydrogen chloride" patented technology

The compound hydrogen chloride has the chemical formula HCl and as such is a hydrogen halide. At room temperature, it is a colourless gas, which forms white fumes of hydrochloric acid upon contact with atmospheric water vapor. Hydrogen chloride gas and hydrochloric acid are important in technology and industry. Hydrochloric acid, the aqueous solution of hydrogen chloride, is also commonly given the formula HCl.

Method and apparatus for producting negative and positive oxidative reductive potential (orp) water

ActiveUS20050121334A1Effective and efficient and economicalCellsWater treatment parameter controlParticulatesElectrolysis
A method and apparatus for electrolytically producing oxidation reduction potential water from aqueous salt solutions for use in disinfection, sterilization, decontamination, wound cleansing. The apparatus includes an electrolysis unit having a three-compartment cell (22) comprising a cathode chamber (18), an anode chamber (16), and a saline solution chamber (20) interposed between the anode and cathod chambers. Two communicating (24, 26) membranes separate the three chambers. The center chamber includes a fluid flow inlet (21a) and outlet (21b) and contains insulative material that ensures direct voltage potential does not travel through the chamber. A supply of water flows through the cathode and anode chambers at the respective sides of the saline chamber. Saline solution flows through the center chamber, either by circulating a pre-prepared aqueous solution containing ionic species, or, alternatively, by circulating pure water or an aqueous solution of, e.g., aqueous hydrogen chloride and ammonium hydroxide, over particulate insulative material coated with a solid electrolyte. Electrical current is provided to the communicating membranes separating the chambers, thus causing an electrolytic reaction that produces both oxidative (positive) and reductive (negative) ORP water.
Owner:SONOMA PHARMA INC

Laser infrared gas analyzer based on TDLAS-WMS (tunable diode laser absorption spectroscopy-wavelength modulation spectroscopy)

The invention belongs to the technical field of gas detection and relates to a laser infrared gas analyzer based on TDLAS-WMS (tunable diode laser absorption spectroscopy-wavelength modulation spectroscopy) for detecting hydrogen chloride, methane, carbon monoxide, water vapor and other gases. The laser infrared gas analyzer comprises a laser, a laser driving circuit, a temperature control circuit, an optical system with an optical cavity, a main detector, a reference detector, an intensity modulation and canceling circuit, a phase-locking and amplification circuit and a data acquisition and display circuit, wherein the laser driving circuit and the temperature control circuit are used for controlling the laser to emit light, the two ends of the optical system are respectively connected with the laser and the detector, the intensity modulation and canceling circuit is used for canceling the influence of intensity modulation in the system, the phase-locking and amplification circuit is used for extracting harmonic signals, and the data acquisition and display circuit is used for displaying the concentration of the gas to be detected. Compared with other detection instruments, the laser infrared gas analyzer has the advantages that division operation is introduced into the intensity modulation and canceling circuit, and the laser infrared gas analyzer is combined with a space double-optical path differential detection method, so that the influence of the intensity modulation can be fundamentally canceled.
Owner:JILIN UNIV

Industrial process for the synthesis of 17a-acetoxy-11ss-[4-(n,n-dimethyl-amino)- phenyl]-19-norpregna-4,9-diene-3,20-dione and new intermediates of the process

The present invention relates to a new industrial process for the synthesis of solvate- free 17a-acetoxy-11ss-[4-(N,N-dimethyl-amino)-phenyl]-19-norpregna-4,9-diene-3,20-dione [CDB -2914] of formula (I) which is a strong antiprogestogene and antiglucocorticoid agent. The invention also relates to compounds of formula (VII) and (VIII) used as intermediates in the process. The process according to the invention is the following: i) 3-(ethylene-dioxy)-estra-5(10),9(11)-diene-17-one of formula (X) is reacted with potassium acetilyde formed in situ in dry tetrahydrofuran by known method, ii) the obtained 3-(ethylene-dioxy)-17a-ethynyl-17ss-hydroxy-estra-5(10),9(11)-diene of formula (IX) is reacted with phenylsulfenyl chloride in dichloromethane in the presence of triethylamine and acetic acid, iii) the obtained isomeric mixture of 3-(ethylene-dioxy)-21-(phenyl-sulfinyl)-19-norpregna-5(10),9(11),17(20),20-tetraene of formula (VIII) is reacted first with sodium methoxide in methanol, then with trimethyl phosphite, iv) the obtained 3-(ethylene-dioxy)-17a-hydroxy-20-methoxy-19-norpregna-5(10),9(11),20-triene of formula (VII) is reacted with hydrogen chloride in methanol, then v) the obtained 3-(ethylene-dioxy)-17a-hydroxy-19-norpregna-5(10),9(11l); -diene-20- one of formula (VI) is reacted with ethylene glycol hi dichloromethane in the presence of trimethyl orthoformate and p-toluenesulfonic acid by known method, vi) the obtained 3,3,20,20-bis(ethylene-dioxy)-17a-hydroxy-19-norpregna- 5(10),9(11)-diene of formula (V) is reacted with hydrogen peroxide in a mixture of pyridine and dichloromethane in the presence of hexachloroacetone by known method, vii) the obtained 3,3,20,20-bis(ethylene-dioxy)-17a-hydroxy-5,10-epoxy-19-norpregn-9(11)-ene of formula (IV), containing approximately a 1:1 mixture of 5a,10a- and 5ss,10ss-epoxides, is isolated from the solution and reacted with a Grignard reagent obtained from 4-bromo-N,N-dimethyl-aniline in tetrahydrofuran.
Owner:RICHTER GEDEON NYRT

Method for preparing polyethylene glycol/silicon dioxide composite shape-stabilized phase change energy storage material and product thereof

The invention discloses a method for preparing a polyethylene glycol / silicon dioxide composite shape-stabilized phase change energy storage material and a product thereof. The method comprises the following steps of: dissolving polyethylene glycol serving as a work substance into water in an amount of between 0.2 and 1.0g / ml to obtain water solution of the polyethylene glycol; dripping a side product SiCl4 of polycrystalline silicon into the obtained water solution of the polyethylene glycol for a hydrolysis and sol-gel reaction to form gel with a three-dimensional network structure; drying the gel to prepare powder, removing water and hydrogen chloride from the powder; and dripping a modifier for modifying the surface of the powder hydrophobically in an amount which accounts for 0.1 to 1.5 weight percent of the powder at the temperature of 80 DEG C under the protection of nitrogen for surface modification to obtain the polyethylene glycol / silicon dioxide composite shape-stabilized phase change energy storage material. The method can change wastes into valuables and reduce the manufacturing cost of the product by using the side product SiCl4 of the polycrystalline as a silicon source, and is favorable for the industrial production and wide popularization and application of the SiO2 shape-stabilized phase change energy storage material.
Owner:SOUTHWEST JIAOTONG UNIV +1

Preparation method of lithium hexafluorophosphate

The invention relates to a preparation method of lithium hexafluorophosphate. The preparation method comprises the following steps of: (1) distilling to obtain hydrogen fluoride liquid of which the purity is over 99.99 weight percent; (2) reacting the high-purity hydrogen fluoride liquid with phosphorus pentachloride to obtain mixed gas of the phosphorus pentafluoride and hydrogen chloride; (3) introducing the mixed gas of the phosphorus pentachloride and the hydrogen chloride into hydrogen fluoride and lithium fluoride, reacting at a certain temperature and under certain pressure to obtain solution of lithium hexafluorophosphate, exhausting hydrogen chloride gas at regular time, and absorbing by using water to prepare byproduct hydrochloric acid; and (4) crystallizing and separating, namely filtering the solution of lithium hexafluorophosphate, delivering filtrate into a crystallizing slot, separating the lithium hexafluorophosphate out at the temperature of between -70 and 80 DEG C, filtering, and performing primary drying and secondary drying to obtain a lithium hexafluorophosphate product, wherein the residual hydrogen fluoride gas is displaced by nitrogen. The preparation method has readily available raw materials and is easy to operate, the purity of the obtained lithium hexafluorophosphate product is over 99.9 percent, the moisture is lower than 10ppm, and the production requirements of lithium ion electrolytic cells are met.
Owner:MORITA NEW ENERGY MATERIALS ZHANGJIAGANG CO LTD

Absorption tower for desulfurization and denitrification combined with oxidant in forward-flow and back-flow spraying and method

The invention discloses an absorption tower for desulfurization and denitrification combined with an oxidant in forward-flow and back-flow spraying mode and a method. The absorption tower includes two washing sections: a first section is a desulfurization loop and arranged on the lower portion of the absorption tower, and sulfur dioxide and hydrogen chloride are removed through slurry forward-flow and back-flow and smoke contact cleaning; a second section cleans oxidized smoke pollutants in slurry back-flow and smoke contact mode mainly for removing oxynitride and heavy metal mercury. A slurry divider is arranged between the two cleaning sections, the bottom of the slurry divider is an oxidization area, and strong oxidant is sprayed in the area. For reducing consumption of the oxidant, a catalyst is added in second-loop slurry for achieving auxiliary oxidization. Sulfur dioxide, oxynitride, heavy metal mercury and the like can be removed simultaneously in a washing tower by the technology, and the absorption tower has the advantages of being high in efficient and simple and suitable for various combustion devices including fuel coal power stations, refuse incineration plants, organic and inorganic production enterprises and the like.
Owner:NORTH CHINA ELECTRIC POWER UNIV (BAODING) +1

Method for processing fly ash used for circulating fluidized bed

The invention relates to a method for processing fly ash used for a circulating fluidized bed, which comprises the following steps: dissolving fly ash from the circulating fluidized bed out by hydrochloric acid, filtering to obtain filter residue and a leaching liquid; adjusting pH value of the leaching liquid to 1.5-3.5 by ammoniacal liquor, deposing, filtering to obtain the filter residue and a filtrate, washing filter residue, drying to obtain a compound of iron; adjusting the pH value of the filtrate after extracting iron to 3.8-5.2 by the ammoniacal liquor, deposing, filtering to obtain the filter residue and the filtrate, washing filter residue, drying to obtain aluminium hydroxide, further calcining to obtain metallurgy alumina; adding magnesium oxide in an ammonium chloride solution after extracting aluminium and performing ammonia distilling and hydrolysis reactions to obtain hydrogen chloride gas, ammonia gas and magnesium oxide. According to the invention, stepwise extraction of useful elements such as aluminium, silicon and iron in fly ash can be realized, cycle utilization of the materials can be realized, process is simple, cost is low, and the method opens new approach for high value utilization of fly ash from the circulating fluidized bed.
Owner:GUIYANG AL-MG DESIGN & RES INST
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