356 results about "Xylylene" patented technology

This invention belongs to the field of coating technology, specifically relating to a moisture-proof and stain-resistant acrylic resin coating and its preparation process. The moisture-proof and stain-resistant acrylic resin coating comprises 100 parts by weight of a main agent and 20-25 parts by weight of a curing agent. The main agent comprises the following raw materials in weight percentages: dispersant 1.5-3%, butyl acetate 10-15%, xylene 5-10%, filler 10-20%, titanium dioxide 10-20%, carbon black 1-5%, cellulose acetate butyrate 1-2%, anti-settling agent 1-1.5%, leveling agent 0.5-1%, defoamer 0.1-0.5%, with the balance being acrylic resin. The moisture-proof and stain-resistant acrylic resin coating of this invention exhibits excellent comprehensive performance, high filling and sealing properties, strong adhesion to alloys, and good stain resistance, water resistance, and gloss retention.

The invention relates to an aliphatic copolyester elastomer and a preparation method thereof, and belongs to the field of high polymer materials. The elastomer is prepared through a series ring-opening copolymerization reaction of epoxide and cyclic anhydride, and the method comprises the following steps: under the action of a metal-free catalyst (a phosphazene ligand P1-tert-octyl / triethyl boron system) and an initiator (terephthalyl alcohol), carrying out a series ring-opening copolymerization reaction on epoxide and cyclic anhydride, the preparation method comprises the following steps: reacting epoxide (such as epoxypropane and allyl glycidyl ether) with aliphatic anhydride (such as glutaric anhydride) in a xylene solvent to generate a polyester prepolymer retaining an active end; adding a second group of epoxide (such as cyclohexene oxide) and anhydride (such as tetrahydrophthalic anhydride and norbornene dianhydride), continuously reacting to form a block copolymer, and then crosslinking. The material performance can be regulated by changing the monomer combination, the atom economy is high, and the raw materials can be produced on a large scale. The process is simple and environment-friendly, and a new choice is provided for application of the degradable elastomer in the fields of medical treatment, environmental protection and the like.

The present invention relates to a cable comprising a polypropylene composition comprising (A) from 80.0 to 99.0 wt.-%, preferably from 82.5 to 97.2 wt. %, most preferably from 85.0 to 95.0 wt.-% of a copolymer of propylene and comonomer units selected from ethylene and alpha-olefins having from 4 to 12 carbon atoms having a total amount of comonomer units of from 10.0 to 16.0 wt %, preferably from 11.0 to 15.0 wt %, most preferably from 12.0 to 14.0 wt %, based on the total amount of monomer units of the copolymer of propylene (A); a melt flow rate MFR2 of from 0.5 to 2.5 g / 10 min, preferably from 0.8 to 2.3 g / 10 min, still more preferably from 1.0 to 2.0 g / 10 min and most preferably from 1.2 to 1.7 g / 10 min; a xylene cold soluble (XCS) fraction in a total amount of from 25.0 to 50.0 wt %, preferably from 27.5 to 45.0 wt %, more preferably from 30.0 to 42.5 wt % and most preferably from 32.5 to 40.0 wt %, based on the total weight amount of the copolymer of propylene (A); and (B) from 1.0 to 20.0 wt.-%, preferably from 2.5 to 17.5 wt %, most preferably from 5.0 to 15.0 wt.-% of a copolymer of ethylene and comonomer units selected from alpha-olefins having from 4 to 12 carbon atoms obtainable in the presence of a single site catalyst and having a density of from 860 to 930 kg / m3, preferably from 865 to 925 kg / m3, most preferably from 870 to 920 kg / m3, determined according to ISO 1183.

The method is for producing para-xylene using, as a main raw material, a mixed gas of carbon dioxide or carbon monoxide or both thereof and hydrogen. The method including: a reaction step of bringing a raw material mixed gas including the mixed gas into contact with a reaction catalyst under high temperature and high pressure to cause a reaction, to thereby obtain a product gas mixture containing para-xylene; a separation step of cooling the product gas mixture obtained in the reaction step to condense a high boiling point component, to thereby separate the product gas mixture into a water phase containing a water-soluble component, an oil phase containing a xylene mixture, and a gas phase containing an unreacted gas; and a circulation step of mixing at least part of the gas phase having been separated in the separation step into the raw material mixed gas.

The present invention relates to a polypropylene composition comprising (A) from 80.0 to 99.0 wt.-% of a copolymer of propylene and comonomer units selected from ethylene and alpha-olefins having from 4 to 12 carbon atoms having a total amount of comonomer units of from 10.0 to 16.0 wt %, based on the total amount of monomer units of the copolymer of propylene (A); a melt flow rate MFR2 of from 0.5 to 2.5 g / 10 min; a xylene cold soluble (XCS) fraction in a total amount of from 25.0 to 50.0 wt %, based on the total weight amount of the copolymer of propylene (A); and (B) from 1.0 to 20.0 wt.-% of an ethylene polymer having a density of from 915 to 960 kg / m3; and a melt flow rate MFR5 (190° C., 5 kg) of from 0.05 to 5.0 g / 10 min, an article comprising said polypropylene composition, preferably a cable comprising an insulation layer comprising said polypropylene composition, and the use of said polypropylene composition as cable insulation for medium and high voltage cables.

Processes and facilities for producing a recycled content organic chemical compound directly or indirectly from waste plastic. Processing schemes are described herein for converting waste plastic (or hydrocarbon having recycled content derived from waste plastic) into useful intermediate chemicals and final products. The waste plastic can be liquified before being introduced to downstream processing. In some aspects, recycled content aromatics (r-aromatics) can be processed to provide recycled content paraxylene (r-paraxylene), which can then be used to provide recycled content terephthalic acid (r-TPA) and / or recycled content polyethylene terephthalate (r-PET).

The invention relates to the field of pesticides, and particularly discloses a pH-light dual-response nano pesticide and a preparation process thereof. The invention relates to a preparation method of a pH-light dual-response nano insecticide. The preparation method comprises the following steps: adding water into polyethylene glycol, castor oil polyoxyethylene ether and sodium lignin sulfonate to prepare a water phase; the preparation method comprises the following steps: uniformly mixing an efficient cyhalothrin active compound with xylene, and adding diisocyanate to prepare an oil phase; adding the oil phase into the water phase, and adding ethylenediamine, YUS-SC3A, glycerol, xanthan gum, magnesium aluminum silicate and benzoic acid to obtain the lambda-cyhalothrin microcapsule suspending agent. The preparation method comprises the following steps: adding water into YUS-SC3A, uniformly mixing, and adding a clothianidin active compound, glycerol, xanthan gum, magnesium aluminum silicate, AF205 and benzoic acid to obtain a clothianidin suspending agent; mixing the two agents to obtain the nano insecticide, adding the composite dispersant, adding the pre-gel, adding azodiisobutyronitrile, blowing with inert gas, and adding Kathon. By preparing the pH-light dual-response nano insecticide, the insecticidal effect is improved, the generation of drug resistance is avoided, and efficient prevention and control of wheat aphids are realized.

The present application belongs to the technical field of cleaning products, and particularly relates to a high-temperature oil stain removing stove cleaner as well as a preparation method and application thereof. The high-temperature oil stain removing stove cleaner provided by the present application comprises the following components and mass fractions: 11-33 parts of an alkaline additive, 1-2 parts of hydroxyethylidene diphosphonic acid, 3-6 parts of a non-ionic surfactant, 4-8 parts of a solvent, 1-3 parts of a solubilizer, 1-3 parts of sodium xylene sulfonate, and 45-79 parts of water; the solvent comprises ethylene glycol monobutyl ether and diethylene glycol ethyl ether. The high-temperature oil stain removing stove cleaner provided by the present application has the advantages of simple cleaning method, high-temperature oil removing effect, good stain removing and oil scale removing effect on commercial kitchen utensils, high safety, no corrosion to metal, simple raw material composition, and no need to add a defoaming agent.

The application provides a C8 aromatic hydrocarbon isomerization catalyst and a preparation method and application thereof. The catalyst contains an active component and a carrier; wherein, based on the weight of the carrier, the carrier contains 5wt%-25wt% of HZSM-23, 5-30wt% of mordenite, 20-60wt% of macroporous alumina and 10wt%-25wt% of a binder component. The method comprises preparation of the carrier and loading of the active metal, wherein the preparation process of the carrier is as follows: HZSM-23 molecular sieve, mordenite, macroporous alumina and a binder are mixed and formed, and the carrier is prepared after drying and calcination. The catalyst is used for C8 aromatic hydrocarbon isomerization reaction, and has the characteristics of high ethylbenzene conversion rate and high xylene yield when the xylene is at an equilibrium concentration.

This application relates to a UV-3 ultraviolet absorber and its preparation method, belonging to the field of chemical synthesis technology. The preparation method employs a one-pot process, in which benzocaine reacts with triethyl orthoformate in xylene solvent. This step utilizes reactive distillation coupling control, continuously removing the generated alcohol distillate through a distillation separation device to promote reaction equilibrium shift, obtaining a xylene solution of the intermediate NET. Subsequently, the solution is heated to a reaction temperature of 135–145°C, and benzyl chloride is added dropwise for N-alkylation, while a tail gas absorption device absorbs byproduct gases. The reaction slurry is then cooled for crystallization, solid-liquid separation, and drying to obtain the UV-3 product. This invention simplifies the production process through a one-pot process, avoids the use of toxic DMF solvent, and solves the technical problem of raw material residues leading to subsequent side reactions in the one-pot process through reactive distillation coupling control, resulting in a final product with high purity and high yield.

The invention discloses an epoxy zinc-rich primer containing modified graphene and a preparation method thereof, and belongs to the technical field of anticorrosive paints.The preparation method comprises the steps that the surface of graphene oxide is carboxylated, then magnesium and cerium ions are used for composite modification, modified graphene oxide is obtained, phenyl Janus-SiO2 particles are synthesized and loaded with a benzotriazole corrosion inhibitor, corrosion inhibition type Janus composite particles are obtained, and the modified graphene oxide is prepared. Finally, xylene, epoxy resin, zinc powder, a dispersing agent, a defoaming agent, heavy calcium carbonate and mica powder are stirred step by step to obtain a component A, an epoxy curing agent, xylene, carboxylated composite powder, corrosion inhibition type Janus composite particles and the dispersing agent are subjected to ultrasonic treatment to prepare a component B, finally, the component A and the component B are evenly mixed, and the epoxy zinc-rich primer containing modified graphene is obtained. The comprehensive performance breakthrough of the primer in the aspects of adhesive force, long-acting corrosion resistance and cathodic disbonding resistance is realized.

The invention relates to the technical field of plant essential oil extraction, and discloses a valerian-rich rhizoma nardostachyos essential oil directional preparation process, which comprises: taking a functionalized compound solvent, adding rhizoma nardostachyos coarse powder according to a liquid-solid ratio, stirring and soaking to obtain a solid-liquid mixture; the solvent component comprises process water, sodium xylene sulfonate, dipotassium phosphate and polyethylene glycol 400; introducing steam into the mixture, heating to maintain slight boiling, carrying out first-stage distillation, and removing distilled low-boiling-point components to obtain resident in the kettle; cooling the resident to a constant temperature, adding sodium chloride, and stirring until the sodium chloride is dissolved to obtain a heterogeneous mixed system; the heating system is subjected to second-stage distillation, and distillate is collected; and carrying out oil-water separation on the distillate, and collecting an oil phase to obtain a finished product of the rhizoma nardostachyos essential oil. According to the method disclosed by the invention, a hydrotropy-salting-out phase change mechanism is matched with fractional distillation, so that high-efficiency desorption and directional enrichment of valerianone which is difficult to volatilize are realized while acidic and light component impurities are removed.

The xylylene diisocyanate composition contains a xylylene diisocyanate and a specific compound. When the xylylene diisocyanate composition is mixed with deuterated chloroform and the mixture is subjected to 1H-NMR measurement, the specific compound has a peak in a chemical shift value range of 2.44 ppm to 2.46 ppm based on chloroform in the deuterated chloroform.

The application discloses a method for selectively hydrogen-dealkylating aromatics and coupling xylene isomerization. + The method comprises the following steps: contacting aromatics, PX-lean C8 aromatics and a catalyst to perform selective hydrogen-dealkylation and xylene isomerization; wherein the catalyst comprises catalyst A, catalyst B and catalyst C, catalyst A is arranged upstream of catalyst B, and catalyst C is arranged downstream of catalyst B; wherein the catalyst A is a composite modified alumina; the catalyst B and the catalyst C are independently selected from group VIII metal modified molecular sieves. + The method provided by the application can concentrate a reaction unit to selectively hydrogen-dealkylate C8 10 C2 + The method can realize xylene isomerization in the PX-lean C8 aromatics while selectively hydrogen-dealkylating the side chains, and can cooperate with liquid phase transalkylation technology, so that an isomerization unit in an existing process is omitted, and device energy consumption, material consumption and investment are greatly reduced.

The invention relates to the technical field of aromatic hydrocarbon separation and purification, in particular to a system and process flow for removing C8 non-aromatic hydrocarbon in xylene through membrane separation, and the system comprises a membrane separation unit, a feeding unit, a permeation side system, an interception side system, an adsorption tower feeding buffer tank outlet line and a crossover line; the membrane separation unit is provided with a membrane feeding pipeline, one end of the membrane separation unit is connected to an outlet of the membrane separation feeding buffer tank, and the other end of the membrane separation unit is connected to an inlet side pipe orifice of the separation pipeline; a membrane feeding booster pump is arranged on the membrane feeding pipeline; a spiral-wound membrane assembly is arranged in the separation pipeline; the feeding unit is provided with a xylene redistillation tower top outlet line which is connected to an inlet of the membrane separation feeding buffer tank from the xylene redistillation tower top. According to the membrane separation process adopted by the method, the non-aromatic hydrocarbon removal rate can be more than 98% under the operation conditions that the feeding pressure is 1.68 MPa, the permeation side is 20 kPa and the interception side is 1.6 MPa, and the method has definite industrial feasibility and technical advantages.

The present invention relates to a xylylene diisocyanate composition and a photopolymerizable composition including the same. The xylylene diisocyanate composition according to an exemplary example includes a xylylene diisocyanate (XDI) and an acidity adjuster having a boiling point of 110°C or more, wherein the acidity of the composition is greater than 100 ppm and 1,000 ppm or less with respect to the total weight of the xylylene diisocyanate (XDI). The polymerization reaction rate is controlled by adjusting the acidity, so that an optical lens having high transmittance and improved optical uniformity can be manufactured.

The utility model provides a cooling device which comprises a cooling cylinder, a plurality of first partition plates and second partition plates which are evenly distributed are arranged in the cooling cylinder, the first partition plates and the second partition plates are installed in a matched mode, a plurality of cooling pipes which are evenly distributed are arranged on the first partition plates and the second partition plates, and a plurality of stirring shafts which are evenly distributed are arranged in the cooling cylinder. And stirring paddles fixedly sleeve the middle parts of the outer arc surfaces of the stirring shafts. According to the cooling device disclosed by the utility model, when the dimethylbenzene stock solution is cooled, the dimethylbenzene stock solution can be continuously and quickly cooled by extending the flowing path of the dimethylbenzene stock solution in the cooling cylinder and matching with the stirring paddle.

The invention discloses a low-surface-energy active and passive synergistic antifouling coating and a preparation method thereof, and belongs to the technical field of marine antifouling materials. The preparation method of the antifouling coating comprises the following steps: S1, mixing acetone and xylene, and stirring in a nitrogen atmosphere to form a mixed solvent; s2, adding vinyl-terminated organic silicon resin and acrylic resin into the mixed solvent, stirring and heating to obtain a coating base solution; s3, adding an initiator into the coating base solution, and continuously stirring and heating for reaction; s4, after the reaction is finished, cooling the coating base solution, and adding a functional filler to form a coating solution; and S5, the coating liquid is coated and then dried, and the low-surface-energy active and passive synergistic antifouling coating is obtained. The low-surface-energy active and passive synergistic antifouling coating prepared by the invention solves the problem that environmental protection property and long-term effect cannot be considered at the same time due to single antifouling mechanism in the existing marine antifouling technology, and has a wide application prospect in the technical field of marine antifouling materials.

The invention relates to a xylylene diisocyanate composition as well as a preparation method and application thereof. The xylylene diisocyanate composition comprises at least 98% of xylylene diisocyanate and has defoaming time less than or equal to 15 seconds. The resin lens prepared from the xylylene diisocyanate composition provided by the invention has a relatively low haze index.

Disclosed are apparatuses and processes for preparation and conversion comprising / using: a fractionation chain (4-6) that produces a xylene fraction (24); a xylene separation unit (10) that treats the xylene fraction to produce a para-xylene extract (39) and a raffinate (40); an isomerization unit (11) treating the raffinate to produce an isomerization product (42) of xylenes fed to the fractionation chain; the synthesis gas production unit (14; 15) that treats the hydrocarbon feedstock (30) to produce a synthesis gas (34) containing CO and CO2; a methanol synthesis reaction section (50) that treats the synthesis gas (34) to produce methanol (51); a toluene alkylation reaction section (13) treating the toluene-containing fraction (23) with methanol (51) to produce an alkylation effluent (32) containing xylene and fed to the fractionation chain.

An object of the present invention is to provide a cover film in which chips during cutting are unlikely to be generated, voids during bonding to a substrate using an enclosing solution are unlikely to be generated, and adhesiveness with the substrate is excellent. The cover film of the present invention is used for covering a test subject on a substrate, the cover film including a support and a polymer layer containing a polymer, in which a fracture toughness value of the polymer layer is 0.2 MPa·m0.5 or more, an in-plane retardation of the support at a wavelength of 590 nm is 1,000 nm or less, and a requirement regarding a dissolution rate of the polymer layer in xylene and a requirement regarding a viscosity of a xylene solution of the polymer layer are satisfied.

The application relates to the technical field of resource utilization of construction waste, and discloses a construction waste and waste cement block xylene impurity removal process. In the process, waste cement blocks and waste concrete blocks in the construction waste are subjected to sorting, crushing and screening to obtain recycled aggregates, the aggregates are subjected to pre-washing with clean water to remove loose impurities, and then are subjected to xylene treatment liquid soaking under specific solid-liquid ratio and temperature conditions, and are subjected to ultrasonic oscillation or mechanical stirring to strengthen mass transfer; after treatment, the aggregates are subjected to solid-liquid separation, distillation and purification, and then are recycled, and the aggregates are subjected to washing and drying to obtain high-quality recycled aggregates. The application has excellent impurity removal effect, does not damage the original structure of the aggregates, can realize recycling of the solvent, does not cause pollution of acidic waste water, has strong process adaptability, and can significantly reduce the water absorption rate and crushing index of the treated recycled aggregates, so that the treated recycled aggregates can meet the preparation requirements of medium and high-grade concrete, and the application realizes high-value and green resource utilization of the construction waste.

This invention belongs to the field of protective coating technology, specifically relating to a protective coating for transportation vehicles resistant to phosphate ester hydraulic oil and its preparation method. The protective coating comprises component A and component B. Component A includes a polyurea-modified polyester resin, a surface tension modifier, a defoamer, and a mixed solvent. Component B includes an isocyanate prepolymer and xylene. The polyurea-modified polyester resin is prepared from polyether polyol, polyisocyanate, polyaspartic acid ester, polyol, catalyst, and xylene through a specific synthesis process. This protective coating can withstand the corrosion of phosphate ester hydraulic oil, providing a durable protective barrier. It solves the problem of softening and peeling of the protective coating due to leakage and diffusion caused by phosphate ester hydraulic oil spills after a period of use in transportation vehicles.

This invention provides a method for producing fine polyolefin powder in micrometer units, characterized by uniform particle shape, average particle size, and particle size distribution. [Solution] This invention relates to a method for producing polyolefin ultrafine powder and the polyolefin ultrafine powder produced thereby. Specifically, the method involves mixing and heating a polyolefin resin with a xylene mixed solvent to produce a polyolefin molten liquid, then cooling and crystallizing it, and then ultrafine grinding the crystallized reactant through a vacuum wet grinding step and a dry grinding step, in which wet grinding and drying are performed simultaneously with the solvent, thereby providing an ultrafine polyolefin powder with an average particle size of approximately 30 μm or less. A xylene mixed solvent is used as the mixed solvent for melting the polyolefin resin, and the ultrafine polyolefin powder produced thereby can be applied to general-purpose material fields such as construction, civil engineering, and chemical products, and has physical properties that are particularly advantageous for the manufacture of secondary battery electrodes.

The invention relates to the technical field of oxadiazon production, and discloses a wastewater circulation treatment system for oxadiazon production, which comprises a wastewater kettle, a water segregator, a first dryer, a dissolving kettle, a filter and a second dryer, and the devices are sequentially communicated through pipelines; the wastewater kettle is provided with a wastewater inlet, an extractant inlet and a discharge port, and the discharge port of the wastewater kettle is connected to the inlet of the water segregator and used for mixing wastewater and extractant xylene and separating the mixture into a water phase and an organic phase; and a water phase outlet of the water segregator is connected to an inlet of the first dryer. According to the waste water circulation treatment system for oxadiazon production, waste water containing triazole and xylene are mixed and separated, a water phase is dehydrated to obtain a solid substance, then the solid substance is dissolved with acetone and filtered, and finally solid triazole and acetone are recycled through distillation, so that valuable raw materials in the waste water are efficiently recycled, waste of triazole is directly reduced in the process, and the cost is reduced. And the follow-up treatment difficulty and cost of the high-salinity wastewater are obviously reduced.

The invention discloses an inorganic fiber protective material and a preparation method thereof. The inorganic fiber protective material comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 4-15 parts of inorganic powder, 5-15 parts of water-based resin and 5-15 parts of water; and the component B comprises the following components in parts by weight: 3-10 parts of organic silicon resin, 15-30 parts of ethanol, 0.5-3 parts of xylene and 0.1-0.5 part of ammonia water. The inorganic fiber protective material can effectively repair the defects of the inorganic fibers, can form a moisture-proof protective layer on the surfaces of the inorganic fibers, and effectively solves the problem that the inorganic fibers are easy to break in the moisture-proof and cable insulation processing process.

The present application belongs to the technical field of petroleum processing and the field of carbon material preparation, and discloses a preparation method of spinnable mesophase pitch based on co-carbonization of coal tar pitch and catalytic cracking slurry. Coal tar pitch and xylene-soluble components of coal tar pitch extracted by xylene are mixed with catalytic cracking slurry, and then co-carbonization reaction is carried out. The reaction product is crushed, secondarily extracted, filtered, and then subjected to low-temperature heat treatment to obtain spinnable mesophase pitch. Through raw material cooperation and multi-stage purification process, the present application realizes high content, high spinnability and structure controllability of mesophase pitch, and the process is simple, environmentally friendly and economical, and is suitable for large-scale production of high-performance pitch-based carbon fiber.

This invention discloses a low surface energy active-passive synergistic antifouling coating and its preparation method, belonging to the field of marine antifouling materials technology. The preparation method of the antifouling coating includes the following steps: S1, mixing acetone and xylene and stirring under a nitrogen atmosphere to form a mixed solvent; S2, adding vinyl-terminated silicone resin and acrylic resin to the mixed solvent, stirring and heating to obtain a coating base liquid; S3, adding an initiator to the coating base liquid and continuously stirring and heating to react; S4, after the reaction is complete and the coating base liquid cools, adding functional fillers to form a coating liquid; S5, coating the coating liquid and drying to obtain a low surface energy active-passive synergistic antifouling coating. The low surface energy active-passive synergistic antifouling coating prepared by this invention solves the problem in existing marine antifouling technologies where the single antifouling mechanism prevents the simultaneous consideration of environmental friendliness and long-term effectiveness, and has broad application prospects in the field of marine antifouling materials technology.

The utility model discloses a p-xylene crystallization device which at least comprises a raw material input pipeline, the at least one crystallization unit is connected with the raw material input pipeline; the at least one separation unit is connected with the outlet of the crystallization unit; the mother liquor buffer tank is connected with an outlet of the separation unit; an inlet of the mother liquor pump is connected with an outlet of the mother liquor buffer tank; the subcooler is connected with an outlet of the mother liquor pump; the industrial wind input pipeline is connected with the other inlet of the mother liquor pump; and the industrial wind output pipeline is connected with the other outlet of the mother liquor pump. According to the p-xylene crystallization device provided by the utility model, the operation stability of the crystallization device can be improved.