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724 results about "Xylylene" patented technology

Xylylene comprises two isomeric organic compounds with the formula C₆H₄(CH₂)₂. These compounds are related to the corresponding quinones by replacement of the oxygen atoms by CH₂ groups. ortho- and para-xylylene are best known, although neither is stable in solid or liquid form. Certain substituted derivatives of xylylenes are however highly stable, an example being tetracyanoquinodimethane.

A moisture-proof and stain-resistant acrylic resin coating and its preparation process

This invention belongs to the field of coating technology, specifically relating to a moisture-proof and stain-resistant acrylic resin coating and its preparation process. The moisture-proof and stain-resistant acrylic resin coating comprises 100 parts by weight of a main agent and 20-25 parts by weight of a curing agent. The main agent comprises the following raw materials in weight percentages: dispersant 1.5-3%, butyl acetate 10-15%, xylene 5-10%, filler 10-20%, titanium dioxide 10-20%, carbon black 1-5%, cellulose acetate butyrate 1-2%, anti-settling agent 1-1.5%, leveling agent 0.5-1%, defoamer 0.1-0.5%, with the balance being acrylic resin. The moisture-proof and stain-resistant acrylic resin coating of this invention exhibits excellent comprehensive performance, high filling and sealing properties, strong adhesion to alloys, and good stain resistance, water resistance, and gloss retention.
Owner:BAOHONG COATINGS (GUANGDONG) CO LTD

Preparation method and application of MFI zeolite membrane

The invention discloses a preparation method and application of an MFI zeolite membrane.The preparation method comprises the steps that an MFI zeolite nanosheet serves as a seed crystal, a uniformly-distributed and compact seed crystal layer is prepared on a carrier through a vacuum filtration method, namely, a nucleation center crystallized into a membrane is loaded on the surface of the carrier, and directional growth and membrane forming of the zeolite nanosheet can be effectively controlled; the highly b-oriented MFI zeolite membrane can be prepared within several hours, the prepared b-oriented MFI zeolite membrane shows a continuous and compact microstructure and almost has no defects, and compared with a traditional hydrothermal method, the method overcomes the defects that the reaction process is too long in time consumption, uneven in heating is prone to occurring, and the like. And therefore, the time required by crystal growth is greatly shortened. The prepared MFI zeolite membrane can be applied to pervaporation separation of xylene isomers, shows good size screening separation performance, and has important industrial application value.
Owner:SOUTH CHINA UNIV OF TECH +1

Power cable

This power cable is provided with: a conductor; and an insulating layer that is provided so as to cover the outer periphery of the conductor and that is configured from a resin composition containing polyethylene. The insulating layer contains, among polyethylene, a crosslinked polyethylene that is insoluble in xylene at 120° C, and uncrosslinked polyethylene that can be eluted in xylene at 120° C. The uncrosslinked polyethylene has a number average molecular weight of 5000 to 25000.
Owner:SUMITOMO ELECTRIC INDUSTRIES LTD

Degradable aliphatic copolyester elastomer and preparation method thereof

PendingCN121378707AXylyleneGlutaric anhydride
The invention relates to an aliphatic copolyester elastomer and a preparation method thereof, and belongs to the field of high polymer materials. The elastomer is prepared through a series ring-opening copolymerization reaction of epoxide and cyclic anhydride, and the method comprises the following steps: under the action of a metal-free catalyst (a phosphazene ligand P1-tert-octyl / triethyl boron system) and an initiator (terephthalyl alcohol), carrying out a series ring-opening copolymerization reaction on epoxide and cyclic anhydride, the preparation method comprises the following steps: reacting epoxide (such as epoxypropane and allyl glycidyl ether) with aliphatic anhydride (such as glutaric anhydride) in a xylene solvent to generate a polyester prepolymer retaining an active end; adding a second group of epoxide (such as cyclohexene oxide) and anhydride (such as tetrahydrophthalic anhydride and norbornene dianhydride), continuously reacting to form a block copolymer, and then crosslinking. The material performance can be regulated by changing the monomer combination, the atom economy is high, and the raw materials can be produced on a large scale. The process is simple and environment-friendly, and a new choice is provided for application of the degradable elastomer in the fields of medical treatment, environmental protection and the like.
Owner:FOSHAN UNIVERSITY

Anti-ionizing radiation fiber with high filling amount, high strength and high elasticity as well as preparation method and application of anti-ionizing radiation fiber

The invention provides an anti-ionizing radiation fiber with high filling amount, high strength and high elasticity and a preparation method and application thereof, and belongs to the field of functional fiber materials.The preparation method comprises the steps that rare earth nitrate and citric acid are dissolved in an acidic alcohol aqueous solution, heated and stirred, the pH value is adjusted, sol is obtained, the sol is subjected to secondary heating treatment to obtain gel, and the gel is dried to obtain the high-filling-amount high-strength high-elasticity anti-ionizing radiation fiber. Aging, drying, grinding and calcining the gel to obtain rare earth composite powder; wherein the rare earth nitrate is a mixture of gadolinium nitrate, dysprosium nitrate and cerium nitrate; adding polyurethane into a mixed solution of DMF and xylene, stirring, adding the rare earth composite powder, stirring, and defoaming to obtain a spinning solution; preparing nascent fibers from the spinning solution through wet spinning; and drawing, washing and drying to obtain the anti-ionizing radiation fiber. The anti-ionizing radiation fiber prepared by the invention has excellent shielding property, mechanical property and air permeability.
Owner:WUHAN TEXTILE UNIV +1

Environment-friendly odorless sealing strip adhesive as well as preparation and application thereof

The invention discloses an environment-friendly odorless sealing strip adhesive as well as preparation and application thereof, and the environment-friendly odorless sealing strip adhesive is prepared from the following components in parts by mass: 15 to 20 parts of polyacrylate resin, 10 to 15 parts of dammar resin, 5 to 10 parts of fir resin, 3 to 5 parts of hydrogenated terpene resin, 2 to 5 parts of tributyl citrate and 45 to 65 parts of n-decane. The preparation method comprises the following steps: uniformly mixing natural resin (dammar resin, fir resin and hydrogenated terpene resin), polymeric monomers (n-octyl acrylate, methyl methacrylate and hydroxyethyl acrylate) and an environment-friendly solvent (n-decane), and then polymerizing to obtain the environment-friendly adhesive. The synthetic resin (polyacrylate resin) and the natural resin are sufficiently and mutually dissolved in n-decane to form stable and uniform composite resin glue, so that the problems of health risk and environmental pollution caused by harmful solvents such as xylene in the traditional sealing glue are effectively avoided, and the characteristics of no toxicity, no odor and environmental protection of the product are realized; meanwhile, the stability and the bonding performance of the section sealing glue are improved, the matching performance of the optical transmittance and the refractive index of the section sealing glue is enhanced, and the section sealing glue has quick-drying performance and is suitable for medical pathological sections.
Owner:WUHAN INST OF TECH

Organic-inorganic hybrid water-based acrylic acid modified epoxy ester resin and preparation method thereof

The invention relates to the technical field of water-based epoxy ester resin, and particularly discloses organic-inorganic hybrid water-based acrylic acid modified epoxy ester resin and a preparation method thereof in order to solve the problem that hardness and salt spray resistance of an existing epoxy ester resin coating are difficult to consider at the same time. Raw materials of the epoxy resin comprise 25-35 parts of epoxy resin, 22-30 parts of dry vegetable oleic acid or semi-dry vegetable oleic acid, 6-10 parts of a hard monomer, 5-15 parts of an inorganic precursor, 4-6 parts of reflux xylene, 3-5 parts of carboxyl acrylic acid, 0.4-0.6 part of an initiator, 0.05-0.25 part of a catalyst and 20-25 parts of an alcohol ether cosolvent. Specific preparation raw materials and production process conditions are adopted to construct the organic-inorganic hybrid water-based acrylic acid modified epoxy ester resin with a stable and uniform structure and a composite network structure, and the epoxy ester resin not only has remarkable hardness, but also has good water resistance, salt fog resistance and drying speed; the epoxy ester resin coating can be suitable for more application scenes.
Owner:MIANYANG MAXWELL TECH CO LTD

Paint removing composition, paint stain cleaning agent and application of paint stain cleaning agent

The invention relates to the technical field of paint removers, and particularly discloses a paint removal composition, a paint stain cleaning agent and application of the paint stain cleaning agent. The paint stain cleaning agent provided by the invention is prepared from the following components in parts by weight: 30 to 40 parts of EDTA-2Na (Ethylene Diamine Tetraacetic Acid), 200 to 300 parts of caustic soda flakes, 140 to 170 parts of sodium alcohol ether sulphate, 160 to 180 parts of sodium xylene sulfonate, 400 to 450 parts of monoethanolamine, 1100 to 1300 parts of diethylene glycol monobutyl ether, 250 to 300 parts of limonene, 40 to 100 parts of saponin extract and 3700 to 3900 parts of water, the saponin extract is selected from one or more of soapnut saponin, fenugreek saponin and aescin; the invention further provides a paint stain cleaning agent prepared from the paint removal composition and application of the paint stain cleaning agent to cleaning of protective clothing. The paint stain cleaning agent provided by the invention can quickly permeate into paint and the contact surface of the paint and protective clothing, so that the paint on the surface of the protective clothing is dissolved and effectively stripped.
Owner:BEIJING BAICHUAN TECH & TRADE CO LTD

Insulating layer for electromagnetic wire and preparation process thereof

The invention relates to the technical field of electromagnetic wire insulating layers, in particular to an insulating layer for an electromagnetic wire and a preparation method thereof, and the preparation method comprises the following steps: coating an insulating improved paint on the electromagnetic wire by adopting an enameling machine, and then continuously baking the electromagnetic wire by adopting the enameling machine to complete the preparation of the insulating layer. According to the insulating layer for the electromagnetic wire, the insulating layer is coated with the insulating improved paint through the enameling machine, the insulating improved paint is prepared from the polyimide paint, the xylene solvent, the weather change resistant functional agent and the modified filler, and the raw materials are co-matched, co-assisted and mutually blended to achieve a synergistic effect; the obtained insulating improved paint optimizes the softening breakdown property, wear resistance and pollution resistance of an insulating layer in a system, the performance coordination of a product is improved, and the weather resistance and temperature change resistance stability effects of the product are remarkable.
Owner:沈阳宏远电磁线股份有限公司

Special bolt for stainless steel mechanical equipment and preparation method thereof

The invention relates to the technical field of bolts, and provides a bolt special for stainless steel mechanical equipment and a preparation method thereof. A bolt special for stainless steel mechanical equipment comprises a bolt body and a surface coating, and the surface coating is prepared from, by weight, 100 parts of epoxy resin E-44, 50-55 parts of a curing agent, 1.5-2 parts of a curing accelerator, 20-25 parts of flaky iron oxide, 10-12 parts of modified boron nitride, 2-3 parts of an ultraviolet light absorber, 3-5 parts of silicon dioxide, 1-1.5 parts of a dispersing agent, 25-35 parts of butanone and 10-12 parts of xylene. According to the bolt special for the stainless steel mechanical equipment, the corrosion resistance of the stainless steel bolt in a high-concentration acid-base solution and high-temperature and high-pressure seawater is improved.
Owner:HANDAN HAOJIN FASTENER MANUFACTURING CO LTD

Polypropylene composition for cable insulation

The present invention relates to a cable comprising a polypropylene composition comprising (A) from 80.0 to 99.0 wt.-%, preferably from 82.5 to 97.2 wt. %, most preferably from 85.0 to 95.0 wt.-% of a copolymer of propylene and comonomer units selected from ethylene and alpha-olefins having from 4 to 12 carbon atoms having a total amount of comonomer units of from 10.0 to 16.0 wt %, preferably from 11.0 to 15.0 wt %, most preferably from 12.0 to 14.0 wt %, based on the total amount of monomer units of the copolymer of propylene (A); a melt flow rate MFR2 of from 0.5 to 2.5 g / 10 min, preferably from 0.8 to 2.3 g / 10 min, still more preferably from 1.0 to 2.0 g / 10 min and most preferably from 1.2 to 1.7 g / 10 min; a xylene cold soluble (XCS) fraction in a total amount of from 25.0 to 50.0 wt %, preferably from 27.5 to 45.0 wt %, more preferably from 30.0 to 42.5 wt % and most preferably from 32.5 to 40.0 wt %, based on the total weight amount of the copolymer of propylene (A); and (B) from 1.0 to 20.0 wt.-%, preferably from 2.5 to 17.5 wt %, most preferably from 5.0 to 15.0 wt.-% of a copolymer of ethylene and comonomer units selected from alpha-olefins having from 4 to 12 carbon atoms obtainable in the presence of a single site catalyst and having a density of from 860 to 930 kg / m3, preferably from 865 to 925 kg / m3, most preferably from 870 to 920 kg / m3, determined according to ISO 1183.
Owner:BOREALIS AG

Pathological slide rack drying device

The utility model discloses a pathological slide rack drying device which comprises a slide rack placing module, and a slide to be input with airflow and dried is accommodated in the slide rack placing module; the fan and the filtering module are arranged on one side of the slide rack placing module and are used for filtering output airflow; the utility model relates to the technical field of slide drying devices. The closed space of the drying section box body can be temporarily formed through the box body cover plate, and air input into the drying section box body from the primary filter can flow in the closed space formed by the drying section box body; and a low-temperature electric heating wire is matched to accelerate the volatilization of xylene on the glass slide placing rack so as to blend the xylene into the air in the drying section box body, finally, a switch of a fan is turned on to output the air with the xylene from an active carbon filter, and the air with the xylene is filtered by the active carbon filter to form clean air.
Owner:WUXI FRESHAIR AQ TECH

Acrylic polyurethane finish coat having high solid content and super weather resistance and preparation method therefor

Disclosed in the present invention are an acrylic polyurethane finish coat having a high solid content and super weather resistance and a preparation method therefor. The finish coat consists of a component A and a component B, the mass ratio of the component A to the component B being 20:(2-5). The component A comprises the following components in parts by mass: 30-45 parts of acrylic resin, 2-10 parts of a modified resin, 2-10 parts of a hyperbranched polyester polyol, 25-40 parts of a pigment and filler, 0-1.5 parts of a thixotropic agent, 0.1-10 parts of a dispersing agent, 0.1-0.5 part of a defoaming agent, 0.01-1 part of a drier and 1-10 parts of a mixed solvent. The component B comprises the following components in parts by mass: 70-95 parts of an aliphatic isocyanate polymer, 2-15 parts of xylene and 2-15 parts of propylene glycol methyl ether acetate. The coat of the present invention exhibits excellent weather resistance, which is comparable to that of super-weather-resistant finish coats fluorocarbon finish coats and polysiloxane finish coats, and has high mechanical strength and an anti-corrosion property, and is thus particularly suitable for surface coating of steel structures in the environment of South China Sea.
Owner:CNOOC CHANGZHOU PAINT & COATINGS IND RES INST +1

Method for producing para-xylene

The method is for producing para-xylene using, as a main raw material, a mixed gas of carbon dioxide or carbon monoxide or both thereof and hydrogen. The method including: a reaction step of bringing a raw material mixed gas including the mixed gas into contact with a reaction catalyst under high temperature and high pressure to cause a reaction, to thereby obtain a product gas mixture containing para-xylene; a separation step of cooling the product gas mixture obtained in the reaction step to condense a high boiling point component, to thereby separate the product gas mixture into a water phase containing a water-soluble component, an oil phase containing a xylene mixture, and a gas phase containing an unreacted gas; and a circulation step of mixing at least part of the gas phase having been separated in the separation step into the raw material mixed gas.
Owner:CHIYODA CORP

Polypropylene composition for cable insulation

The present invention relates to a polypropylene composition comprising (A) from 80.0 to 99.0 wt.-% of a copolymer of propylene and comonomer units selected from ethylene and alpha-olefins having from 4 to 12 carbon atoms having a total amount of comonomer units of from 10.0 to 16.0 wt %, based on the total amount of monomer units of the copolymer of propylene (A); a melt flow rate MFR2 of from 0.5 to 2.5 g / 10 min; a xylene cold soluble (XCS) fraction in a total amount of from 25.0 to 50.0 wt %, based on the total weight amount of the copolymer of propylene (A); and (B) from 1.0 to 20.0 wt.-% of an ethylene polymer having a density of from 915 to 960 kg / m3; and a melt flow rate MFR5 (190° C., 5 kg) of from 0.05 to 5.0 g / 10 min, an article comprising said polypropylene composition, preferably a cable comprising an insulation layer comprising said polypropylene composition, and the use of said polypropylene composition as cable insulation for medium and high voltage cables.
Owner:BOREALIS AG

Method for synthesizing mesitylene through isomerization of unsym-trimethylbenzene

According to the method, a heteroatom EWT structure molecular sieve with a framework containing aluminum atoms and heteroatoms is adopted as a catalyst, the molecular sieve has the advantage of improving the utilization rate of an acid center, and when the molecular sieve is used for a gas-phase non-hydroisomerization reaction of the unsym-trimethylbenzene, the utilization rate of the acid center is increased; according to the present invention, the activity, the selectivity and the stability are high, the catalytic performance is significantly improved, the mesitylene selectivity and the mesitylene yield are higher than the heteroatom-free [Si, Al]-EWT structure molecular sieve, and the by-products such as tetratoluene and xylene are significantly reduced.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Method for converting melted or dissolved waste plastic in a fluidized catalytic cracker and / or in a hydrocracking unit

Processes and facilities for producing a recycled content organic chemical compound directly or indirectly from waste plastic. Processing schemes are described herein for converting waste plastic (or hydrocarbon having recycled content derived from waste plastic) into useful intermediate chemicals and final products. The waste plastic can be liquified before being introduced to downstream processing. In some aspects, recycled content aromatics (r-aromatics) can be processed to provide recycled content paraxylene (r-paraxylene), which can then be used to provide recycled content terephthalic acid (r-TPA) and / or recycled content polyethylene terephthalate (r-PET).
Owner:EASTMAN CHEM CO

Preparation and purification method of crystal form of p-xylylene dicamphor sulfonate

The invention provides a preparation and purification method of a p-xylylene dicamphor sulfonate crystal form, which comprises the following steps: carrying out condensation polymerization on camphorsulfonic acid and terephthalaldehyde under the action of organic alkali to prepare p-xylylene dicamphor sulfonate, carrying out post-treatment, dissolving, clarifying and layering, dropwise adding ethanol, and sequentially carrying out first crystal growing and second crystal growing to obtain the p-xylylene dicamphor sulfonate crystal form. The preparation method comprises the following steps: dissolving p-xylylene dicamphor sulfonate in water to obtain a crude product of the p-xylylene dicamphor sulfonate crystal form, decolorizing the crude product, and carrying out gradient cooling crystallization, so that the high-purity p-xylylene dicamphor sulfonate crystal form product with high yield can be prepared, the content of impurities in the product is effectively controlled, the irritation of the impurities to the skin is reduced, and the safety of the product is improved. Meanwhile, the product has a crystal form, the moisture absorption of the product can be improved, and storage is easy.
Owner:COFFROSEN (SHANGHAI) CHEM CO LTD +1

Inorganic silicon hybrid polyurethane primer as well as preparation method and application thereof

The invention provides an inorganic silicon hybrid polyurethane primer as well as a preparation method and application thereof, and belongs to the technical field of primer. The primer provided by the invention is prepared from the following raw materials: polyester polyol, polyether polyol, trimethylolpropane, hexamethylene diisocyanate, 3-(phenylamino) propyltrimethoxysilane, ethyl acetate, xylene, an antioxidant, a light stabilizer, stannous octoate and a catalyst. An isocyanate-terminated polyurethane prepolymer is selected as a base material, a silane hybrid structure is introduced, a Si-O-Si network is formed after silane is hydrolyzed, the Si-O-Si network and Ca < 2 + > in concrete form a coordinate bond, and meanwhile, an isocyanate group reacts with water to generate a urea bond to reinforce anchoring. According to the primer disclosed by the invention, through a chemical-physical synergistic effect, the technical problem of bonding failure of a floating dust hardened layer is systematically solved, and an innovative solution is provided for long-acting sealing of a concrete joint.
Owner:XINJIANG AGRI UNIV +1

Preparation process of high-elasticity pressure-resistant air-permeable and water-permeable sponge

The invention provides a preparation process of a high-elastic pressure-resistant air-permeable and water-permeable sponge. The sponge is prepared from the following components in parts: 40 to 60 parts of highly branched polyester polyol, 37 to 43 parts of polyether polyol, 50 to 56 parts of isocyanate, 1.5 parts of multiwalled carbon nanotubes, 2.0 parts of nano silicon dioxide, 1.0 part of montmorillonite, 0.54 to 0.7 part of silane coupling agent, 2.0 to 3.1 parts of polyethylene glycol and 0.8 part of bimetallic catalyst. 1.8 parts of a foaming agent, 15 parts of a supercritical agent and 1.2 parts of an opening agent; the preparation method comprises the following steps: S1, carrying out segmented vacuum dehydration on highly branched polyester polyol and polyether polyol, carrying out xylene ultrasonic treatment on multi-walled carbon nanotubes and a silane coupling agent, and carrying out high-shear mixing to prepare a nanofiller dispersion liquid; through step-by-step dehydration, polyol thermal degradation is reduced, the hydroxyl value retention rate is improved, the integrity of a cross-linked network is ensured, through step-by-step dehydration and magnetic field dispersion, the problems of polyol thermal degradation and nano agglomeration are solved, and superuniform dissolution and precise regulation and control of double-peak aperture are realized through pulse injection and magnetic field coupling foaming.
Owner:HUBEI XINJIAYUAN IND & TRADE CO LTD

Polymer-derived ceramic thin film thermocouple and preparation method thereof

The present disclosure provides a polymer-derived ceramic thin film thermocouple and a preparation method thereof. The polymer-derived ceramic thin film thermocouple comprises an A electrode and a B electrode, wherein one end of the A electrode and one end of the B electrode intersect and overlap to form hot junctions, an end of the A electrode away from the hot junction and the end of the B electrode away from the hot junction are provided with solder joints. Each solder joint may be connected to a lead wire, the lead wire is configured for output a signal; the A electrode is prepared by mixing a polysilazane solution, nanocomposite powder and a xylene solution, and the nanocomposite is prepared by mixing indium oxide nanopowder, zinc oxide powder and anhydrous ethanol; the B electrode is prepared by mixing a polysilazane solution, indium oxide nanopowder, and a xylene solution.
Owner:ZHONGBEI UNIV

PH-light dual-response nano insecticide and preparation process thereof

The invention relates to the field of pesticides, and particularly discloses a pH-light dual-response nano pesticide and a preparation process thereof. The invention relates to a preparation method of a pH-light dual-response nano insecticide. The preparation method comprises the following steps: adding water into polyethylene glycol, castor oil polyoxyethylene ether and sodium lignin sulfonate to prepare a water phase; the preparation method comprises the following steps: uniformly mixing an efficient cyhalothrin active compound with xylene, and adding diisocyanate to prepare an oil phase; adding the oil phase into the water phase, and adding ethylenediamine, YUS-SC3A, glycerol, xanthan gum, magnesium aluminum silicate and benzoic acid to obtain the lambda-cyhalothrin microcapsule suspending agent. The preparation method comprises the following steps: adding water into YUS-SC3A, uniformly mixing, and adding a clothianidin active compound, glycerol, xanthan gum, magnesium aluminum silicate, AF205 and benzoic acid to obtain a clothianidin suspending agent; mixing the two agents to obtain the nano insecticide, adding the composite dispersant, adding the pre-gel, adding azodiisobutyronitrile, blowing with inert gas, and adding Kathon. By preparing the pH-light dual-response nano insecticide, the insecticidal effect is improved, the generation of drug resistance is avoided, and efficient prevention and control of wheat aphids are realized.
Owner:SHANDONG AOKUN CROP SCI CO LTD

High-temperature oil-stain removing stove cleaner, its preparation method and application

The present application belongs to the technical field of cleaning products, and particularly relates to a high-temperature oil stain removing stove cleaner as well as a preparation method and application thereof. The high-temperature oil stain removing stove cleaner provided by the present application comprises the following components and mass fractions: 11-33 parts of an alkaline additive, 1-2 parts of hydroxyethylidene diphosphonic acid, 3-6 parts of a non-ionic surfactant, 4-8 parts of a solvent, 1-3 parts of a solubilizer, 1-3 parts of sodium xylene sulfonate, and 45-79 parts of water; the solvent comprises ethylene glycol monobutyl ether and diethylene glycol ethyl ether. The high-temperature oil stain removing stove cleaner provided by the present application has the advantages of simple cleaning method, high-temperature oil removing effect, good stain removing and oil scale removing effect on commercial kitchen utensils, high safety, no corrosion to metal, simple raw material composition, and no need to add a defoaming agent.
Owner:BCL HYGIENE MFG CO LTD

C8 aromatic isomerization catalyst, process for its preparation and use

The application provides a C8 aromatic hydrocarbon isomerization catalyst and a preparation method and application thereof. The catalyst contains an active component and a carrier; wherein, based on the weight of the carrier, the carrier contains 5wt%-25wt% of HZSM-23, 5-30wt% of mordenite, 20-60wt% of macroporous alumina and 10wt%-25wt% of a binder component. The method comprises preparation of the carrier and loading of the active metal, wherein the preparation process of the carrier is as follows: HZSM-23 molecular sieve, mordenite, macroporous alumina and a binder are mixed and formed, and the carrier is prepared after drying and calcination. The catalyst is used for C8 aromatic hydrocarbon isomerization reaction, and has the characteristics of high ethylbenzene conversion rate and high xylene yield when the xylene is at an equilibrium concentration.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

A uv-3 ultraviolet absorber and a method for preparing the same

PendingCN122325354AXylyleneChemical synthesis
This application relates to a UV-3 ultraviolet absorber and its preparation method, belonging to the field of chemical synthesis technology. The preparation method employs a one-pot process, in which benzocaine reacts with triethyl orthoformate in xylene solvent. This step utilizes reactive distillation coupling control, continuously removing the generated alcohol distillate through a distillation separation device to promote reaction equilibrium shift, obtaining a xylene solution of the intermediate NET. Subsequently, the solution is heated to a reaction temperature of 135–145°C, and benzyl chloride is added dropwise for N-alkylation, while a tail gas absorption device absorbs byproduct gases. The reaction slurry is then cooled for crystallization, solid-liquid separation, and drying to obtain the UV-3 product. This invention simplifies the production process through a one-pot process, avoids the use of toxic DMF solvent, and solves the technical problem of raw material residues leading to subsequent side reactions in the one-pot process through reactive distillation coupling control, resulting in a final product with high purity and high yield.
Owner:CHANGZHOU YONGHE FINE CHEM

Epoxy zinc-rich primer containing modified graphene and preparation method thereof

The invention discloses an epoxy zinc-rich primer containing modified graphene and a preparation method thereof, and belongs to the technical field of anticorrosive paints.The preparation method comprises the steps that the surface of graphene oxide is carboxylated, then magnesium and cerium ions are used for composite modification, modified graphene oxide is obtained, phenyl Janus-SiO2 particles are synthesized and loaded with a benzotriazole corrosion inhibitor, corrosion inhibition type Janus composite particles are obtained, and the modified graphene oxide is prepared. Finally, xylene, epoxy resin, zinc powder, a dispersing agent, a defoaming agent, heavy calcium carbonate and mica powder are stirred step by step to obtain a component A, an epoxy curing agent, xylene, carboxylated composite powder, corrosion inhibition type Janus composite particles and the dispersing agent are subjected to ultrasonic treatment to prepare a component B, finally, the component A and the component B are evenly mixed, and the epoxy zinc-rich primer containing modified graphene is obtained. The comprehensive performance breakthrough of the primer in the aspects of adhesive force, long-acting corrosion resistance and cathodic disbonding resistance is realized.
Owner:ANHUI JIANGRUI NEW MATERIAL CO LTD

Preparation method and application of graphite / PDMS-based flexible spinning fiber sensor

The invention discloses a preparation method and application of a graphite / PDMS-based flexible spinning fiber sensor. Comprising the following steps: mixing graphite flakes and a PDMS liquid prepolymer, and carrying out ultrasonic stirring; adding a curing agent, continuing ultrasonic stirring uniformly, putting into a vacuum drying oven, standing and defoaming to obtain a spinning solution, putting into an injector, injecting the spinning solution into a coagulating bath through an injection pump to obtain a flexible spinning fiber, immersing into xylene, performing swelling treatment, and then drying; silver wire electrodes are pasted to the two ends of the flexible spinning fiber through conductive adhesive, the silver wire electrodes are wrapped with thermoplastic pipes, and the flexible fiber sensor is obtained; and carrying out cyclic stretching on the flexible fiber sensor by adopting an electronic fatigue testing machine, collecting the resistance in the cyclic stretching process, and stopping cyclic stretching after the resistance reaches a stable state, so as to obtain the graphite / PDMS-based flexible spinning fiber sensor. The sensor is large in sensing strain range and high in sensitivity.
Owner:WUHAN UNIV OF TECH

Directional preparation process of valerian-rich rhizoma nardostachyos essential oil

PendingCN121852137AAchieve targeted enrichmentChange gas-liquid balance distributionEssential-oils/perfumesDipotassium hydrogen phosphateXylylene
The invention relates to the technical field of plant essential oil extraction, and discloses a valerian-rich rhizoma nardostachyos essential oil directional preparation process, which comprises: taking a functionalized compound solvent, adding rhizoma nardostachyos coarse powder according to a liquid-solid ratio, stirring and soaking to obtain a solid-liquid mixture; the solvent component comprises process water, sodium xylene sulfonate, dipotassium phosphate and polyethylene glycol 400; introducing steam into the mixture, heating to maintain slight boiling, carrying out first-stage distillation, and removing distilled low-boiling-point components to obtain resident in the kettle; cooling the resident to a constant temperature, adding sodium chloride, and stirring until the sodium chloride is dissolved to obtain a heterogeneous mixed system; the heating system is subjected to second-stage distillation, and distillate is collected; and carrying out oil-water separation on the distillate, and collecting an oil phase to obtain a finished product of the rhizoma nardostachyos essential oil. According to the method disclosed by the invention, a hydrotropy-salting-out phase change mechanism is matched with fractional distillation, so that high-efficiency desorption and directional enrichment of valerianone which is difficult to volatilize are realized while acidic and light component impurities are removed.
Owner:RANGTANG COUNTY ZANGLANOLIN CULTURE & TECHNOLOGY DEVELOPMENT CO LTD

Corrosion-resistant coatings for electroosmotic reinforcement electrodes and their preparation methods; methods for electrodes and electroosmotic reinforcement of soft soil.

This invention relates to the field of electroosmotic reinforcement technology, and particularly to an anti-corrosion coating for electroosmotic reinforcement electrodes, its preparation method, the electrode, and a method for electroosmotic reinforcement of soft soil. An embodiment of this invention discloses an anti-corrosion coating for electroosmotic reinforcement electrodes. The raw materials, calculated by weight, include: 32-40 parts of organosilicon epoxy resin, 2-4 parts of carbon black, 4-8 parts of graphite, 1-2 parts of carbon fiber filament, 2-4 parts of iron(III) oxide, 0.5-1 part of silver powder, 1-2 parts of organobentonite, 0.5-1.5 parts of talc, 15-20 parts of methyl isobutyl ketone, 8-12 parts of xylene, 3-5 parts of polyvinyl alcohol, 3-8 parts of tributyl phosphate, 0.5-1 part of polysiloxane, 0.5-1 part of polyethylene glycol, 1-5 parts of butyl butyrate, and 1-5 parts of polyaniline. The anti-corrosion coating used in this invention, when applied to the electrode for electroosmotic reinforcement, exhibits excellent conductivity and anti-corrosion properties, as well as good sealing performance and resistance to cracking.
Owner:GUANGDONG POWER GRID CO LTD +1