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8088 results about "Hydrochloric acid" patented technology

Hydrochloric acid or muriatic acid is a colorless inorganic chemical system with the formula HCl:H2O and is a ionically bonded acid. Hydrochloric acid has a distinctive pungent smell. It is classified as strongly acidic and can attack the skin over a wide composition range, since the hydrogen chloride completely dissociates in aqueous solution.

Compounds and combinations thereof for treating neurological and psychiatric conditions

ActiveUS12364674B2Organic active ingredientsNervous disorderDextromethorphan HydrobromideDepressant
This disclosure relates to administration of a combination of: 1) about 100-110 mg, about 104-106 mg, or about 105 mg of bupropion hydrochloride, or a molar equivalent amount of the free base form or another salt form of bupropion; and 2) about 40-50 mg, about 44-46 mg, or about 45 mg of dextromethorphan hydrobromide, or a molar equivalent amount of the free base form or another salt form of dextromethorphan in certain patient populations, such as patients having moderate renal impairment, patients receiving a concomitant strong CYP2D6 inhibitor, patients who are known CYP2D6 poor metabolizers, those in need of an NMDA antagonist that does not cause dissociation, and those at risk of QT prolongation.
Owner:ANTECIP BIOVENTURES II LLC

High-strength concrete and preparation method thereof

PendingCN120271293AFiberCrack resistance
The invention relates to the field of concrete, and provides high-strength concrete and a preparation method thereof, and the high-strength concrete comprises modified basalt chopped fiber, a self-repairing agent, cement, fly ash, slag powder, coarse aggregate, natural sand, a water reducing agent and an air entraining agent. The modified basalt chopped fiber is oxidized by hydrogen peroxide, etched by hydrochloric acid and modified by a nano silicon dioxide coating, so that the interface bonding force is enhanced. The self-repairing agent is prepared by adopting expanded perlite to load bacillus through thallus culture, purification, dipping adsorption and low-temperature vacuum drying, CaCO3 deposition can be induced at concrete cracks, and self-repairing is achieved. The invention further provides a preparation method of the concrete. The preparation method comprises the steps of aggregate screening, hydrated liquid preparation, wet mixing, fiber and self-repairing agent adding, vibration forming and curing. The crack resistance of the concrete is improved by enhancing the fiber-matrix interface bonding force, meanwhile, the service life of the concrete is prolonged by utilizing a biological self-repairing technology, and the concrete is suitable for high-durability concrete engineering.
Owner:SHENZHEN LIJIAN CONCRETE CO LTD

Process for the preparation of (2-(3,6-dimethoxy-9H-carbazol-9-yl)ethyl)phosphonic acid

The application provides a process method for preparing (2-(3,6-dimethoxy-9H-carbazol-9-yl)ethyl) phosphonic acid, and particularly relates to the technical field of organic synthesis. The process method is that, under alkaline conditions, a halogenated phosphonate compound is added into a 3,6-dimethoxy-9H-carbazole solution to perform a reaction, hydrochloric acid aqueous solution is added after the reaction to perform acidolysis degreasing, and finally (2-(3,6-dimethoxy-9H-carbazol-9-yl)ethyl) phosphonic acid is obtained through extraction, reflux adsorption and beating purification. The process method uses 3,6-dimethoxy-9H-carbazole as a starting material, realizes the synthesis of the target product through one-pot reaction, has mild reaction conditions, uses non-toxic raw materials which are easy to obtain, has simple synthesis process, is convenient to operate, and has high separation yield.
Owner:DAGAO IND TECH RES INST (GUANGZHOU) CO LTD

Compounds and combinations thereof for treating neurological and psychiatric conditions

This disclosure relates to administration of a combination of: 1) about 100-110 mg, about 104-106 mg, or about 105 mg of bupropion hydrochloride, or a molar equivalent amount of a free base form or another salt form of bupropion; and 2) about 40-50 mg, about 44-46 mg, or about 45 mg of dextromethorphan hydrobromide, or a molar equivalent amount of a free base form or another salt form of dextromethorphan in certain patient populations, such as patients having moderate renal impairment, patients receiving a concomitant strong CYP2D6 inhibitor, patients who are known CYP2D6 poor metabolizers, those in need of an NMDA antagonist that does not cause dissociation, and those at risk of QT prolongation.
Owner:ANTECIP BIOVENTURES II LLC

Preparation and application of chemical copper plating cellulose composite fiber

The invention belongs to the field of new materials, and particularly relates to preparation and application of chemical copper plating cellulose composite fibers. The preparation method of the composite fiber comprises the following steps: (1) mixing absolute ethyl alcohol, ammonia water and water in proportion, adding cellulose fiber, heating, stirring and uniformly mixing, adding a dopamine hydrochloride solution, washing and drying to obtain a polydopamine coating / cellulose composite fiber; (2) adding the composite fiber prepared in the step (1) into an alkaline solution, adding a silver nitrate solution, stirring, washing and drying to obtain a polydopamine reduced nano-silver / cellulose composite fiber; and (3) adding the composite fiber obtained in the step (2) into a chemical plating solution containing copper ions for plating to obtain the chemical copper-plated cellulose composite fiber. The electroless copper-plated cellulose composite fiber shows outstanding electric heating and photo-thermal properties, can accurately capture electrocardiosignals of a human body before and after movement at the same time, and provides a new thought for development of wearable electronic fabrics and intelligent sensors.
Owner:ZHENGZHOU UNIV

Pre-sodium-modified negative electrode dry-method electrode and preparation method thereof

The preparation method comprises the following steps: S1, mixing a hydrochloric acid solution with organic sodium sulfonate, then adding aniline and water, stirring and dissolving, then adding an oxidizing agent to carry out doping reaction, and carrying out suction filtration, washing, drying and grinding on a reaction product to obtain sodium-modified polyaniline; s2, uniformly mixing a negative electrode active material, a conductive agent and polytetrafluoroethylene, and then adding sodium polyaniline and an organic sodium supplement agent in a nitrogen or inert atmosphere for fibration treatment to obtain fibration powder; and S3, performing hot pressing on the fiberized powder onto the current collector to obtain the lithium ion battery. The prepared pre-sodium-modified negative electrode dry-method electrode has relatively good peeling strength and pole piece flexibility, and the condition that a traditional wet-method thick electrode is easy to crack is relieved; meanwhile, the dry-method electrode subjected to sodium modification treatment can induce uniform deposition of sodium ions, so that the dynamic performance of the whole sodium battery is improved, the problem of cyclic sodium precipitation is avoided, and the service life of the battery is further prolonged.
Owner:XIAOGAN CORNEX NEW ENERGY INNOVATION TECHNOLOGY CO LTD

Porous titanium-based implant with photo-thermal surface as well as preparation method and application of porous titanium-based implant

The invention discloses a porous titanium-based implant with a photo-thermal surface and a preparation method and application of the porous titanium-based implant, and belongs to the technical field of biomedical materials. The preparation method comprises the steps that a porous titanium substrate is prepared through 3D printing, then flowing acid etching treatment and anodic oxidation treatment are conducted in sequence, then the porous titanium substrate is placed in photo-thermal coating dispersion liquid for reaction, cleaning and drying are conducted, and the porous titanium-based implant with the photo-thermal surface is obtained. The photo-thermal coating dispersion liquid is obtained by dispersing MXene-ZnO composite particles in a dopamine hydrochloride solution. The porous titanium-based implant provided by the invention can be rapidly heated to a proper temperature under the irradiation of near-infrared light, and has good antibacterial, anti-tumor and osteogenesis promoting properties and biocompatibility.
Owner:SHANDONG UNIV

Composition containing dendrobium officinale enzymolysis extract as well as preparation method and application of composition

The invention relates to the technical field of cosmetics, and provides a composition containing a dendrobium officinale enzymolysis extract, which is prepared from the following components in percentage by mass: 18 to 22 percent of dendrobium officinale enzymolysis extract, 9 to 11 percent of chitosan oligosaccharide, 6.5 to 7.5 percent of bionic moisturizing enhancer, 0.1 to 0.2 percent of sodium alginate, 0.05 to 0.15 percent of citric acid / sodium citrate buffer pair and 60.4 to 65.4 percent of solvent matrix. By combining low-temperature enzymolysis with a biological purification process, efficient extraction of dendrobium candidum polysaccharides and phenolic substances is realized, dendrophenol oxidation inactivation caused by high temperature can be effectively avoided, hydrochloric acid residues in chitosan oligosaccharide preparation are effectively removed, formula irritation is remarkably reduced, and the dendrobium candidum extract is more suitable for sensitive skin care; the components in the composition have a synergistic effect, the dendrobium officinale enzymolysis extract and the enzymolysis chitosan oligosaccharide form a composite moisturizing network, the moisturizing rate is remarkably increased, the oxidation resistance is remarkably improved, and the composition can be applied to products such as essence, masks and freeze-dried powder.
Owner:XINKANGMEI (FUJIAN) COSMETICS CO LTD

Compounds and combinations thereof for treating neurological and psychiatric conditions

This disclosure relates to administration of a combination of: 1) about 100-110 mg, about 104-106 mg, or about 105 mg of bupropion hydrochloride, or a molar equivalent amount of the free base form or another salt form of bupropion; and 2) about 40-50 mg, about 44-46 mg, or about 45 mg of dextromethorphan hydrobromide, or a molar equivalent amount of the free base form or another salt form of dextromethorphan in certain patient populations, such as patients having moderate renal impairment, patients receiving a concomitant strong CYP2D6 inhibitor, patients who are known CYP2D6 poor metabolizers, those in need of an NMDA antagonist that does not cause dissociation, and those at risk of QT prolongation.
Owner:ANTECIP BIOVENTURES II LLC

Method for recycling lithium iron phosphate powder with iron salts and recovering all components

This invention discloses a method for leaching lithium iron phosphate mixed powder with iron salts and recovering all components, belonging to the field of battery recycling. The invention uses an iron salt solution to leach the mixed powder, obtaining a lithium-containing leachate and leaching residue. Ferrous ions in the leachate are regenerated into ferric iron through acidification and oxidation, and recycled for leaching the next batch of mixed powder. After reaching a preset number of cycles, the leachate is used for re-leaching multiple batches of leaching residue to improve the lithium leaching rate. Ultimately, a enriched solution containing Li, Fe, Cu, and Al and graphite-containing iron phosphate residue are obtained. Copper is recovered from the enriched solution through iron powder replacement, and a high-purity lithium chloride solution is obtained through extraction and separation, while ferric chloride (recycled) and aluminum chloride crystals are also recovered. The leaching residue is treated with hydrochloric acid to obtain regenerated graphite, and the pH is adjusted with alkali to obtain high-purity iron phosphate. This method achieves full component recovery under mild conditions, reducing separation steps and chemical consumption through a "leaching-regeneration-leaching" cycle mechanism, thus achieving both environmental and economic benefits.
Owner:ZHEJIANG UNIV +1

Bupropion as a modulator of drug activity

This disclosure relates to administration of a combination of: 1) about 100-110 mg, about 104-106 mg, or about 105 mg or less of bupropion hydrochloride, or a molar equivalent amount of the free base form or another salt form of bupropion; and 2) about 40-50 mg, about 44-46 mg, or about 45 mg or less of dextromethorphan hydrobromide, or a molar equivalent amount of the free base form or another salt form of dextromethorphan in human patients for treating neurological and psychiatric conditions, such as agitation associated Alzheimer's disease and / or reducing relapse of agitation in Alzheimer's disease.
Owner:ANTECIP BIOVENTURES II LLC

Method for preparing fiber-reinforced coal gangue-based composite functional aerogel

The invention belongs to the field of coal gangue resource utilization, and particularly discloses a method for preparing fiber-reinforced coal gangue-based composite functional aerogel. After being activated, the coal gangue is put into an acid leaching solution to be leached, and an aluminum-rich solution is obtained; adding ammonia water into the aluminum-rich solution to adjust the pH to obtain hydroxide precipitate; adding a sodium hydroxide solution into the precipitate to react to obtain a sodium aluminate solution; neutralizing the sodium aluminate solution with hydrochloric acid to obtain an aluminum chloride solution, stirring to obtain aluminum sol, and adding ceramic fibers into the aluminum sol; violently stirring the sol, and adding epoxypropane to obtain wet gel; after aging the wet gel, carrying out surface modification to obtain hydrophobic coal gangue-based aluminum oxide and composite wet gel of the hydrophobic coal gangue-based aluminum oxide; and drying the modified wet gel at normal pressure to obtain the hydrophobic coal gangue-based aluminum oxide and the composite aerogel thereof. Ceramic fibers are introduced as a reinforcing phase, so that the compressive strength and toughness of the material are improved; the composite aerogel is subjected to surface modification, uniform modification is ensured, the contact angle is remarkably increased, the hygroscopicity is reduced, and the stability of the material is enhanced.
Owner:CHANGZHOU UNIV

Compounds and combinations thereof for treating neurological and psychiatric conditions

This disclosure relates to administration of a combination of: 1) about 100-110 mg, about 104-106 mg, or about 105 mg of bupropion hydrochloride, or a molar equivalent amount of the free base form or another salt form of bupropion; and 2) about 40-50 mg, about 44-46 mg, or about 45 mg of dextromethorphan hydrobromide, or a molar equivalent amount of the free base form or another salt form of dextromethorphan in certain patient populations, such as patients having moderate renal impairment, patients receiving a concomitant strong CYP2D6 inhibitor, patients who are known CYP2D6 poor metabolizers, those in need of an NMDA antagonist that does not cause dissociation, and those at risk of QT prolongation.
Owner:ANTECIP BIOVENTURES II LLC

Superfine tungsten powder and preparation method thereof

ActiveCN120228281ATungstateArgon atmosphere
The invention belongs to the technical field of superfine tungsten powder, and particularly relates to superfine tungsten powder and a preparation method thereof.The preparation method includes the steps that an ammonium tungstate solution, hydrochloric acid and carbon black serve as raw materials to prepare a mixture of tungstic acid and a carbon precursor; calcining the tungstic acid and carbon precursor mixture in a nitrogen atmosphere to obtain a tungsten oxide and carbon mixture; a tungsten oxide and carbon mixture is calcined in an argon atmosphere, the argon atmosphere is kept for natural cooling, the superfine tungsten powder is obtained, the superfine tungsten powder is uniform in dispersion, complete in grain development, smooth in surface, free of pores and complex in morphology, the crystal structure of the superfine tungsten powder is a body-centered cube, the average particle size is smaller than or equal to 0.7 micrometer, and the specific surface area is smaller than or equal to 1.0 m < 2 > / g.
Owner:CHONGYI ZHANGYUAN TUNGSTEN

Method for preparing bismuth ferrite composite catalytic material by using red mud as well as product and application of bismuth ferrite composite catalytic material

The invention discloses a method for preparing a bismuth ferrite composite catalytic material by using red mud as well as a product and application of the bismuth ferrite composite catalytic material. The method comprises the following steps: mixing chlorine salt and red mud, uniformly stirring, adding a hydrochloric acid solution, uniformly stirring, roasting, recovering flue gas generated in the roasting process, and obtaining roasting residues and roasting dust generated by recovering the flue gas after roasting is finished; and mixing the roasted dust and bismuth nitrate, uniformly stirring, adding the calcined residue, uniformly grinding, adding water, stirring, drying the material, and calcining to obtain the bismuth ferrite composite catalytic material. The preparation process is simple, the red mud is used as a main raw material, and full-amount resource utilization of the red mud can be achieved. The prepared composite catalytic material can be used for efficiently purifying landfill leachate, and COD, ammonia nitrogen, total phosphorus and heavy metal pollution are efficiently removed through a photocatalysis mechanism.
Owner:CHANGSHU INSTITUTE OF TECHNOLOGY

Flexible EVA cable sheath material and preparation method thereof

The invention relates to the technical field of cable materials, and provides a flexible EVA cable sheath material and a preparation method thereof. The cable sheath material is prepared from the following raw materials in parts by weight: 25 to 50 parts of ethylene-vinyl acetate copolymer EVA, 15 to 30 parts of ultra-low density polyethylene, 2 to 10 parts of grafted EVA, 2 to 10 parts of flame retardant, 2 to 10 parts of polydopamine modified montmorillonite-boron nitride fiber composite material, 0.5 to 3 parts of flexibilizer, 0.2 to 1 part of silicone and 0.2 to 1 part of organopolysiloxane. A grafting monomer for grafting EVA comprises maleic anhydride and / or an acrylate compound; the polydopamine modified montmorillonite-boron nitride fiber composite material is prepared from montmorillonite, boron nitride fibers, hydroxylated lignin, dopamine hydrochloride and polyethyleneimine through a reaction. Various functional raw materials are compounded, and the obtained cable sheath has good flexibility, flame retardance, thermal deformation resistance, aging resistance and mechanical performance.
Owner:GUANGZHOU PANYU CABLE WORKS

System and method for producing activated carbon material from cow dung

The present invention generally relates to a system for producing activated carbon from cow dung. The process begins with a drying and washing unit to pre-treat the raw material. Dried cow dung is then milled and sieved to a specific particle size. A second drying step prepares the sieved material for carbonization in a nitrogen atmosphere. The resulting carbonized material undergoes chemical activation using a sodium hydroxide solution. Subsequent pyrolysis in a nitrogen environment further develops the pore structure of the activated carbon. The pyrolyzed material is then washed with hydrochloric acid to remove impurities. A final drying step yields the desired activated carbon product, which is then crushed. This system provides a controlled and efficient method for converting cow dung into valuable activated carbon, offering a sustainable waste management solution and a source of high-quality material for various applications.
Owner:PRINCESS NORA BINT ABDULRAHMAN UNIV

Device and method for controlling PH of hydrochloric acid in germanium oxide production process

The embodiment of the invention provides a hydrochloric acid PH control device in a germanium oxide production process and a control method thereof, and belongs to the field of chemical process automatic control. The device comprises an acid liquor storage tank used for storing raw liquor hydrochloric acid and connected to an acid mixing tank through a raw acid feeding control valve; the acid mixing tank is used for mixing an acid solution with a diluent and is connected to the pH regulation reaction tank through a mixed acid feeding control valve; the alkali liquor storage tank is connected to the pH regulation reaction tank through an alkali liquor adding control valve; the pH regulation reaction tank is used for receiving the mixed acid liquor and the alkali liquor and regulating the pH value of a reaction system, and is provided with a pH sensor for detecting the pH value in real time; and the control unit is used for dynamically adjusting the opening degree of each valve by adopting an improved fuzzy self-adaptive PID control algorithm according to a detection result of the pH sensor so as to control the pH value to be within a target range. According to the scheme, the problems of overshoot and lag caused by traditional fixed parameter PID adjustment are solved, and therefore the stability of the pH value of the solution and the consistency of the technology in the germanium oxide production process are guaranteed.
Owner:SICHUAN HIGH GERMANIUM RENEWABLE RESOURCES CO LTD

High-temperature-resistant lignite resin and preparation method thereof

The invention discloses a high-temperature-resistant lignite resin and a preparation method thereof, and belongs to the field of drilling fluids, and the preparation method comprises the following steps: obtaining and preparing an extracting solution containing humic acid from lignite; adding hydrochloric acid into the extracting solution, separating, filtering and precipitating, dissolving the precipitating in a sodium hydroxide solution to obtain a humic acid solution, adding formaldehyde and sodium pyrosulfite into the humic acid solution, preheating to 80 DEG C, adding the extracting solution, heating to 110-130 DEG C, continuously stirring, reacting for 1-3 hours, and cooling to 60 DEG C or below to obtain a reaction product; transferring a reaction product to a neutralizing tank, dropwise adding a NaOH solution, adjusting the pH value to 10-11, and controlling the temperature below 55 DEG C; the mass ratio of the dry basis mass of sulfonated humic acid to ECH is 1: (0.05-0.15), the temperature is kept at 45-55 DEG C, the stirring speed is 400-600 rpm, and the reaction is performed for 2-4 hours; meanwhile, a NaOH solution is continuously added, and the pH is kept at 10-11. Adjusting the pH value of the reaction liquid to 7-8 by using dilute HCl, and terminating the reaction; and obtaining a resin product.
Owner:WUHAI SHENGSHIYUAN PETROLEUM TECH CO LTD

Carbon-doped titanium dioxide nanotube-molybdenum disulfide energy-storage antibacterial material and preparation method thereof

The invention discloses a carbon-doped titanium dioxide nanotube-molybdenum disulfide energy-storage antibacterial material and a preparation method thereof. The preparation method comprises the following steps: carrying out primary anodic oxidation on a clean titanium foil in a mixed electrolyte of ethylene glycol, water and ammonium fluoride; after ultrasonic treatment is carried out in a hydrochloric acid solution for set time, secondary anodic oxidation is carried out, and the mixed electrolyte of the secondary anodic oxidation is the same as that of the primary anodic oxidation; annealing the titanium foil subjected to anodic oxidation twice in an argon atmosphere, putting an annealed sample into a mixed solution of sodium molybdate, a sulfur source and glucose, and carrying out hydrothermal treatment; and the titanium foil subjected to hydro-thermal treatment is cleaned and dried, and the carbon-doped titanium dioxide titanium foil with the surface covered with molybdenum disulfide is obtained. The MoS2-coated carbon-doped titanium dioxide nanotube (TNT-C-atMoS2) with high biocompatibility developed by the invention has a synergistic effect of charge antibiosis and chemical sterilization, so that the problem of intractable biological fouling of a titanium-based metal material in ocean engineering equipment is effectively solved.
Owner:SHANDONG UNIV

Double-layer carbon-coated sodium ion battery hard carbon negative electrode material as well as preparation method and application thereof

The invention belongs to the technical field of sodium ion negative electrode material preparation, and particularly relates to a double-layer carbon-coated sodium ion battery hard carbon negative electrode material as well as a preparation method and application thereof. The method comprises the following steps: firstly, dispersing activated carbon powder into a tris (hydroxymethyl) aminomethane hydrochloride buffer solution, and then adding dopamine hydrochloride to carry out self-polymerization reaction, so as to obtain activated carbon powder coated with a first layer of polydopamine; then putting the activated carbon powder into a second layer of carbon source precursor solution, and heating in a water bath to obtain double-layer carbon-coated activated carbon powder; and finally, carrying out heat treatment. The preparation method comprises the following steps: firstly, coating the surface of activated carbon with a first layer of polydopamine by an in-situ polymerization method, then promoting uniform coating of a second layer of carbon source precursor by utilizing strong adhesion of the polydopamine, and carrying out heat treatment to obtain the double-layer carbon-coated hard carbon negative electrode material. The hard carbon negative electrode material can improve the energy density of the current sodium ion battery and accelerate the industrial application of the sodium ion battery.
Owner:NANCHANG UNIV

High-toughness ultrathin flexible glass and preparation method thereof

The invention discloses high-toughness ultrathin flexible glass and a preparation method thereof, and relates to the technical field of glass manufacturing. The ultrathin flexible glass is prepared from the following raw materials: silicon dioxide, aluminum oxide, lithium oxide, sodium oxide, magnesium oxide, a modified nano reinforced phase, a high-temperature melting regulator and cerium dioxide. The modified nano reinforced phase is prepared by the following steps: pre-treating silicon carbide and silicon nitride with hydrochloric acid, and mixing with nano zirconium oxide to obtain a mixture; and modifying the mixture with a silane coupling agent to obtain the modified nano reinforced phase. The high-temperature melting regulator is a mixture of lithium borate, sodium sulfate and lithium fluoride. The preparation method of the ultra-thin flexible glass comprises the following steps: preparing the modified nano reinforced phase, melting and homogenizing the glass, forming the glass substrate, and preparing the ultra-thin flexible glass. The ultra-thin flexible glass prepared by the invention has relatively high fracture toughness and structural rigidity, excellent flexibility and bending fatigue durability, and excellent thermal shock resistance.
Owner:LONGGUANGTIANXU SOLAR ENERGY ZHUCHENG

Waste oil-mediated preparation method of global low-defect pseudographite domain-rich hard carbon material and method and high-rate sodium storage

The invention belongs to the technical field of batteries, and particularly relates to a waste oil mediated preparation method of a whole-domain low-defect pseudographite domain-rich hard carbon material and a method and high-rate sodium ion energy storage. The preparation method comprises the following steps: uniformly mixing and stirring dried biomass and waste grease, putting the mixture into a tubular furnace, heating under protective gas, carrying out high-temperature carbonization, washing with a diluted hydrochloric acid solution and deionized water in sequence, and drying to obtain the waste oil mediated whole-domain low-defect pseudo-graphite domain high-rate hard carbon negative electrode material. According to the waste oil mediated global low-defect and pseudo-graphite domain-enriched high-rate hard carbon negative electrode material obtained by the invention, the structural stability of the material in an ion intercalation / deintercalation process is enhanced, the cycle life of an electrode is effectively prolonged, the high-rate performance of the material can be considered while the platform capacity is ensured, and the service life of the material is prolonged. And it is ensured that the electrode can still maintain high capacity output and good cycling stability under the large-current charging and discharging condition.
Owner:QILU UNIVERSITY OF TECHNOLOGY (SHANDONG ACADEMY OF SCIENCES)

Hydrogel patch for gastric perforation repair and preparation method thereof

The invention discloses a hydrogel patch for gastric perforation repair and a preparation method thereof, and belongs to the technical field of biomedical materials. The preparation method comprises the following steps: dissolving acryloyl valine, acrylic acid, methylene bisacrylamide, a compound A and a photoinitiator in an alcohol solvent, and defoaming to obtain a precursor solution; and placing the precursor solution in a mold, carrying out ultraviolet-induced curing, soaking the obtained hydrogel in a hydrochloric acid solution, and replacing the alcohol solvent to obtain the hydrogel patch for gastric perforation repair. The hydrogel patch provided by the invention has the advantages of strong acid corrosion resistance, good biocompatibility, low swelling ratio, stable adhesion performance in a fluctuating pH environment and the like. The tough and stable adhesion performance ensures that the hydrogel can be permanently and reliably adhered to a gastric perforation part in a dynamic gastric acid environment, and a stable platform is provided for drug delivery, so that the surgical operation time is expected to be shortened, and wound healing is promoted.
Owner:ZHEJIANG UNIV

Antibacterial nylon material as well as preparation method and application thereof

The invention relates to the technical field of antibacterial high polymer materials, in particular to an antibacterial nylon material as well as a preparation method and application thereof. The method comprises the following steps: carrying out anion ring-opening copolymerization on a seven-membered ring lysine monomer obtained by ring formation of lysine and a lactam monomer to obtain copolyamide, dissolving the copolyamide, and carrying out complete quaternization reaction by using halogenated hydrocarbon to obtain the antibacterial nylon material. The preparation method provided by the invention effectively avoids the problems of insufficient antibacterial property, obvious mechanical property reduction, poor thermal stability and the like of an antibacterial nylon material prepared by hydrochloric acid protonation in the prior art. Meanwhile, the seven-membered cyclic lysine monomer can be copolymerized without alkylation, the synthesis process is greatly simplified, the production efficiency is high, and the production cost is low. The prepared antibacterial nylon material has the characteristics of lasting and efficient antibacterial performance, high safety, environment friendliness, excellent mechanical property and thermal stability and the like, and can be widely applied to the fields of textiles, daily necessities, packaging materials, panels and the like.
Owner:CHANGCHUN INSTITUTE OF APPLIED CHEMISTRY CHINESE ACADEMY OF SCIENCES

High-cracking-resistance concrete and preparation method thereof

The invention relates to the field of concrete, and provides high-cracking-resistance concrete and a preparation method thereof.The concrete comprises a surface modified rubber fiber composition, surface modified end-hooked steel fibers, Portland cement, fly ash, silica fume, a superplasticizer, mineral powder, coarse aggregate, fine aggregate and water. The surface modified rubber fiber composition is composed of millimeter-sized and micron-sized rubber fibers, and is subjected to alkali treatment, oxidative sulfonation and amination modification, so that the cement compatibility and interface bonding force of the fibers are improved; the surface modified end-hooked steel fiber is subjected to dopamine hydrochloride auto-polymerization deposition and drying curing treatment, and the reinforcing effect is improved. The preparation method comprises the steps of fiber pretreatment, admixture mixing, aggregate dry mixing, slurry preparation, fiber uniform dispersion and concrete forming maintenance, and material uniformity and performance stability are ensured. By optimizing fiber modification and component proportion, the cracking resistance and durability of the concrete are improved, and the concrete is suitable for high-performance building structures and engineering application.
Owner:SHENZHEN LIJIAN CONCRETE CO LTD

Solar interface evaporator and preparation method and application thereof

The invention discloses a solar interface evaporator and a preparation method and application thereof. The evaporator comprises a porous cellulose supporting layer and a photo-thermal composite hydrogel layer loaded on the cellulose supporting layer, and the porous cellulose supporting layer and the photo-thermal composite hydrogel layer are combined in a gel in-situ cross-linking mode to form an integrated composite structure. The photo-thermal composite hydrogel layer is composite hydrogel formed by cross-linking polyvinyl alcohol, chitosan quaternary ammonium salt and carbon black. The preparation method comprises the following steps: adding polyvinyl alcohol and chitosan quaternary ammonium salt into a solvent to form a transparent mixed solution, adding the carbon-based photothermal conversion material, and continuously heating and stirring to prepare a hydrogel precursor solution; then adding glutaraldehyde and hydrochloric acid, and carrying out cross-linking reaction to form a hydrogel system; and immersing the cellulose sponge, standing, circularly and alternately freezing and unfreezing, and finally freeze-drying to obtain the product. The evaporator disclosed by the invention integrates highlight absorption, high heat utilization, water transportation, salt resistance and antibiosis, can realize large-scale production, and is suitable for scenes such as seawater desalination, sewage purification and emergency water supply.
Owner:SOUTHEAST UNIV

Fermentation medium for regulating and controlling target product of clostridium aerovorans and fermentation method of fermentation medium

The invention discloses a fermentation medium for regulating and controlling a clostridium aerovorans target product and a fermentation method of the clostridium aerovorans target product. The medium comprises a basic component and a regulating component, the basic components comprise ammonium chloride, potassium chloride, magnesium sulfate heptahydrate, sodium chloride, monopotassium phosphate, yeast powder, calcium chloride dihydrate, sodium selenite, nickel chloride hexahydrate, biotin, folic acid, pyridoxine hydrochloride, thiamine, riboflavin, nicotinic acid, D-calcium pantothenate, cobalamin, para aminobenzoic acid and lipoic acid; the adjusting component comprises sodium tungstate, ferrous sulfate and sodium molybdate, sodium tungstate and ferrous sulfate have a forward adjusting effect on increasing the yield of acetic acid, ethanol and butanol in the target product, and sodium molybdate has a reverse adjusting effect on the target product. By optimizing the proportion of trace elements in the culture medium, the clostridium metabolism efficiency is improved, synthesis of a target product is regulated and controlled, and the method is particularly suitable for industrial production of acetic acid, ethanol, butanol and the like.
Owner:NANJING SHIQI BIOCHEMICAL TECH CO LTD

Recycling method of waste photovoltaic panel

The invention relates to a waste photovoltaic panel recycling method which comprises the following steps: crushing a waste photovoltaic panel until the size of the waste photovoltaic panel is 80-160 meshes, and preparing powder; carrying out acid leaching treatment on the powder, and respectively collecting a leaching solution and a solid material; an acid leaching solution adopted in the acid leaching treatment is a mixed acid aqueous solution of hydrochloric acid and sulfuric acid; the pH of the leachate is adjusted to be neutral with an alkaline agent, then the leachate is mixed with metal iron to be subjected to a replacement reaction, and metal copper is prepared; the solid material is mixed with water, hydrofluoric acid and a flotation agent are added into the obtained mixture for flotation treatment, floats and precipitates are collected respectively, the floats comprise silicon powder, the precipitates comprise glass powder, and the flotation agent comprises one or two of hexadecyl potassium hydrogen phosphate and sodium dodecyl sulfate. According to the recycling method, the silicon powder, the glass powder and the metal copper can be comprehensively recycled from the waste photovoltaic panel.
Owner:HEFEI INSTITUTE OF PHYSICAL SCIENCE CHINESE ACADEMY OF SCIENCES

Electrochromic fabric and its preparation method

The present invention provides an electrochromic fabric and a preparation method thereof. The conductive fabric is treated to make its surface rich in active functional groups; oxalic acid and sodium tungstate solution are mixed, hydrochloric acid is added to adjust the pH, and then n-butanol is added to obtain a precursor solution. The fabric is placed in the precursor solution for high-temperature reaction to obtain the electrochromic fabric. By pre-treating the fabric, the number of functional groups on the fabric surface is increased, and adjusting the pH enhances the binding force between WO3 and the fabric; n-butanol ensures the stable formation of tungsten trioxide, promotes the interaction between oxalic acid and the functional groups on the fabric surface, improves the interfacial interaction force between the WO3 crystal nucleus and the fabric, and at the same time affects the crystal nucleus growth direction, forming a nanorod-like or three-dimensional microsphere structure, and improving the electrochromic performance. Through the synergistic cooperation of each process and related parameters, the electrochromic fabric of the present invention has obvious color change, good cycle stability and high mechanical properties; and the process is simple, the cost is low, and it is suitable for industrial mass production.
Owner:WUHAN TEXTILE UNIV