The invention relates to the technical field of aluminum
nitride synthesis, provides a preparation method of low-
oxygen-content aluminum
nitride powder, and solves the problems of
high oxygen content of a product, difficulty in control of a reaction process and relatively high production cost when the aluminum
nitride powder is prepared by a traditional
combustion synthesis method. Comprising the following steps: S1, mixing aluminum
powder, aluminum nitride powder and
ammonium salt to obtain mixed powder; s2, the mixed powder is laid in a
metal material frame, an ignition wire is fixed, and an ignition agent is added; s3, the mixture is placed in a high-pressure
combustion synthesis reaction kettle,
nitrogen is introduced after gas washing and vacuumizing are conducted, current is introduced to ignite an ignition agent, a self-propagating
combustion synthesis reaction is induced, cooling and pressure relief are conducted after the reaction is completed, a product is taken out, and micron-sized aluminum nitride powder is obtained through fine
grinding; and S4, taking the micron-sized aluminum nitride powder as an aluminum nitride
raw material, re-mixing the micron-sized aluminum nitride powder with the corresponding parts by weight of the aluminum powder and the
ammonium salt according to the proportion in S1, and repeating the steps from S1 to S3 for six times to obtain the low-
oxygen-content aluminum nitride
ceramic powder.