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146 results about "Vacuum evaporation" patented technology

Vacuum evaporation is the process of causing the pressure in a liquid-filled container to be reduced below the vapor pressure of the liquid, causing the liquid to evaporate at a lower temperature than normal. Although the process can be applied to any type of liquid at any vapor pressure, it is generally used to describe the boiling of water by lowering the container's internal pressure below standard atmospheric pressure and causing the water to boil at room temperature.

An integrated vacuum air circulation system for the exterior of a vacuum evaporation machine

This invention proposes an integrated vacuum pumping system for the exterior of a vacuum evaporation machine, comprising a coarse pumping pipe and a fine pumping pipe. A first three-way pipe and the fine pumping pipe are connected by a telescopic motor that drives the valve cover to rise and fall, enabling rapid switching between the coarse and fine pumping lines and avoiding vacuum fluctuations. Under the precise pressure control of the telescopic motor, the valve cover maintains uniform contact pressure on the sealing surface. The transition pipe directly connects the coarse and fine pumping pipes, eliminating flow channel redundancy in traditional multi-valve systems and reducing gas flow resistance. The telescopic motor is linked with a vacuum sensor to automatically switch the pumping mode based on the cavity pressure threshold, avoiding errors caused by manual intervention. The integrated three-way pipe reduces external connecting components, shrinks the equipment size, and lowers manufacturing costs and maintenance complexity.
Owner:SUZHOU YOULUN VACUUM EQUIP TECH CO LTD

Preparation method of white organic light-emitting diode based on a kind of sub-copper complex

The present application relates to the technical field of organic optoelectronic materials and devices, in particular to a preparation method of white organic light-emitting diodes based on a kind of blue, yellow and other color cMa copper (I) TADF complex with nitrogen heterocyclic carbene-copper-arylamines structure, including three steps: first, synthesis of cMa type copper (I) TADF complex containing blue light emitter and yellow light emitter as representative, obtained by ligand selection, intermediate preparation and purification;Second, construct layered WOLEDs device, from bottom to top in turn for substrate, ITO anode, hole injection layer, hole transport layer, buffer layer, yellow light emitting layer, blue light emitting layer, electron transport layer, electron injection layer and Al cathode;Third, through substrate pretreatment, mbar high vacuum evaporation and nitrogen glove box packaging complete device preparation.The WOLEDs device W1, W2 prepared by the present application has excellent photoelectric performance, the CRI is up to 83, the maximum external quantum efficiency is greater than or equal to 13.3%, has good stability and low cost, and is suitable for lighting and display fields.
Owner:BEIJING INFORMATION SCI & TECH UNIV +1

Carbon nanotube composite charge generation layer and preparation method thereof, and laminated OLED device

The application provides a carbon nanotube composite charge generation layer, a preparation method thereof and application of the carbon nanotube composite charge generation layer in a laminated OLED device. The preparation method comprises the following steps: placing a ferrous oxide loaded carbon nanotube composite material in a solvent to obtain a solution, spraying the solution on a substrate surface, drying to obtain a modified base film; placing the modified base film in a magnetic field with a fixed direction and a fixed frequency to obtain a modified base film with oriented arrangement of carbon nanotubes; and preparing the carbon nanotube composite charge generation layer by using a high-vacuum evaporation method. Compared with the prior art, the carbon nanotube material with regular arrangement is obtained, the axial conductivity of the carbon nanotube material is far higher than the radial conductivity, the traditional evaporation process is used, the CGL is prepared on the carbon nanotube layer with regular arrangement by the thermal evaporation method, and therefore the electrical crosstalk (lateral conductivity) of the CGL is reduced, and the performance of the laminated OLED device is improved.
Owner:ANHUI SEMICON INTEGRATED DISPLAY TECH CO LTD

Double-layer sealing door device of ultrahigh vacuum evaporation machine

This invention proposes a double-layer sealing door device for an ultra-high vacuum evaporation coating machine, including a processing chamber. A sealing door is provided on the outer side of the processing chamber, and the two are connected by a hinge assembly. A sealing area is provided on the outer end face of the processing chamber, and at least one evacuation hole is opened in this area. An inner sealing ring and an outer sealing ring are arranged sequentially on the inner side of the sealing door. When closed, the inner and outer sealing rings simultaneously press against the sealing area to form an annular vacuum chamber. The evacuation hole is located inside the vacuum chamber and is used to independently evacuate the chamber to form a secondary seal. Through the coordinated design of the inner and outer double sealing rings and the vacuum chamber, a transition vacuum zone is constructed between the sealing door and the processing chamber, making the pressure difference between the inside and outside of the door approach zero, significantly reducing the stress deformation of the sealing rings and extending their service life. At the same time, the double vacuum barrier greatly reduces the leakage rate of the main chamber and improves the sealing reliability.
Owner:SUZHOU YOULUN VACUUM EQUIP TECH CO LTD

High-performance two-dimensional perovskite photodetector and preparation method thereof

The application belongs to the technical field of photoelectric detectors, and discloses a high-performance two-dimensional perovskite photoelectric detector and a preparation method thereof. First, a SiO2 glass substrate is cleaned, and a precursor solution is dropped on the surface of the glass substrate. Chloroform antisolvent solution doped with ZnO quantum dots is dropped on the precursor solution. Then, ZnO quantum dots / (PEA)2PbI4 nanosheet thin film is formed by spin coating, and the thin film is annealed. The above steps are repeated multiple times to obtain a uniform thin film. The glass substrate with the uniform thin film is plated with gold by a vacuum evaporation method to obtain an electrode. The application improves the carrier migration rate by doping the concentration of ZnO quantum dots, improves the photocurrent size, obtains higher responsivity and detection rate, and shorter response time. The manufacturing process is simple and has strong repeatability. The application has high photocurrent size, high responsivity and high detection sensitivity. The application selects a suitable concentration of ZnO quantum dots. The application can be prepared in an air environment and has strong stability.
Owner:YANGTZE DELTA REGION INST OF UNIV OF ELECTRONICS SCI & TECH OF CHINE (HUZHOU)

Solar photovoltaic photo-thermal cold storage system and central air conditioner cold storage method

PendingCN121631435APhotovoltaicsSteam generation using solar heatWater circulationSewage
The invention relates to the technical field of central air conditioners, in particular to a solar photovoltaic photo-thermal cold storage system and a central air conditioner cold storage method. The cold storage system comprises a photovoltaic photo-thermal assembly; the hot water circulation pipeline is connected with a cooling water channel of the photovoltaic photo-thermal assembly, a cooling water inlet is used for being connected with a building sewage input end, and water in the hot water circulation pipeline can be cooled under the action of building sewage; a water inlet of the vacuum evaporator is connected with a cooling water outlet of the photo-thermal evaporator, an air inlet of the vacuum evaporator is connected with a photo-thermal steam outlet of the photo-thermal evaporator, and the vacuum evaporator can absorb heat of building sewage through vacuum low-temperature evaporation and convey condensate water and residual water; the fire water tank is connected with the condensate water outlet and the residual water outlet of the vacuum evaporator; the air conditioner cold water heat exchanger is installed in the fire water tank, PVT low-grade heat energy can be directly utilized, and a low-energy-consumption system integrating building cold storage and sewage reuse is achieved. The cold storage method is based on the cold storage system.
Owner:SICHUAN PROVINCIAL ARCHITECTURAL DESIGN & RES INST

Continuous vacuum evaporation device for anti-fingerprint film

The utility model discloses a continuous vacuum evaporation device for an anti-fingerprint film. The continuous vacuum evaporation device comprises a vacuum film coating machine body and a film coating main roller of a roll-to-roll vacuum film coating machine, wherein the film coating main roller is arranged in the middle of the vacuum film coating machine body; an evaporation boat is arranged at the bottom position of a coating main roller of the opposite-roll vacuum coating machine, a steel wool rope winding device is arranged on the side face position of a guide wheel, a steel wool rope unwinding device is arranged on the steel wool rope winding device on the right side, and a steel wool rope body is arranged in the middle positions of the steel wool rope winding device, the guide wheel and the evaporation boat. The bottom of the evaporation boat is connected with a power supply connecting power supply, the steel wool rope body also travels in a winding mode according to process requirements, and the fingerprint-proof liquid medicine on the steel wool rope body can be continuously evaporated to the bottom of a coating main roller of the opposite-winding vacuum coating machine under the condition that the evaporation boat is heated. After the device is improved, the roll-to-roll vacuum coating machine can continuously evaporate the anti-fingerprint film for a long time.
Owner:KUNSHAN PUYUAN VACUUM TECH ENG CO LTD

Method for recovering ammonium fluoride from semiconductor photovoltaic wastewater

PendingCN121872406ATreatment involving filtrationCounter-current extractionMagnesium saltPhosphate
The invention discloses a method for recovering ammonium fluoride from semiconductor photovoltaic wastewater. The method comprises the following steps: adjusting pH in a pretreatment stage, and adding sodium citrate to complex metal ions; a composite extraction agent composed of diisooctyl phosphate, trialkyl phosphine oxide and methyl trioctyl ammonium chloride is adopted for multi-stage counter-current extraction; sequentially carrying out washing and two-stage gradient ammonia water reverse extraction to improve the selectivity and inhibit silicon-boron co-dissolution; the strip liquor is subjected to calcium and magnesium salt impurity removal, reduced pressure evaporation, graded cooling crystallization and vacuum drying, an ammonium fluoride product with the purity larger than or equal to 94% and the water content smaller than or equal to 0.5% is finally obtained, the extracting agent can be recycled, mother liquor and washing liquor are recycled, and the process is closed, environmentally friendly, economical and suitable for industrial application.
Owner:HUIZHOU ZHENDING ENVIRONMENTAL PROTECTION TECH CO LTD

Waste treatment method in radiopharmaceutical production process

The invention discloses a waste treatment method in a radiopharmaceutical production process, which comprises the following steps: adding a DNA-silver nano composite material into wastewater, so that silver ions are combined with iodine-131 to generate stable silver iodide crystals, thereby fixing radionuclides in the wastewater; the risk of iodine-131 volatilization is reduced by adopting a vacuum evaporation process, and water is ensured to be separated from radioactive pollutants; condensate water is discharged after reaching the standard through detection, and concentrated waste is subjected to curing treatment; by mixing concentrated waste with cement and adding a silicate additive, the physical stability and chemical inertness of a solidified body are enhanced, and the possibility of leakage is reduced; and finally, safely storing the cured concentrated waste in a special storage container. According to the method, efficient and safe radioactive waste management is achieved through the synergistic effect of a series of steps, the safety of long-term storage is greatly improved, and the method has great significance in protecting human health and protecting the ecological environment from radioactive contamination.
Owner:HUAYI PHARM (GUANGDONG) CO LTD

Control device for managing vacuum evaporation water generators

A management device 100 manages a vacuum vaporization-type fresh water generation device 1 producing fresh water from seawater, and comprises: an operating condition acquisition unit 110 that acquires information relating to an operating condition of the vacuum vaporization-type fresh water generation device 1; and an abnormality detection unit 120 that detects an abnormality in the vacuum vaporization-type fresh water generation device 1 on the basis of the information acquired by the operating condition acquisition unit 110.
Owner:SASAKURA ENG CO LTD

Functional current collector with corrosion-resistant coating and preparation method thereof

The invention discloses a functional current collector with a corrosion-resistant coating and a preparation method of the functional current collector, and relates to the technical field of current collectors. The functional current collector with the corrosion-resistant coating comprises a macromolecular base film, a metal layer and a high-entropy alloy corrosion-resistant coating, the metal layer is arranged on at least one side of the surface of the base film; the high-entropy alloy corrosion-resistant coating is arranged on one side, far away from the polymer base film, of the surface of the metal layer; the high-entropy alloy corrosion-resistant coating is selected from at least four metal elements of Al, Ti, Cr, Ni, Cu, Mo, Si, Nb, Zr, W, Y, Li, V, Fe, Zn, Co, Mn, Mg and Hf; the high-entropy alloy corrosion-resistant coating is prepared by any one of a magnetron sputtering method and an ion implantation method; the metal layer is prepared by any one of vacuum evaporation, magnetron sputtering, atomic layer deposition and electrochemistry.
Owner:YANGZHOU NANOPORE INNOVATIVE MATERIALS TECH LTD

Methods and apparatus for controlling water balance during lithium chloride brine electrolysis

The invention relates to methods and apparatus for controlling water balance during lithium chloride brine electrolysis. A method is provided comprising supplying the anolyte product stream from electrolysis to a flash evaporator without mixing it with any other liquid stream between exiting the electrolyser and entering the flash evaporator, concentrating it by vacuum evaporation and recirculating the concentrated anolyte product to the electrolyser. A method is also provided comprising the use of forward osmosis prior to electrolysis in order to adjust the concentration of the initial feed brine such that it can be purified by ion exchange and then concentrated for electrolysis, in a manner that means that the entire feed brine can be prepared for electrolysis using forward osmosis, which requires very little energy input. Apparatus for performing the above processes is also provided.
Owner:LIFTHIUM ENERGY SA

A pleuromutilin extraction system

The utility model relates to the technical field of industrial production of pleuromutilin, and specifically discloses a pleuromutilin extraction system to solve the problems of low yield, insufficient purity and low efficiency of clarity treatment in the existing pleuromutilin extraction mode, which comprises a three-stage countercurrent leaching system, a double-effect evaporation system, a methanol evaporation kettle, a layered tank and a vacuum evaporation crystallization system connected in sequence from the head to the tail. The three-stage countercurrent leaching system comprises three countercurrent leaching tanks and dryers connected in series from the head to the tail, and the discharge end of the first countercurrent leaching tank and the discharge end of the second countercurrent leaching tank are both provided with a slag excavator, and the discharge end of the third countercurrent leaching tank is provided with a slag extruder. The extraction system is used for extracting and processing pleuromutilin, and the pleuromutilin has high yield, high degree of automation and high purity.
Owner:INNER MONGOLIA XINYUAN BIOCHEMICAL CO LTD

Vacuum evaporation apparatus

ActiveCN116791039BThermodynamicsMixing effect
The application discloses a vacuum evaporation equipment, which is characterized by the following technical scheme: a gasification tank is fixedly installed on the top of an evaporation box, a purification box is arranged between the gasification tank and the evaporation box, a second rotating rod is rotatably installed in the gasification tank, second stirring rods are arranged on the outer wall of the second rotating rod, the end of the second stirring rods is provided with a connecting rod with a stirring needle and a stirring column, a filter plate with a plurality of filter holes is elastically installed in the gasification tank and above the second rotating rod, a third rotating rod is rotatably installed on one side in the purification box, a plurality of third stirring rods are arranged on the outer wall of the third rotating rod, and the outer wall of the third stirring rods is oppositely provided with a stirring block and a stirring plate with a wavy structure. The vacuum evaporation equipment can uniformly mix evaporation materials for multiple times, and can filter the evaporation materials for multiple times, so that the mixing effect of the evaporation materials and the consistency of evaporation particles are effectively improved, and the evaporation quality of the device is improved.
Owner:SUZHOU YIKAIXUAN ELECTRONICS TECH CO LTD

Preparation method of high-purity aluminum wire for vacuum coating, high-purity aluminum wire and application thereof

The present application relates to the technical field of high-purity aluminum preparation, in particular to a preparation method of high-purity aluminum wire for vacuum coating, high-purity aluminum wire and application thereof, the number and size of the second phase are reduced by controlling the content of metal impurities in the high-purity aluminum wire, the hydrogen content in the aluminum liquid is ≤0.10 mL / 100g through degassing treatment, and the impurity content in the high-purity aluminum wire is less; the thickness of the oxide film on the surface of the aluminum wire and the grain size are controlled by controlling the roughing and finishing temperature, and intermediate annealing treatment is not performed to avoid the thickening of the oxide film on the surface of the aluminum wire; the strength and surface quality of the aluminum wire are improved through drawing and wire scraping treatment; the above-mentioned performance improvement reduces the splashing phenomenon of the aluminum wire in the evaporation process, the composite aluminum film obtained through vacuum evaporation has excellent performance, the square resistance in the TD direction is ≤29 mΩ / sq, the surface roughness Sa is ≤0.18 μm, the tensile strength is ≥215 MPa, and the pinhole rate is ≤0.02 ea / m 2 , the adhesion is measured by pasting the surface of the aluminum film with 3M adhesive tape, and there is no aluminum foil falling off.
Owner:CHINALCO MATERIALS APPL RES INST CO LTD

Efficient centrifugal film vacuum evaporation device

The utility model belongs to the technical field of film vacuum evaporation devices, and discloses an efficient centrifugal film vacuum evaporation device which comprises a shell, a heat exchange cavity is formed in the side surface of the shell, an air inlet is formed in the outer surface of the upper end of one side of the shell, and an overflow liquid recycling mechanism is arranged in the lower end of the shell. And by means of the mode that the materials which are not evaporated in time are recycled and reversely pumped into the functional rod, secondary treatment on the overflowing materials is omitted. According to the efficient centrifugal film vacuum evaporation device, an overflow liquid recycling mechanism is arranged in the lower end of the device, materials which are not evaporated in time and overflow and accumulate at the bottom can be efficiently recycled, reciprocating piston motion is achieved through the action of a spring between a functional cylinder and a piston rod, and under cooperation of a first one-way valve and a second one-way valve, the materials can be recycled. And the materials in the bearing ring are reversely pumped into the functional rod, so that the materials are recycled, and a complex, time-consuming and labor-consuming treatment process for the overflowing materials is omitted.
Owner:SHANGHAI DUOLI CONTROL ENG CO LTD

Preparation method of shading anti-counterfeiting alumite

The invention belongs to the technical field of alumite, and particularly discloses a shading anti-counterfeiting alumite preparation method which comprises the steps that a base film layer serves as a carrier, coating is conducted in sequence in a roller coating mode, drying is conducted, a release layer and a color layer are formed, and the color layer contains an anti-doodling auxiliary; preparing a laser pattern on the color layer through a mold pressing process; coating a shading layer solution on the mould-pressed color layer in a roller coating manner, incompletely spreading the shading layer solution based on the low surface energy characteristic of the surface of the color layer, and drying to form a shading layer which incompletely covers the color layer; performing vacuum evaporation on the shading layer to form a plating layer; and coating a thermosensitive adhesive layer on the plating layer to obtain the shading anti-counterfeiting alumite. According to the invention, a double anti-counterfeiting structure of the laser pattern and the random shading is constructed, and the problem that a traditional mould pressing pattern is easy to counterfeit due to a layout rule is solved.
Owner:HUBEI HUAGONG IMAGE TECH DEV CO LTD

A breakage-resistant crystal oscillator system for vacuum evaporation machines

This invention relates to the field of crystal oscillator systems for vacuum evaporation coating machines, specifically a breakage-resistant crystal oscillator system for such machines. The system includes a first rotating mechanism and a support ring assembly mounted on its lower outer side. A carrier to be coated is connected to the lower interior of the support ring assembly. A second rotating mechanism is housed within the cavity of the first rotating mechanism, and the rotating shaft of the second rotating mechanism is connected to an intermediate rotating shaft. A crystal oscillator assembly is connected to the bottom end of the intermediate rotating shaft. A water-cooling jacket for storing cooling water is provided inside the water-cooling shaft, and an adjustment assembly is installed inside the water-cooling jacket. This breakage-resistant crystal oscillator system for vacuum evaporation coating machines ensures uniform temperature of the cooling water within the water-cooling jacket, thereby improving the cooling effect and preventing the crystal oscillator from breaking due to the high-temperature environment generated during vacuum evaporation coating machine operation, thus avoiding impact on the manufacturing of electronic materials.
Owner:SUZHOU YOULUN VACUUM EQUIP TECH CO LTD

Preparation method of component gradient inorganic framework layer for ink-jet printing and battery

The invention relates to a preparation method of an ink-jet printed component gradient inorganic framework layer and a battery. The preparation method sequentially comprises the following steps: step 1, providing a conductive substrate provided with a functional layer; 2, the conductive substrate is placed in vacuum evaporation equipment, and a first inorganic source and a second inorganic source are provided for the vacuum evaporation equipment; and step 3, co-evaporating the first inorganic source and the second inorganic source so that the first inorganic source and the second inorganic source are deposited on the functional layer of the conductive substrate to form an inorganic skeleton layer. According to the gradient inorganic framework layer prepared by the invention, the longitudinal component change means that various reaction interfaces and permeation channels are provided at different depths, so that one framework layer can adapt to various organic salt solutions with different concentrations, different solvent compositions or different additives, and high-quality perovskite films can be obtained; and the problems of debugging workload in research and development and formula sensitivity in production are greatly reduced.
Owner:HUZHOU QUAIL FIRE PHOTOELECTRIC CO LTD

Evaporation method and application thereof

The invention provides an evaporation method and application thereof, and relates to the technical field of vacuum evaporation, the evaporation method comprises the following steps: preheating an evaporation boat, a tungsten mesh and a solid aluminum source arranged on the tungsten mesh; pre-melting treatment is conducted, the solid aluminum source is melted, and molten aluminum covering part of the surface of the tungsten net is formed; pre-evaporation treatment is conducted, the molten aluminum is evaporated, and an initial infiltration area is formed; in the primary wire feeding stage, aluminum wires are fed at the first wire feeding speed, molten aluminum obtained after the aluminum wires are molten is spread in the initial infiltration area till the tungsten mesh is completely infiltrated by the molten aluminum, and at least part of the tungsten mesh is consumed; in the secondary wire feeding stage, aluminum wires are fed at the second wire feeding speed, and the tungsten net is completely consumed; and an evaporation stage: evaporating an aluminum metal layer on the base film. According to the evaporation method provided by the invention, the spreading uniformity and evaporation stability of the molten aluminum are improved, and the technical problems of narrow liquid level, frequent splashing and non-uniform coating thickness caused by non-uniform heat distribution in the traditional process are solved.
Owner:JIANGSU ENPACK COMPOSITE CURRENT COLLECTORS CO LTD

A ceramic transfer roller device for vacuum evaporation with a circulating cooling liquid cooling system

This utility model relates to the field of ceramic transfer roller technology, and discloses a ceramic transfer roller device for vacuum evaporation with a circulating coolant cooling system. It includes a base, a mounting frame fixedly connected to the center of the base, a safety film screen roller rotatably connected to the center of the mounting frame, a ceramic transfer roller body disposed on the upper front side of the mounting frame, mounting blocks fixedly connected to the left and right sides of the upper part of the base, a heating oil roller rotatably connected to the opposite side of the mounting blocks, an L-shaped frame fixedly connected to the left rear side of the mounting frame, an installation roller rotatably connected inside the L-shaped frame, and a coating main drum fixedly connected to the outside of the installation roller. In this utility model, through the cooperation of structures such as the handle, connecting block, return spring, telescopic column, limit block, mounting groove, cylinder, support block, installation roller, and coating main drum, the ceramic transfer roller device facilitates the replacement of the substrate film, reducing downtime.
Owner:GUANGDONG SHUNDE CAPIST ELECTRONIC MATERIAL CO LTD

Heat dissipation electromagnetic shielding film for spaceflight and preparation method thereof

The invention discloses a heat dissipation electromagnetic shielding film for spaceflight and a preparation method thereof, the prepared film is of a multi-layer structure, and a transition layer, an electromagnetic absorption layer, an isolation layer, an electromagnetic reflection layer and a thermal radiation reflection layer are sequentially arranged on a first surface of a base material; an electromagnetic reflecting layer, a heat radiation reflecting layer, a heat radiation layer and an anti-static layer are sequentially arranged on the second surface of the conductive base material; through holes are distributed in the surface of the electromagnetic shielding film; metal coatings are attached to the inner walls of the through holes, and all layers of the thin film are communicated through the metal coatings. The anti-static layer is prepared by sequentially sputtering the electromagnetic reflecting layer on the second surface of the base material, depositing the thermal radiation reflecting layer through vacuum evaporation, then coating the thermal radiation layer and curing, and coating conductive liquid or in a magnetron sputtering mode. The second surface of the electromagnetic shielding film has low solar absorptivity and high hemispherical emissivity, the solar absorptivity is less than or equal to 0.40, the hemispherical emissivity is not less than 0.60, and the electromagnetic shielding film has a good heat dissipation function and adapts to harsh application scenes in the aerospace field.
Owner:BEIJING TIANYU AEROSPACE NEW MATERIAL TECH CO LTD

Method for improving photoyield of Cs3Cu2I5 scintillator through Cr < 3 + > / Mn < 2 + > co-doping

The invention discloses a method for improving the photoyield of a Cs3Cu2I5 scintillator through Cr < 3 + > / Mn < 2 + > co-doping. Compared with a traditional high-temperature melting method, a vacuum evaporation method, an anti-solvent method and other processes which depend on complex equipment, high temperature and high pressure or a large amount of toxic organic solvents, the method has the advantages that important innovation is achieved on the scintillator preparation process, and high efficiency, environment friendliness and excellent expandability are achieved; according to the method, a solution method cooling crystallization strategy taking a hydroiodic acid-hypophosphorous acid mixed solution as a medium is adopted, so that the process is fundamentally simplified, the reaction condition is mild, the dependence on harsh equipment and the preparation cost are remarkably reduced, meanwhile, the use of a toxic solvent is avoided, and the method has better environmental friendliness. According to the method, heating reaction is carried out at the temperature of 180-240 DEG C for only 0.5-2.0 hours, then natural cooling is carried out for 8-24 hours, a large number of evenly-crystallized Cs3Cu2I5: Cr < 3 + > and Mn < 2 + > small broken crystals can be obtained, the technological process is high in controllability and repeatability, large-scale preparation of large-area and high-quality scintillator materials is easy to achieve, and a reliable path is provided for industrial popularization.
Owner:JIAXING RES INST ZHEJIANG UNIV +1

Coating process for manufacturing optical lens

The invention relates to the general plating field of a vacuum evaporation method, a sputtering method, an ion implantation method or a chemical vapor deposition method, in particular to a coating process for manufacturing an optical lens. The coating process comprises the steps that a base material and a vacuum chamber are prepared, and the preparation content comprises the steps that before the base material is placed into the vacuum chamber, an ion cleaning source is adopted for carrying out pretreatment including cleaning and static electricity removing on the base material; the temperature and the vacuum degree of the vacuum chamber are adjusted to reach a first preset interval and a second preset interval respectively; putting the base material into a vacuum chamber, and carrying out deep cleaning and surface activation on the base material by adopting an ion activation source; high-refractive-index film layers and low-refractive-index film layers are sequentially deposited on the surface of the base material in a vacuum chamber through evaporation, and the multiple high-refractive-index film layers and the multiple low-refractive-index film layers are alternately deposited to form color layers; meanwhile, the compactness and adhesive force of the high-refractive-index film layer and the low-refractive-index film layer are improved by using an ion-assisted deposition source; and immersing into a detection reagent, taking out, and detecting the completeness of the coating film.
Owner:HUAKAI SPORTING GOODS (SUZHOU) CO LTD

Conductive tape, photovoltaic module and method for manufacturing conductive tape

PendingCN122121345ATinningSputtering
The embodiment of the present application discloses a conductive strip, a photovoltaic module and a preparation method of the conductive strip. The conductive strip comprises a substrate, the substrate has a first side and a second side arranged oppositely, the first side has a light reflection structure, a light reflection layer is arranged on the surface of the light reflection structure, and a welding layer is arranged on the second side. The light reflection layer is formed by electroplating or a non-liquid deposition process. The light reflection layer is formed by electroplating or a non-liquid deposition process (such as vacuum evaporation and magnetron sputtering), the plating layer material is deposited in the form of atoms, ions or gas, and the surface of the light reflection structure is uniformly covered. Compared with a traditional hot-dip tinning process, the accumulation and particles of liquid metal in the groove are reduced, and the original morphology of the light reflection structure is maintained to reduce the adverse effect on the reflectivity.
Owner:SUZHOU YOURBEST NEW TYPE MATERIALS

Freezing film concentration device

PendingCN121927322ARetain original nutrientssolve decompositionSolution crystallizationHeat exchange cooling cystallizationThin membraneRefrigerant
The invention discloses a frozen film concentration device and belongs to the technical field of vacuum concentration. The invention solves the problem that the product quality is easy to decline because the feed liquid needs to be continuously heated in the existing vacuum evaporation and concentration operation process. A refrigerant inlet is formed in the top of the rotor, a refrigerant outlet is formed in the bottom of the rotor, the top of the rotor is connected into the liquid collecting disc and rotates along the central axis of the liquid collecting disc, and a plurality of overflow holes are formed in a first area of the side wall of the liquid collecting disc. A scraping plate is fixedly connected to the side wall, far away from the first area, of the concentrator shell, and the other end of the scraping plate is tightly pressed on the side wall of the rotor. Refrigerant flows in the rotor, so that the surface of the rotor is kept in a low-temperature frozen state, a plurality of frozen film concentrators are connected in series to form a multi-stage continuous concentration process, the whole concentration process is performed in a low-temperature environment, original nutritional ingredients of feed liquid are reserved to the greatest extent, and the quality of concentrated products is greatly improved.
Owner:SHENYANG AGRI UNIV

A lens vacuum evaporation head structure with adjustable evaporation rate

The present application relates to the technical field of lens vacuum evaporation, and discloses a lens vacuum evaporation head structure capable of adjusting evaporation rate, which comprises an operating table, a regulating groove is formed in the lower part of the inner wall of the operating table and below a heating groove, a plurality of heating rings are installed at the edge of the inner wall of the heating groove at equal distances, a metal block is connected to the inner wall of the heating groove, a contact shaft is fixedly arranged at the bottom of the metal block, an adjusting shaft is fixedly arranged at one end of the connecting shaft, and a pushing shaft is fixedly arranged at one end of the adjusting shaft, the pushing shaft pushes the adjusting shaft in the regulating groove, the hemispherical end head at one end of the adjusting shaft is in contact with the contact shaft at the bottom of the metal block, the contact shaft at the hemispherical bottom is extruded and then rises and falls in the heating groove, different numbers of heating rings are blocked, different degrees of heat emission are blocked, the heating intensity of the coating raw material is controlled, the control of the evaporation rate is realized, and the efficiency of lens processing is improved.
Owner:江西华派光电科技有限公司

Evaporation boat and vacuum evaporation device

The utility model discloses an evaporating boat and vacuum evaporation device, include: boat body, its top surface is recessed to form evaporating groove, the groove bottom of evaporating groove has the adjacent distribution of coating area and non-coating area, and the drop point of material is located coating area, and is close to the junction of coating area and non-coating area, wet coating, coating in coating area, wherein, coating area has with first side of junction opposite, non-coating area has with second side of junction opposite, and second side compares first side and is closer to drop point distribution. The utility model adopts above -mentioned structure, can make the liquid material that drops to evaporating groove spread out fast, evenly, and can effectively avoid material splashing.
Owner:JIANGSU YINGLIAN COMPOSITE FLUID COLLECTION CO LTD

Top anti-sticking device of vacuum evaporator

The utility model provides a vacuum evaporator top anti-sticking device, the evaporator comprises a cavity, the cavity is enclosed by a top plate, a coaming and a bottom plate, the top of the cavity is provided with the anti-sticking device, the anti-sticking device comprises a side wall anti-sticking plate, a first anti-sticking plate and a second anti-sticking plate, the side wall anti-sticking plate surrounds the upper part of the cavity by a circle and is arranged on the inner side of the coaming, and the first anti-sticking plate and the second anti-sticking plate are arranged on the top of the cavity. A first anti-adhesion plate and a second anti-adhesion plate are arranged below the top plate, the outer edge of the first anti-adhesion plate is connected with the top of the side wall anti-adhesion plate, the second anti-adhesion plate is arranged above the first anti-adhesion plate and used for preventing reverse sedimentation of a film material in the evaporation process and facilitating maintenance, and heating devices are arranged on the first anti-adhesion plate and the side wall anti-adhesion plate and used for heating the film material in the evaporation process. A plurality of cushion columns are symmetrically arranged between the first anti-adhesion plate and the second anti-adhesion plate, so that a gap is formed between the first anti-adhesion plate and the second anti-adhesion plate, the thickness of the gap is equal to that of the cushion columns, and the gap is used for forming a heat preservation layer between the first anti-adhesion plate and the second anti-adhesion plate so that heat preservation can be conducted on the heating device, and meanwhile the influence of external water cooling is isolated.
Owner:SUZHOU YOULUN VACUUM EQUIP TECH CO LTD