2141results about "Solution crystallization" patented technology

The invention relates to the technical field of parameter adjustment, and discloses a low-temperature evaporative crystallization machine parameter adjustment method, device and equipment and a storage medium, and the method comprises the steps: collecting M groups of temperature sensor data and N groups of pressure sensor data of a low-temperature evaporative crystallization machine, calculating a first uncertainty representation of temperature parameter measurement and a second uncertainty representation of pressure parameter measurement; performing data fusion to obtain an optimal estimated value of a temperature state and an optimal estimated value of a pressure state; parallel prediction is carried out through the thermodynamic equilibrium model, the crystallization kinetic model and the system response model, and a crystallization process prediction result is obtained; according to the technical scheme of the invention, the interference of the feeding fluctuation, the environmental change and the like can be effectively handled, and the real-time updating of the control strategy and the accurate adjustment of the temperature and pressure parameters can be realized.

The invention provides a method for recovering a BHET monomer from a waste polyester textile alcoholysis solution, and is characterized in that the recovery method comprises the following steps: (1) filtering: mixing the waste polyester textile alcoholysis solution with water under a stirring condition, and filtering at 55-70 DEG C; and (2) cooling crystallization: under a stirring condition, carrying out primary cooling on the filtrate obtained by filtering in the step (1) from 55-70 DEG C to 45-55 DEG C, then adding a BHET seed crystal, then carrying out secondary cooling to 5-15 DEG C, and maintaining the temperature for 20-60 min to obtain the BHET monomer. The mixed solution cooling crystallization method is developed on the basis of complexity of components of the waste polyester textile fabric, the problems that in the conventional production process, a BHET crystal product is low in quality, prone to scaling, difficult to filter and dry and the like are solved, and the obtained BHET product is large in particle size, narrow in particle size distribution, high in purity, good in fluidity and high in stability.

The invention relates to the technical field of automatic control, in particular to a monitoring method and system for synthesizing ceramide based on alpha-hydroxy fatty acid, and the monitoring system for synthesizing ceramide based on alpha-hydroxy fatty acid comprises a raw material feeding module, a reaction control module, a quenching-crystallization joint control module and a data integration module; carrying out dynamic weighing monitoring on the raw materials based on the received synthesis instruction, and starting a reaction kettle according to weighing data; performing multi-dimensional data acquisition in real time according to the set reaction data, and performing dynamic feeding control according to the set reaction data; when the TLC detection substrate reaction is completed, the cooling process and the crystallization process are regulated and controlled in real time according to the reaction data until the end point judgment standard is met; according to a received synthesis completion instruction, product quality data is obtained, a monitoring data packet is generated, the synthesis instruction is marked and then stored, process control is accurately monitored and controlled, and the purity and crystal form of the product are ensured.

The invention provides a method and system for salt separation, evaporation and crystallization of printing and dyeing wastewater, and the method comprises the following steps: sequentially carrying out multi-stage synergistic pretreatment on textile printing and dyeing wastewater to remove suspended solids, degrade organic matters and reduce hardness; the pretreated wastewater is subjected to membrane salt separation treatment, and preliminary separation of salt is achieved through reverse osmosis pre-concentration and nanofiltration salt separation; and respectively carrying out evaporative crystallization treatment on the separated high-concentration salt solution to obtain high-purity sodium sulfate and sodium chloride products. According to the method, the salt recovery rate and the product purity are remarkably improved, the energy consumption and the operation cost are reduced, meanwhile, the problems that in traditional printing and dyeing wastewater treatment, salt is difficult to separate, and the crystallization purity is low are solved, and an innovative solution is provided for high-valued resource recovery of industrial wastewater.

The invention provides an evaporative crystallization device and process for fluorine-containing high-salinity wastewater, and relates to the technical field of high-salinity wastewater treatment.The evaporative crystallization device for the fluorine-containing high-salinity wastewater comprises a support and an evaporation tank, and a first material opening used for communicating a stacking ring cavity with a material storage cavity is formed in an inner cylinder; a second material opening for communicating the material storage cavity with the material discharge cavity is formed in the first baffle plate; the heating assembly is in contact with and heats the wastewater to evaporate and discharge a wastewater solvent, a wastewater solute is gradually separated out to form crystals and moves towards the material stacking ring cavity, the first material opening is controlled to be opened, the second material opening is controlled to be closed, the crystals in the material stacking ring cavity enter the material storage cavity through the first material opening, and then the first material opening is controlled to be closed and the second material opening is controlled to be opened; the crystals in the material storage cavity enter the material discharging cavity through the second material opening, the crystals in the material discharging cavity are discharged through the first auger, the separated crystals can be continuously discharged without shutdown, meanwhile, the negative pressure environment in the evaporation tank is prevented from being damaged, and the working efficiency is improved.

The utility model discloses an atomization rotational flow crystallization device for CO2 resource recovery, which relates to the technical field of recovery of CO2 in combustion flue gas and comprises a spray gas inlet device, a spherical cyclone and a condensation crystallization device. According to the utility model, the atomization rotational flow crystallization device is adopted to realize CO2 resource recovery of flue gas, the flue gas is firstly in full contact with atomization absorption liquid sprayed by the multi-point spraying array assembly to form a flue gas absorption liquid mixture, the flue gas absorption liquid mixture is in a rotational flow state after entering the spherical hydrocyclone, and gas-liquid phase separation is carried out, so that the CO2 resource recovery is realized. The liquid phase is condensed under the condensation action of the condensation crystallization device to obtain a solid-phase product sodium bicarbonate and a liquid-phase absorption liquid, and the liquid-phase absorption liquid is subjected to temperature control adjustment and atomization again to provide an absorption liquid for the multi-point spray array assembly; and the method can also be used for large-scale CO2 resource recovery scenes such as thermal power plants and the like, the process and equipment are stable and reliable, the operation is flexible, and the CO2 absorption conversion rate is high.

The invention relates to the technical field of fluorination processes, in particular to a purification method of a high-purity fluorocarbonate-based solvent, which comprises the following steps: S1, introducing fluorocarbonate-based solvent crude gas into a purification cavity, and liquefying the crude gas through a liquefaction separation module; s2, separating the liquid obtained in the step S1, conveying the separated liquid into a crystallizing pond, cooling the liquid in the crystallizing pond to enter a crystallization critical state, rotating the rotating crystal plate group in the crystallizing pond, crystallizing the liquid on the surface of the rotating crystal plate group, and continuously collecting crystals above the crystallizing pond through a collecting assembly; and S3, washing and filtering the crystals collected in S2 to obtain the high-purity fluorocarbonic ester-based solvent. According to the purification method of the high-purity fluorocarbonate-based solvent provided by the invention, crude gas is liquefied by adopting the liquefaction module, and then the liquefied liquid is continuously crystallized and collected by adopting the rotary crystallization module, so that the high-purity fluorocarbonate-based solvent can be efficiently and simply prepared, and the purification method has good industrial value.

The invention relates to the technical field of nitrate production, in particular to a potassium nitrate purification device which comprises a dissolving tank, a filtering device, a crystallization kettle, a centrifugal machine and a drying machine with a steam jacket which are sequentially connected in series through pipelines. The dissolving tank first jacket is connected with a heat source through a circulating pipeline; a liquid outlet of the centrifugal machine is sequentially connected with the cyclone separator, the ceramic membrane filter, the cationic resin column, the first temporary storage tank and the heat source, and the first heat exchanger and the second heat exchanger are sequentially installed between the first temporary storage tank and a heating medium inlet of the heat source. A steam outlet pipeline of the steam jacket is connected with a heat medium inlet of the first heat exchanger, the first heat exchanger is connected with the second temporary storage tank through a pipeline, and the second temporary storage tank is connected with the heat source through a pipeline. A pipeline of the second vacuum unit is connected with a thermal medium inlet of a second heat exchanger, and the second heat exchanger is connected with a second temporary storage tank. According to the method, the potassium nitrate purification efficiency, the product purity, the resource utilization rate and the energy economy are synergistically improved.

The invention provides a cooling rate optimization control method and system for continuous cooling crystallization, and the method comprises the steps: collecting crystal slurry concentration data and temperature data of each stage of crystallization tank in real time; the crystal slurry concentration data, the temperature data and the feeding flow data are input into a deep learning model, and a prediction result is obtained; based on the prediction result and crystal mush concentration data, dynamically adjusting the cooling rate of each stage of crystallizing tank and the addition amount of a co-crystallizing solvent; and feeding back an outlet crystal mush concentration signal of the last-stage crystallizing tank to the solid-liquid separation unit, and adjusting the running rotating speed of the solid-liquid separation unit in a linkage manner. According to the cooling rate optimization control method and system for continuous cooling crystallization, prospective correction of the cooling rate is carried out by using the predicted supersaturation degree, and adjustment of the additive amount of the auxiliary crystallization solvent is carried out by using the predicted crystal particle size distribution; and finally, an outlet concentration signal of the last-stage crystallizing tank is fed back to the solid-liquid separation unit in real time to adjust the separation rotating speed in a linkage manner, so that the crystal particle size deviation is reduced, and the triazole crystallization recovery rate is improved.

The invention relates to the technical field of preparation of high-purity boron oxide, and discloses a purification method of high-purity boron oxide and a device thereof, and the purification method comprises the following steps: step 1, mixing crude boron oxide with a liquid metal alloy, and dissolving metal impurities through gradient temperature control; 2, applying ultrasonic treatment to the mixed system, introducing a vortex field, and stripping impurities on the surface of the boron oxide; 3, a liquid metal phase and a boron oxide solid phase are separated through cooperation of a magnetic field and a pulse high-voltage electrostatic field; 4, non-metal ion impurities are removed through a gradient porous ceramic adsorption bed; and step 5, melting boron oxide in vacuum and carrying out gradient cooling crystallization. By adopting the technical scheme of a Ga-I n-Bi-Er quaternary liquid alloy system, the technical effect of selective targeted removal of metal impurities is achieved, and compared with a liquid metal system depending on single phase solubility difference in the prior art, the defect that efficient chelating and dynamic settling separation of the impurities cannot be achieved at the same time is overcome.

The embodiment of the invention provides an evaporation system control method and an evaporation system, and relates to the technical field of control, the method is applied to a control system in an MVR evaporation system.The method comprises the steps that in response to a starting instruction, a feeding system is controlled to pump to-be-treated liquid into an evaporation crystallization system, and the real-time boiling point rise of the evaporation crystallization system is monitored; and determining to adopt an optimal recovery rate control mode or a boiling point rise control mode as a target control mode based on the real-time boiling point rise, and controlling the feeding system, the evaporative crystallization system and the water production system to treat the to-be-treated liquid according to a preset strategy corresponding to the target control mode, the frequency of the distilled water and the flow of the to-be-treated liquid pumped by the feeding system meet the corresponding recovery rate, so that the control intelligence and reliability of the MVR evaporation system are improved.

The invention discloses a crystallization reaction kettle for medicine preparation, and relates to the technical field of medicine preparation, and the crystallization reaction kettle is technically characterized by comprising a reaction kettle body and a stirring mechanism, the stirring mechanism comprises a rotation driving assembly arranged at one end of the reaction kettle body, and an output shaft of the rotation driving assembly extends into the kettle and is connected with a stirring center pipe; the other end of the stirring central pipe communicates with an inert gas supply assembly; the side wall of the stirring central pipe is communicated with a stirring branch pipe; a scraper group is arranged at the end part of the movable pipe and comprises a plurality of scraper blades; an elastic sealing assembly is arranged and comprises a V-shaped sealing plate, and the two ends of the V-shaped sealing plate are connected with the end face of the movable pipe through elastic connecting pieces; during gas supply, inert gas passes through all parts and exhaust gaps, air pressure enables the movable pipe to abut against the kettle wall, the sealing plate is jacked up to form a flow guide gas channel, and the gas is guided to be exhausted and scour the scraper blade; according to the method, crystals can be efficiently scraped, secondary deposition can be avoided, and the problem that the fitting degree is reduced due to abrasion can be solved.

The invention relates to the technical field of fluorination equipment, in particular to high-purity fluorocarbonate-based solvent purification equipment, which comprises a purification main body internally provided with a purification cavity; the liquefaction separation module is arranged at the top of the purification cavity and is used for exchanging heat with the crude gas entering the purification cavity, so that the crude gas is liquefied and then subjected to gas-liquid separation; the rotary crystallization module comprises a crystallization pond, a rotary crystal plate group and a collection assembly, the crystallization pond is arranged below the purification cavity and used for receiving the liquefied and separated liquid phase, the rotary crystal plate group partially extends into the crystallization pond, and the rotary crystal plate group continuously rotates, so that liquid in the crystallization pond is crystallized on the surface of the rotary crystal plate group; and then the crystals are collected by the collecting assembly after rotating to the upper part of the crystallizing pond. According to the purification equipment for the high-purity fluorocarbonic ester-based solvent, the high-purity fluorocarbonic ester-based solvent can be continuously obtained in a manner of liquefying and then continuously crystallizing and collecting, so that the purification equipment has a good industrial value.

The utility model discloses piezoelectric polymer crystallization equipment which comprises an equipment body and a high-frequency power supply, an upper polar plate is arranged above the equipment body; a lower polar plate is arranged below the equipment body; one end of the high-frequency power supply is electrically connected to the upper polar plate, and the other end of the high-frequency power supply is electrically connected to the lower polar plate; a polymer solution is arranged in the equipment body; the high-frequency heating PVDF piezoelectric polymer solvent crystallization equipment has the advantages of uniform temperature, high heating speed, convenience in reaction control, heating selectivity and the like, dipoles in the solvent are oriented and polarized under the action of a high-frequency alternating electric field to form a temperature gradient (high inside and low outside), so that the solvent is promoted to be volatilized and dried from inside to outside, and meanwhile, vacuum high-frequency heating can be matched, so that the crystallization efficiency is improved. The boiling point of the solvent can be reduced within a certain vacuum degree, and meanwhile, in a negative pressure environment, the pressure in the solution is greater than the surface, so that the diffusion speed of the solvent from inside to outside is accelerated.

The invention belongs to the technical field of impurity separation, and particularly discloses a method for separating and purifying impurities in a process for preparing glyoxylic acid through oxalic acid electrolysis, a crystallization kettle is included, an isolation device is arranged in the crystallization kettle, and the isolation device comprises a conical top cover, a conveying pipe, an annular filter screen, a directional conveying assembly and a sealing assembly; the conical top cover is arranged at the axis of the crystallization kettle, an opening of the conical top cover faces downwards, and a plurality of fixing rods are fixedly connected between the top of the conical top cover and the inner wall of the side face of the crystallization kettle. According to the method, glyoxylic acid product solutions with different concentration specifications and the high-purity glyoxylic acid crystal can be obtained after the electrolyte is sequentially subjected to pre-evaporation, electrodialysis, secondary evaporation, cooling crystallization, solid-liquid separation, washing and drying and other procedures, so that the prepared high-purity glyoxylic acid crystal can be popularized and applied in the field of high-end medicine.

The invention provides an ultrasonic-assisted gamma-aminobutyric acid crystallization particle size regulation and control method, which comprises the following steps: removing impurities and decolorizing gamma-aminobutyric acid-containing feed liquid, heating, stirring and concentrating to a nearly saturated state, then carrying out ultrasonic-assisted crystallization, cooling, aging and suction filtration to obtain coarse crystals, and finally washing and drying to obtain target crystals. According to the method, a synergistic process of raw material liquid pretreatment, evaporation concentration-ultrasonic-cooling coupling crystallization, aging and post-treatment is adopted, an ultrasonic cavitation effect is utilized to reduce a nucleation barrier, and a supersaturation degree precise control and gradient cooling strategy is combined, so that grain size refinement, obvious narrowing of distribution and effective inhibition of agglomeration of crystals are realized; the median particle size of the crystal can be controlled to be smaller than or equal to 200 microns, the particle size distribution span is smaller than or equal to 1.5, the agglomeration phenomenon is remarkably inhibited, the crystal form is kept stable, the crystal habit is complete and smooth, the crystal product quality and the process efficiency are remarkably improved, and the method has important industrial application value.

The present invention relates to a high-salt wastewater resource utilization technology, particularly to the resource utilization of potassium nitrate mother liquor, and specifically to a method for recycling potassium resources in the potassium nitrate mother liquor. The method comprises brine adjustment, first-stage cooling, second-stage cooling, solid-liquid separation, decomposition and washing, and evaporation and concentration. A decomposition liquid produced by the decomposition and washing is mixed with a concentrated liquid produced by evaporation and concentration to adjust the MgCl2 content in the system. The brine-adjusted system is cooled in two stages, followed by solid-liquid separation to obtain a crystalline solid and a crystalline mother liquor. The crystalline solid is added to the potassium nitrate mother liquor and stirred thoroughly, followed by solid-liquid separation to obtain potassium chloride solid and a decomposition liquid. The potassium chloride solid is reused as a production raw material. The crystalline mother liquor is evaporated and concentrated, and a portion of the concentrated liquid and the decomposition liquid are recycled by mixing brine. The remaining concentrated liquid is cooled to room temperature to obtain MgCl2·6H2O solid. The present invention recycles potassium chloride in the by-product mother liquor without adding additional steam and water.

The invention relates to equipment for preparing clobetasol propionate liniment and a preparation method of the clobetasol propionate liniment. The equipment comprises a material mixing mechanism, a barrel, a stirring shaft rotationally arranged on the barrel, stirring blades for stirring substances, a partition plate for separating the interior of the barrel, a crystallization rod for cooling materials and a drying mechanism for drying the substances. Wherein the stirring blades are fixedly arranged around the stirring shaft, and the stirring blades at the bottom are arranged around the stirring shaft in a swinging manner; the partition plate is movably arranged in the barrel around the stirring shaft; the crystallization rod is movably arranged at the bottom of the barrel; the drying mechanism communicates with the bottom of the barrel; the drying mechanism is communicated with the mixing mechanism; the partition plate is arranged between the fixed first ring frame and the rotary second ring frame; the partition plate is connected with the first ring frame and the second ring frame. The second ring frame rotates to drive the partition plate to open or separate the cylinder. The preparation method solves the problem that the preparation efficiency of clobetasol propionate is affected due to more preparation equipment caused by complex process steps in the clobetasol propionate liniment preparation process in the existing scheme.

The invention discloses a preparation technology of high-purity potassium chloride, and relates to the technical field of potassium chloride preparation, the preparation technology comprises the steps of raw material treatment, impurity removal, dissolution and filtration, a crystallization reaction kettle stage and drying and packaging, a driving motor is arranged at the top end of a crystallization kettle main body, and a reaction cavity is formed in the crystallization kettle main body; the inner wall of the collecting box is scraped through the edge of a fixed scraper, crystals which are not cleaned up on the surface of the collecting box are cleaned again through a Y-shaped scraper, and the situation that the crystals on the surface of the collecting box are omitted and left on the surface of the collecting box is avoided; the crystals on the surface of the collecting box are scraped, so that high-purity potassium chloride can be discharged, the end of the scraping knife is always in contact with the side wall of the collecting box, the potassium chloride crystals on the side wall of the collecting box are cleaned more thoroughly, and the collecting box and the stirring fork rotate in opposite directions, so that the potassium chloride crystals on the surface of the collecting box can be quickly cleaned.

The invention belongs to the technical field of energy storage batteries, and particularly relates to a desalting, dehumidifying and cooling integrated thermal management device and method for a marine environment energy storage battery. The device is composed of an energy storage battery module, an air inlet dehumidification and desalination module, an air return reprocessing module, a salt crystallization and separation module, a cold source heat exchanger and a heat source heat exchanger. Wherein the inlet air dehumidification and desalination module cools inlet air by utilizing a first solvent and inlet air cross flow heat exchange mode, meanwhile, the first solvent dissolves salt mist ions in inlet sea wind, and the purposes of reducing the dew point temperature and dehumidifying the inlet sea wind are further achieved; in order to ensure water-salt concentration balance of the first solution, a salt crystallization precipitation module and a return air retreatment module are adopted to jointly adjust the concentration of the first solution. A solution is provided for safe and reliable operation of the energy storage battery system under the ocean high-temperature, high-humidity and high-salt links.

The invention belongs to the technical field of chemical fertilizer production and livestock feed, and particularly relates to a combined preparation method of water-soluble potassium sulfate and feed-grade potash magnesium sulphate fertilizer. According to the method, the picromerite concentrate wet material is taken as an initial raw material, the picromerite concentrate wet material with relatively low potassium and magnesium content is purified into high-grade potassium sulfate and the potash magnesium sulphate fertilizer by utilizing hot melt mother liquor at different mother liquor points through multi-stage hot melt and multi-stage vacuum evaporative crystallization, so that efficient distribution and conversion of potassium and magnesium elements in the raw material are realized, resource waste is avoided, and the production cost is reduced. The comprehensive utilization rate of raw materials is greatly improved. Two high-added-value products, namely the water-soluble potassium sulfate and the feed-grade potassium-magnesium fertilizer, are prepared at the same time, and the blank of combined preparation of raw materials required by agriculture and animal husbandry is filled.

The invention relates to the technical field of sodium chloride crystal preparation systems, in particular to a sodium chloride crystal preparation system which comprises a crystal separation tank, an annular isolation cylinder 2, a first heat exchanger, a center cylinder and an annular isolation cylinder. The annular isolation barrel is provided with an upper guide section and a lower acceleration section which are sequentially connected, the upper end of the upper guide section is fixedly connected to the inner circumferential wall of the crystallization separation tank, the upper guide section is gradually and downwards inclined from outside to inside of the crystallization separation tank, and the lower acceleration section is located at the lower end of the upper guide section. Through circulating conveying of the first conveying pump and cooperation of the first conveying pump, the heating mechanism and the fine grain eliminating mechanism, circulating treatment of brine in the crystallization separation tank is achieved, the functions of particle size grading and particle size growth are achieved, the salt crystallization process is optimized, the proportion of the salt product with the size smaller than 450 micrometers is reduced to be within 18% from 45%, and the crystal breaking force is enhanced and is increased to 3.30-6.77 N from 1.39-6.61 N.

The utility model discloses a liquid-phase synthesis system of lithium sulfide. Comprising a first lithium sulfate dissolving device, a first barium sulfide dissolving device, a chemical combination reaction device, a first separation device and a second separation device, the liquid phase after-treatment unit is used for concentrating, purifying and drying the liquid phase to obtain lithium sulfide, and the solid phase after-treatment unit is used for washing and drying the solid phase to obtain barium sulfate; the first lithium sulfate dissolving device and the first barium sulfide dissolving device are both connected with a raw material inlet of the combination reaction device; and a reaction product outlet of the combination reaction device is connected with the first separation device. The liquid-phase synthesis system of the lithium sulfide has the advantages that products are easy to separate, the purity of the lithium sulfide products is high, the liquid-phase synthesis system of the lithium sulfide is very suitable for industrial-scale production, and the produced high-purity anhydrous lithium sulfide is very suitable for solid-state battery anode materials and has huge potential economic benefits.

The invention belongs to the technical field of magnesium desulfurization wastewater treatment, and particularly relates to a magnesium desulfurization wastewater evaporation concentration material transfer anti-crystallization blockage system which comprises an evaporation separator and crystallizers, a circulation pipeline is arranged between an inlet and an outlet of a material transfer pump, and a material transfer pipeline is connected between a material transfer regulating valve and the crystallizers. The circulating pipeline and the branch pipelines are respectively communicated with the material transferring pipeline through branch pipelines, and the circulating pipeline and the branch pipelines are detachable metal hoses; a steam inner pipe is arranged in the material transferring pipeline, a heat preservation layer is arranged outside the material transferring pipeline, and opening degrees of the material transferring adjusting valve and the steam adjusting valve are in linkage control. Compared with the prior art, the device has the beneficial effects that effective anti-blocking prevention and emergency treatment are carried out on materials which are long in material transfer pipeline, rapid in concentration and temperature change and easy to crystallize in multi-point material transfer, cooperative control over the temperature of the separator feed liquid and the temperature of the material transfer pipe feed liquid is achieved, and concentration and temperature monitoring is carried out on the output feed liquid; materials always flow in the material transfer pipeline, and continuous production operation is guaranteed.

The invention relates to the technical field of separation and purification devices, in particular to a separation and purification device for 8-hydroxyquinoline crystallization. The device comprises a crystallization kettle used for cooling an 8-hydroxyquinoline solution, a stirring assembly is arranged in the crystallization kettle, the stirring assembly is provided with a plurality of cleaning assemblies in the radial direction of the crystallization kettle, each cleaning assembly comprises a scraping part and a pneumatic part, the scraping parts are slidably connected to the side, close to the inner wall of the crystallization kettle, of the stirring assembly, and the pneumatic parts are arranged on the scraping parts. The pneumatic part is used for pushing the scraping part to be close to the inner wall of the crystallization kettle; the increased air pressure in the pressure-bearing cavity pushes the pressure-bearing plate to slide towards one side close to the contraction groove, the telescopic arm is pushed out of the contraction groove through the sliding rod, and due to the fact that large air pressure is accumulated in the pressure-bearing cavity before the telescopic arm stretches out of the contraction groove, the conical part is inserted into the crystal above the liquid level at the moment that the top of the contraction groove is completely out of shielding of the installation groove. The telescopic arm instantly releases large force, and it can be ensured that the conical part is inserted into crystals tightly combined with the inner wall of the crystallization kettle.

The invention relates to the technical field of purification, in particular to Chinese cabbage moss allergy-free factor purification equipment which comprises an outer box, one side of the outer box is communicated with a feeding pipe, a self-cleaning filtering assembly capable of automatically scraping impurities attached to different side faces is arranged in the outer box, and the self-cleaning filtering assembly comprises a filtering cylinder rotationally connected with the side wall of the outer box; one side of the filter cartridge is communicated with a transverse pipe, the transverse pipe extends to the outside of the outer box, the feeding pipe penetrates through the transverse pipe, a scraping assembly is arranged in the filter cartridge, the scraping assembly is dragged to rise when the filter cartridge rotates and then slides down to conduct scraping, a driving assembly used for driving the transverse pipe and the filter cartridge to rotate is arranged on the outer box, and the scraping assembly comprises an arc-shaped plate in sliding connection with the inner wall of the filter cartridge; and a plurality of sliding plates are fixedly connected between the two arc-shaped plates. The technical problems that particles in Chinese cabbage moss juice of existing purification equipment are prone to blocking a filter screen, the amount of blocked Chinese cabbage moss particles is large, the cleaning difficulty is increased, and the process of cleaning the filter screen is time-consuming and labor-consuming are solved.

The present invention discloses a sodium bicarbonate continuous crystallization system and process thereof, comprising a continuous crystallization tank, wherein a cooling mechanism for the flow of coolant is provided in the continuous crystallization tank, the cooling mechanism comprising a cooling mesh pipe, the cooling mesh pipe being annular, a first connecting pipe being provided at the inner ring of one side of the cooling mesh pipe, and a second connecting pipe being provided at the outer ring of the other side of the cooling mesh pipe, adjacent cooling mesh pipes being connected via the corresponding first connecting pipe and the second connecting pipe, respectively, a feed trough being provided at the bottom of the continuous crystallization tank, and a conveying mechanism for conveying the crystallized material outward being provided in the feed trough. The cooling mechanism is distributed more evenly in the continuous crystallization tank, the coolant is distributed more evenly in the continuous crystallization tank, the coolant can more fully cool down and crystallize the material in the continuous crystallization tank, and the crystallization efficiency is improved; the present invention overcomes the shortcomings of the prior art, has a reasonable design, a compact structure, and has high social use value and application prospects.

The invention relates to a liquid level control device of a vacuum crystallizer. Relates to the technical field of vacuum crystallization. The device comprises a flash tank arranged below a crystallization pot, the flash tank is provided with an overflow port, and the bottom end of a discharge pipe extends into the flash tank and is lower than the overflow port, so that feed liquid and liquid level in the flash tank automatically flow out of the overflow port when reaching the height of the overflow port. The overflow port is formed in the overflow groove, the bottom end of the discharge pipe extends to the position below the overflow port in the overflow groove, when the liquid level of feed liquid in the overflow groove reaches the height where the overflow port is located, the feed liquid automatically flows out of the overflow port, liquid level control over the feed liquid in the overflow groove is achieved, and therefore the liquid level of the feed liquid in the overflow groove is controlled. The liquid level control device is simple in structure, reliability of liquid level control in the vacuum crystallizer can be improved, and then the effect of liquid level control in the vacuum crystallizer is guaranteed.

The utility model discloses a pyrolysis material balanced self-circulation conveying structure, which relates to the technical field of waste liquid treatment, and comprises a bottom plate, the top of the bottom plate is fixedly connected with two limiting plates, the interiors of the two limiting plates are fixedly connected with heating jackets, the top of the bottom plate is fixedly connected with a fixed plate positioned on one side of one limiting plate, and the top of the bottom plate is fixedly connected with the heating jackets. And a supporting plate is fixedly connected to the position, located on one side of one limiting plate, of the top of the bottom plate, second sealing supporting assemblies are installed on one side of the fixing plate and one side of the supporting plate correspondingly, and a rotary shell is installed on the outer sides of the two second sealing supporting assemblies. By arranging the rotary shell, the heating sleeve and the conveying shell, compared with the prior art, the structure has the advantages that the structure is simple, the occupied area is small, more equipment is not needed, and the treatment cost is reduced.

The utility model provides a brine evaporative crystallization device for industrial salt production, which comprises a box body, foot stools which are uniformly distributed are fixedly connected to the bottom wall of the box body, a ventilation bin is fixedly connected to the top wall of the box body, and the brine evaporative crystallization device further comprises a bearing assembly which is rotatably connected to the inner wall of the box body and is used for bearing brine to be evaporated, the bearing assembly comprises rotating frames rotationally connected to the inner wall of the box body and symmetrically distributed about the central axis of the box body, an evaporation disc rotationally connected to the inner wall of the box body through the rotating frames, and an adapter fixedly connected to the bottom wall of the evaporation disc; the supporting assembly is rotationally connected to the inner wall of the box body; the heating assembly is fixedly connected to the bottom wall of the evaporation disc; the ventilation assembly is arranged on the inner wall of the ventilation bin; the collecting assembly is arranged on the inner wall of the box body. The brine evaporation device can control the air velocity on the surface of brine in the brine evaporation process, accelerates the evaporation and crystallization rate, can automatically collect crystals evaporated from the brine, reduces the labor intensity of workers, and improves the collection efficiency of the crystals.