The application belongs to the technical field of
thermoelectric materials, and provides a preparation method of a beta-SrZrS3
thermoelectric conversion bulk material, which comprises the following steps: subjecting SrZrO3
powder to a sulfuration reaction to obtain beta-SrZrS3
powder; and subjecting the beta-SrZrS3
powder to rapid hot-press
sintering to obtain the beta-SrZrS3
thermoelectric conversion bulk material. The preparation method has the advantages of low cost, simplicity and rapidness, can realize batch synthesis of SrZrS3 bulk materials, shorten the
synthesis period, and obtain the beta-SrZrS3
thermoelectric conversion bulk material with pure phase, uniform composition distribution and
high density. The
raw material used is SrZrO3 powder which is inexpensive, non-toxic and does not require
inert storage environment. The
vacuum tube furnace and the rapid hot-press furnace are used, the sulfuration reaction and the hot-press
sintering are used for preparation, and since the
raw material, the preparation process and the target product meet the requirements of environmental friendliness, the preparation method can be directly extended to the development of the application of
perovskite sulfide thermoelectric conversion, and provides a new way for the development of a new thermoelectric
system.