The invention belongs to the technical field of TG-DSC testing of
metal powder materials, and particularly relates to an anti-oxidation high-precision TG-DSC testing method of high-temperature
alloy powder, which comprises the following steps: placing the high-temperature
alloy powder in a furnace body of a TG-DSC instrument, carrying out high-purity
argon replacement on the
atmosphere in the furnace body by taking high-purity
argon as furnace body purging gas, and carrying out high-purity
argon replacement on the
atmosphere in the furnace body; the initial
oxygen content in the furnace body is reduced to 0.1 ppm or below; continuously introducing
hydrogen-argon
mixed gas as flowing gas into the furnace body, controlling the temperature of the furnace body to be increased to a target temperature, and ending the test to obtain a TG curve and a DSC curve of the to-be-tested high-temperature
alloy powder; according to the invention, through physical cleaning of
oxygen in the furnace body by circulating vacuumizing before testing and
chemical cleaning of
oxygen permeating into the furnace body by
hydrogen-argon
mixed gas in the whole process in the testing process, a dual anti-oxidation barrier is constructed, so that oxidation weight increment and oxidation heat release interference of a powder sample are eliminated fundamentally; therefore, the real
mass change and the
heat flow signal change of the alloy powder sample in the temperature
programming process can be accurately measured.