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194 results about "Calorimetry" patented technology

Calorimietry is the science or act of measuring changes in state variables of a body for the purpose of deriving the heat transfer associated with changes of its state due, for example, to chemical reactions, physical changes, or phase transitions under specified constraints. Calorimetry is performed with a calorimeter. The word calorimetry is derived from the Latin word calor, meaning heat and the Greek word μέτρον (metron), meaning measure. Scottish physician and scientist Joseph Black, who was the first to recognize the distinction between heat and temperature, is said to be the founder of the science of calorimetry.

Thermal power measurement device

A thermal power measurement device is characterized in that the device comprises a calorimetry cylinder, a constant-temperature and heat-insulation system, a temperature equalization system, a calibration system, a signal processing and controlling system and a box body, wherein the calorimetry cylinder is a three-layer embedded composite structure; the inner-most layer is a sample chamber, the middle layer is semiconductor thermoelectric modules that are connected in series and the external wall is a constant-temperature layer; the sample chamber is internally provided with a thermocouple and a thermal resistor; the semiconductor thermoelectric modules are fixedly arranged between the sample chamber and the external wall by a mechanical method; the constant-temperature and heat-insulation system comprises a constant-temperature system and a heat insulation system; the constant-temperature system comprises a circular constant-temperature bath and a red copper fluid pipe; the red copper fluid pipe is closely attached to the external wall of the calorimetry cylinder; the inlet of the red copper fluid pipe is connected with the circular constant-temperature bath by a constant-temperature trough; the constant-temperature trough is internally provided with a remote temperature probe that is connected with the circular constant-temperature bath; the temperature equalization system comprises a fan that is arranged in the sample chamber; the calibration system comprises the thermal resistor; and the signal processing and controlling system comprises a computer and a data collecting card and is used for collecting signals in real time and controlling the fan power, calibration power and water bath temperature.
Owner:INST OF CHEM CHINESE ACAD OF SCI

M-w grade microwave power instrumentation system based on calorimetric method

The utility model belongs to a microwave power measurement system, specifically discloses a megawatt grade impulse microwave power measurement system based on calorimetric method, wherein an outlet temperature pickup is arranged on the stream outlet of a water pipe and an electric heater is arranged in the water pipe; the electric heater is connected with a rated power electricity supply; a microwave detecting device is arranged on the inlet of a microwave power absorbing device; the water runs through the inwall water pipe of the power absorbing device and an inlet temperature pickup is arranged on the stream inlet of the water pipe; an NTC thermal resistance R3 of the inlet temperature pickup is connected with a equilibrium resistance R1, while an NTC thermal resistance R4 of the outlet temperature pickup is connected with a equilibrium resistance R2; the NTC thermal resistance R3, the NTC thermal resistance R4, the equilibrium resistance R1 and the equilibrium resistance R2 form a Winston bridge and the Winston bridge is connected with a differential amplifying circuit. The utility model can measure the multiplex pulse high-power microwave power in millimetric wave band and the measuring range can be one kilowatt up to two or three megawatt.
Owner:SOUTHWESTERN INST OF PHYSICS

Adiabatic accelerating rate calorimeter with dynamic thermal inertia correction features

The invention discloses an adiabatic accelerating rate calorimeter with dynamic thermal inertia correction features. The adiabatic accelerating rate calorimeter comprises highly symmetrical dual testchannels, a standard heater, an external plugging type spherical reaction cell, a temperature and power measurement module, a system circuit board, and control software for data display and recording.The differences between the adiabatic accelerating rate calorimeter and a classical adiabatic accelerating rate calorimeter in structure and data processing are that: in terms of calorimetry, the adiabatic accelerating rate calorimeter can obtain dynamic thermal inertia factors in an adiabatic reaction process in real time by utilizing heating power of the standard heater measured by means of thetwo channel symmetric structure; and in terms of thermal analysis, for the deficiency that a thermal inertia factor is considered as a constant in the existing thermal analysis kinetics solving method based on adiabatic accelerated calorimetry, a novel kinetics solving method considers the dynamic changes of the thermal inertia factor and combines a non-linear fitting method for kinetics solution. The adiabatic accelerating rate calorimeter is higher in applicability, and is of great significance for improving the accuracy of the chemical reaction heat risk assessment.
Owner:CHINA JILIANG UNIV

Mixed calorimetry based specific heat calculating method for frozen soil

ActiveCN106770436ARaise the temperature field to predict the temperatureEnsure safetyMaterial heat developmentPreparing sample for investigationMaximum errorSoil science
The invention provides a mixed calorimetry based specific heat calculating method for frozen soil. The method comprises the following steps: a soil sample with the mass of m is taken, and water content w of the soil sample is measured; the soil sample is placed in a freezer at the constant negative temperature t lower than 0 DEG C for 60 h, and the total heat Q0 of the frozen soil sample is acquired; the frozen soil sample is placed in the freezer for 60 h; the total heat Q1 and Q2 required by the soil sample at the constant negative temperature (t-delta t) and (t+ delta t) for being heated to heat exchange balance temperature t1 and t2 from initial temperature are calculated respectively; the heat Q3 and Q4 are determined by measuring specific heat and content of soil particles and water; the specific heat c of the frozen soil sample at the specific negative temperature t is obtained according to a formula. The method has the beneficial effects that the specific heat of the frozen soil sample at a certain temperature point can be calculated precisely, conventional errors caused by thermal calculation based on average specific heat are improved, the minimum error is 0.039 DEG C, the maximum error is 0.5955 DEG C, and actual engineering needs can be met. Predicted temperature of a temperature field in a freezing method construction process can be increased to a larger extent by aid of precision improvement, and the safety of freezing method construction is guaranteed.
Owner:TIANJIN CHENGJIAN UNIV

Benzene imide structure based high-temperature self-crosslinking copolyester with effects of flame retardancy, smoke suppression and melt drop resistance and preparation method of copolyester

ActiveCN108359084APreserve thermoplastic processabilityIncrease melt viscosityStructural unitStructure based
The invention discloses a benzene imide structure based high-temperature self-crosslinking copolyester with effects of flame retardancy, smoke suppression and melt drop resistance. Copolyester is prepared from structural units represented by I, II and III or structural units represented by I, II and IV through random copolymerization, wherein the characteristic viscosity [eta] of copolyester is 0.41-1.12 dL / g, and the limit oxygen index is 24.2%-38.7%; the vertical combustion class is in a range from V-2 to V-0; the p-HRR (peak of heat release rate) in a cone calorimetry test is reduced by 7.1%-72.1% as compared with that of pure PET, and total smoke release is decreased by 2.0%-59.2% as compared with that of pure PET. The invention further discloses a preparation method of copolyester. Ahigh-temperature self-crosslinking group introduced in the preparation process is a benzene imide group, and prepared copolyeste cannot be subjected to crosslinking during processing and polymerization, so that thermoplastic processability of polyester is retained; meanwhile, due to the tackifying effect and high charring property brought by the self-crosslinking action at high temperature or during combustion, prepared copolyester has excellent flame retardancy, smoke suppression and melt drop resistance effects.
Owner:SICHUAN UNIV

A method for testing accuracy of animal breath calorimetry system

The invention discloses a method for inspecting the detection accuracy of an animal respiratory calorimetry system, which comprises the following steps: accurately weighing an alcohol lamp, wherein an appropriate amount of anhydrous alcohol is filled in the alcohol lamp; putting the alcohol lamp into a test chamber of a respiratory calorimetry system to be detected, and igniting the alcohol lamp to start a compensation test of the system; recording the start time and the internal and external temperatures, humidities and atmospheric pressures of the test chamber; after the system runs four operating cycles, extinguishing the alcohol lamp to complete the test; recording the end time, and weighing the alcohol lamp; and finally, according to the data acquired by the system, such as gas concentration, air mass flow, anhydrous alcohol consumption, burning time and the like, calculating the recovery ratios of carbon dioxide and oxygen, and then judging the detection accuracy of the animal respiratory calorimetry system. In the method disclosed by the invention, through burning the anhydrous alcohol, an animal respiratory test is simulated so as to rapidly and accurately assess the accuracy of detection results of the animal respiratory calorimetry system, thereby providing an important method and a technical means for the development of the verification test of the system.
Owner:INST OF ANIMAL SCI OF CHINESE ACAD OF AGRI SCI

Cold-hot stage type high-speed calorimeter capable of being combined with other microstructure characterization techniques

The invention discloses a cold-hot stage type high-speed calorimeter capable of being combined with other microstructure characterization techniques, and relates to the phase and microstructure analysis device technology field. The cold-hot stage type high-speed calorimeter includes a sample chamber having a light transmission transparent window and a light reflection transparent window on the wall, a cold-hot stage having the interior including a heating element and a refrigerant circulation pipeline for controlling the temperature and having a transmission hole, a sample chamber temperature control system and a high-speed calorimetric system. The cold-hot stage type high-speed calorimeter has the advantages that: 1, the high-speed calorimetric system having the temperature rising / dropping rate is miniaturized to the cold-hot stage, and with utilization of the reflection window, the transmission window and the cold-hot stage transmission hole, on-site combination of calorimetry and microstructure characterization are carried out; and 2, response is rapid through programmable control, sample temperature disturbance caused by incident light in structure measurement is dynamically compensated, the sample temperature is stabilized, thereby being conveniently used for researches on a metastable state.
Owner:NANJING UNIV
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