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82 results about "Diffractometer" patented technology

A diffractometer (pronunciation: di-"frak-'tä-m&-t&r) is a measuring instrument for analyzing the structure of a material from the scattering pattern produced when a beam of radiation or particles (such as X-rays or neutrons) interacts with it.

AI-based lithium manganate process parameter regulation and control method and system

The invention relates to the technical field of image processing, and discloses an AI-based lithium manganate process parameter regulation and control method and system. The method comprises the following steps: collecting lithium manganate preparation whole-process technological parameters through an infrared temperature measurement array, a pH sensor and an electrochemical workstation to establish a database, training and generating a technological parameter predictor by using an Actor-Critic deep reinforcement learning algorithm, quantifying a deviation degree output early warning level based on a fuzzy comprehensive evaluation algorithm, and determining the lithium manganate preparation whole-process early warning level according to the deviation degree output early warning level. And starting a self-adaptive PID control algorithm to generate a multi-equipment coordination control instruction set, synchronously driving an inclined mixer, a roasting kiln fan and an electrolytic bath temperature control system to adjust, detecting the product quality through an X-ray diffractometer, and feeding back an optimization control instruction. According to the invention, the process parameter control precision and the product quality stability in the lithium manganate preparation process are improved.
Owner:XINXIANG HONGLI SUPPLY SOURCE TECH CO LTD

X-ray diffractometer high temperature in-situ detection device

The application discloses an X-ray diffractometer high-temperature in-situ detection device, a base lifting assembly is installed on the diffractometer, a tank body assembly rear end is connected with a lifting pad in the base lifting assembly, and a tank body assembly front end is connected with an upper cover in a tank body cover assembly; a heat preservation cavity assembly is arranged in the tank body assembly; a heating chamber assembly is arranged in the heat preservation cavity assembly, and a connecting pipe at a tail of the heating chamber assembly is connected with a gas distribution connector in the tank body cover assembly; sample entering holes for sample passing are arranged at lower ends of the tank body assembly and the heat preservation cavity assembly; the tank body and the tank body cover are provided with cooling water channels; a sample holder assembly is fixed at the tank body assembly lower end, and a measured sample is placed in a sample holder in the sample holder assembly and is sent into the heating chamber assembly; the application has novel structure, stable performance and convenient use, and greatly improves the temperature range of the heating chamber. Since the heat preservation cavity is in a sealed form, the heating speed is fast, and heat preservation is long-lasting.
Owner:DANDONG HAOYUAN INSTR

Sample table for table type X-ray diffractometer

The invention provides a sample table for a table type X-ray diffractometer, and relates to the field of diffractometers, the sample table comprises a sample rack, a sample table structure is inserted in the sample rack, the sample rack is provided with a lifting locking part used for limiting the sample table structure, the lifting locking part comprises a first T-shaped tube mounted at the bottom of the sample rack, and the first T-shaped tube is provided with a second T-shaped tube; a second T-shaped pipe is inserted into the bottom end of the first T-shaped pipe, a second T-shaped rod is connected to the second T-shaped pipe in a penetrating mode, a first T-shaped rod is connected to the top end of the second T-shaped rod, the top of the first T-shaped rod penetrates through the sample frame and extends into the sample frame, and the top of the first T-shaped rod makes contact with the bottom of the sample table structure. According to the sample table structure, the lifting locking part is arranged, the lifting locking part can complete locking of the sample table structure in a mode of rotating after lifting, the lifting locking part can complete unlocking action by moving downwards and resetting after rotating, operation is convenient and fast, use is facilitated, and the abrasion problem of traditional screw adjustment is avoided.
Owner:EDU NANOTECHNOLOGY (SHANGHAI) CO LTD

Material surface and interface damage in-situ characterization system for multi-factor coupling corrosion

The invention provides a material surface and interface damage in-situ characterization system for multi-factor coupling corrosion, and relates to the technical field of in-situ detection equipment. The technical problem that in the prior art, in-situ microscopic observation cannot be conducted on a material surface interface in a simulated service environment, and the dynamic evolution rule of surface interface corrosion behaviors in the same area in the corrosion process cannot be accurately tracked is solved. According to the material surface and interface damage in-situ characterization system for multi-factor coupling corrosion, simulation of heat, salt and force multi-field coupling corrosion is achieved through a salt mist generating device, a multi-point heating module and a corrosion-resistant loading table, an X-ray diffractometer is allowed to conduct in-situ diffraction testing through an X-ray incident window and an X-ray emergent window, corrosion product in-situ phase analysis under the simulated working condition is achieved, and in-situ phase analysis of the corrosion product under the simulated working condition is achieved. And the corrosion-resistant loading table can enter the electron microscope for micro-area structure and micro-area component analysis, the multi-point heating module can keep the consistency of the sample state in the X-ray diffractometer and the electron microscope, and different heating sites can be used for heat, salt and force environment experiments.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACAD OF SCI

Silver electrode and method of manufacturing silver electrode

The present invention provides a silver electrode having smaller change in resistivity due to temperature change as compared with the related arts, and a method of manufacturing the silver electrode. The silver electrode is configured to have one peak in a range of a diffraction angle 2θ=37.5° to 38.3° in an X-ray diffraction pattern measured by an X-ray diffractometer using a CuKα1 ray, and a change rate of the diffraction angle of the peak after heated at 150° C. for 30 minutes is less than or equal to 0.5%. In this way, the silver electrode has smaller change in resistivity due to temperature change as compared with the related arts.
Owner:KANEKA CORP

An x-ray diffractometer sample stage for bulk solid samples

An X-ray diffractometer sample stage for bulk solid samples is disclosed. In use, the base is moved to the designated position, and the bulk solid sample is placed on the sample stage within the sample placement groove and secured with modeling clay. Since there are three wedge mechanisms arranged in a triangle, based on the principle that three points not on the same straight line can define a plane, the three wedge mechanisms can support the sample stage. Furthermore, because the wedge mechanisms drive the bottom of the sample stage and can convert horizontal movement into vertical movement, the corresponding parts of the sample stage can be raised or lowered by the wedge mechanisms, thereby adjusting the height and angle of the sample stage. This eliminates the need for cutting or processing the bulk solid sample, simplifying operation. When the sample quantity is small, there is no need to lay a large amount of modeling clay on the sample stage, making it more convenient to use. In summary, by using this sample stage, the depth and angle of the sample stage can be adjusted.
Owner:NORTHWEST A & F UNIV

Preparation and application of hollow mesoporous COF-carboxylic acid / chiral amide multi-catalyst

The invention aims to establish a synergistic catalytic system in which catalysts cannot coexist. The amide chiral catalyst is prepared through a series of synthesis. The hollow mesoporous COF-carboxylic acid / chiral amide multi-catalyst is prepared by a hydrothermal method. The morphology and the structure of the material are characterized by using a scanning electron microscope, a transmission electron microscope, an X-ray diffractometer, a specific surface instrument, an infrared spectrometer and the like, an asymmetric tandem-addition reaction is catalyzed to construct a chiral acetal compound, high performance liquid chromatography analysis is combined, and multiple catalysts are continuously recycled. Results show that the hollow mesoporous COF-carboxylic acid / chiral amide multi-catalyst not only has good morphology, excellent specific surface area and high porosity, but also enables contradictory catalysts to coexist for synergistic catalysis. The catalyst can be used for rapidly catalyzing an asymmetric tandem-addition reaction, high selectivity of ee = 99% and high yield of 98% are achieved, and the catalyst can be repeatedly used for 10 times. The method is green, environment-friendly, low in cost and suitable for concerted catalysis of catalysts which cannot coexist.
Owner:CHONGQING UNIV OF POSTS & TELECOMM

X-ray diffractometer sample table compatible with different manufacturers

The invention belongs to the related technical field of diffractometer corollary equipment, and discloses an X-ray diffractometer sample stage compatible with different manufacturers, which comprises three structural layers in vertical layering and splicing design, the X-ray diffractometer and goniometer butt joint layer is used for being in butt joint with X-ray diffractometers and goniometer of different manufacturers, and meanwhile splicing with the core function execution layer is achieved through a conical surface positioning pin, an annular magnetic attraction groove and the like. An independent driving and control module is arranged in the core function execution layer and is used for independently completing the functions of translation, rotation, inclination angle adjustment and the like; the sample bearing and fixing layer is provided with a plurality of sample clamps matched with samples in different forms. The technical problems that mechanical interfaces of sample tables of different manufacturers are not uniform, control protocols are not compatible, and recalibration is needed after replacement are effectively solved, and the sample table has the advantages of being compact in structure, convenient to control, high in switching efficiency, accurate and reliable in positioning, capable of achieving plug and play and the like.
Owner:HUAZHONG UNIV OF SCI & TECH

Special fixture for sample detection of X-ray diffractometer

The utility model relates to the field of X-ray diffraction, in particular to a special fixture for sample detection of an X-ray diffractometer, which is used for being matched with the X-ray diffractometer to carry out phase analysis and residual stress test and is suitable for residual stress detection of workpieces with square and cylindrical structures. The utility model aims to provide a special fixture for sample detection of an X-ray diffractometer. The fixture has the characteristics of simplicity in operation and high positioning precision. According to the technical scheme, the clamp special for sample detection of the X-ray diffractometer is characterized by comprising a base, a limiting plate fixed to the top of the base, a supporting plate located between the base and the limiting plate in a liftable mode, and a spring pushing the supporting plate to ascend so that a workpiece can be clamped and fixed between the supporting plate and the limiting plate; a detection cavity allowing the supporting plate to ascend and descend and containing a workpiece is formed in the base, the limiting plate is provided with a detection hole allowing X-rays to irradiate the workpiece, and the bottom face of the limiting plate serves as a positioning face for determining the highest point position of the workpiece.
Owner:ZHEJIANG PROVINCIAL SPECIAL EQUIP INSPECTION & RES INST

Solid electrolyte, active material, electrode mixture, solid electrolyte layer, and solid-state battery

The present invention addresses the problem of providing a solid-state battery and active material capable of suppressing decreases in the recovery capacity of the solid-state battery and capable of suppressing increases in the resistance of the solid-state battery, even if the solid-state battery is stored in a high-temperature environment in a charged state. A solid electrolyte, according to the present invention, contains a lithium (Li) element, a phosphorus (P) element, a sulfur (S) element, an oxygen (O) element, and a halogen (X) element. The molar ratio of the halogen (X) element to the phosphorus (P) element is less than 1.2. The molar ratio of the oxygen (O) element to the phosphorus (P) element is greater than 0.001 but less than 1.0. According to the present invention, the X-ray diffraction pattern measured by an X-ray diffractometer using Cu Kα radiation has diffraction peaks at a position of 2θ=15.4°±1° and at a position of 2θ=17.8°±1°.
Owner:MITSUI MINING & SMELTING CO LTD

Concentric ring roll sample table for wide-angle X-ray diffractometer and use method

The invention discloses a concentric ring roll sample table for a wide-angle X-ray diffractometer and a use method, and belongs to the technical field of X-ray diffraction analysis equipment.The concentric ring roll sample table comprises a base and a concentric ring sample table body arranged on the base, and the concentric ring sample table body comprises an external supporting seat and an internal rotating circular ring sleeve; the rotary circular ring sleeve is rotatably connected to the supporting seat through an angle adjusting mechanism, and the rotation axis of the rotary circular ring sleeve is configured to coincide with the direction of an incident X-ray beam, so that a sample fixed on the rotary circular ring sleeve can roll and rotate around an incident light path. Through the unique concentric ring design, it is ensured that the rotation axis of a sample coincides with an X-ray light path, the position of a measured point of the sample is constant in the rotation process, the side inclination range of 60 degrees is achieved through cooperation with the fine adjustment bolt, the measurement blank between vertical transmission and grazing incidence is filled, and the measurement precision is improved. And a key tool is provided for all-dimensional structure characterization of anisotropic materials.
Owner:SUZHOU LABORATORY

Method for measuring original austenite grain size of low-alloy quenched steel by X-ray diffractometer method

The invention discloses a method for determining the original austenite grain size of low-alloy quenched steel by an X-ray diffractometer method, and belongs to the technical field of metal material detection. According to the method provided by the invention, nondestructive testing is realized by establishing the quantitative relation model of the martensite phase change product and the original grain size, chemical erosion and mechanical damage of a traditional metallographic method to a sample are avoided, and the problems of large destructiveness, complex operation, limited application range and the like of a traditional detection means are solved; the method can be directly used for quality inspection of finished products, and a new technical means is provided for whole-process quality control of steel products. An optimized diffraction peak analysis algorithm is combined, so that the measurement precision is remarkably improved; the detection process is simple, convenient and efficient, the single detection time can be shortened to be within 30 minutes, the detection efficiency is greatly improved, and the method is particularly suitable for rapid detection requirements of batch samples.
Owner:ANGANG STEEL CO LTD

X-ray system and method for tissue structural analysis and imaging

In some embodiments, an X-ray system comprises a work-station and a mammography apparatus. The mammography apparatus can comprise: a breast positioning area; an absorption contrast imaging apparatus; and a diffractometer for analyzing structure of tissue within a breast. The absorption contrast imaging apparatus and the diffractometer can be configured to move in order to interchangeably align with the breast positioning area. The work-station can be configured to control the mammography apparatus, and to process data received from the mammography apparatus. In some embodiments, a method of controlling an X-ray system comprises: measuring the denseness of the breast tissue using an absorption contrast imaging apparatus; processing the absorption contrast imaging measurement results using the work-station to determine coordinates of potential cancer sites; performing measurements at the coordinates of the potential cancer sites using the diffractometer; and processing the diffractometer measurement results to perform diagnostics.
Owner:EOSDX INC

A method for assessing the aging of a cable sheath and related devices

The application discloses a cable sheath aging evaluation method and related device, comprising: intercepting a test sample from a cable sheath to be evaluated, wiping the test sample with alcohol and keeping it still; testing the test sample by using a RIGAKU-X ray polycrystalline diffractometer, recording an X ray diffraction pattern of the test sample, obtaining two crystalline diffraction peak intensities D fi and D si of a diffraction curve and angles θ fi and θ si corresponding to the two peaks according to the X ray diffraction pattern; substituting the two crystalline diffraction peak intensities D fi and D si and the angles θ fi and θ si corresponding to the two peaks into a diffraction evaluation factor calculation formula to obtain a diffraction evaluation factor; and analyzing an aging state of the cable sheath to be evaluated based on the diffraction evaluation factor. The application can conveniently, efficiently and safely detect and evaluate the aging degree of a 110kV XLPE cable sheath, and avoids damage and grounding faults caused by serious aging of the cable sheath.
Owner:GUANGDONG POWER GRID CO LTD +1

Method for measuring original austenite grain size of high alloy steel by X-ray diffractometer method

The invention discloses a method for measuring the original austenite grain size of high alloy steel through an X-ray diffractometer method, and belongs to the technical field of metal material detection. According to the method provided by the invention, nondestructive testing is realized by establishing the quantitative relation model of the martensite phase change product and the original grain size, chemical erosion and mechanical damage of a traditional metallographic method to a sample are avoided, the method can be directly used for quality inspection of a finished product, and a new technical means is provided for whole-process quality control of a steel product; an optimized diffraction peak analysis algorithm is combined, so that the measurement precision is remarkably improved; the detection process is simple, convenient and efficient, the single detection time can be shortened to be within 30 minutes, the detection efficiency is greatly improved, and the method is particularly suitable for rapid detection requirements of batch samples.
Owner:ANGANG STEEL CO LTD

Tissue diffractometer for determining a diagnostic indicator

The present disclosure provides systems and methods for determining one or more diagnostic indicators using X-ray diffraction (XRD). In some embodiments, the techniques described herein relate to a system including: a fixture configured to position a region of skin of a patient within a measurement region; an X-ray source coupled to the fixture and configured to emit an X-ray beam that overlaps with the measurement region; an X-ray receiver coupled to the fixture, the X-ray receiver including a coordinate-sensitive digital detector of X-rays; and one or more processors coupled to the X-ray receiver. The one or more processors can be configured to collect XRD data from the X-ray receiver, to process the XRD data, and to determine a diagnostic indicator for assessment of a physiological or pathological condition based on the processed XRD data.
Owner:EOSDX INC

Method and system for rapidly detecting TiC in carbide slag

The invention belongs to the field of chemistry, and relates to a method and a system for rapidly detecting TiC in carbide slag. The method comprises the following steps: preparing a standard sample: preparing a series of carbide slag standard samples with known TiC content; acquiring XRD (X-Ray Diffraction) data: scanning the standard sample and the sample to be detected by using an X-ray diffractometer in a range of 2theta = 34-38 degrees to obtain a diffraction pattern; processing data and drawing a standard working curve: extracting a characteristic diffraction peak of TiC at 2theta = 36.1 + / -0.2 degrees, carrying out area integration, and establishing a standard working curve of the TiC content and a peak area integral value; and determining an unknown sample: carrying out the same treatment on the sample to be detected, substituting the peak area integral value into the standard working curve, and calculating to obtain the TiC content. According to the method, a diffraction peak with a diffraction angle 2theta of 36.1 degrees is adopted for fitting and then quantitative analysis is performed, so that the problem of long consumed time of an existing method for measuring the content of TiC in the carbide slag is solved.
Owner:PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP

A method of cutting a superalloy seed

The application discloses a high-temperature alloy seed crystal cutting method, which comprises the following steps: firstly, a single crystal test plate with a near [001] orientation under space operation conditions is prepared; according to the position of a specific orientation point of a seed crystal to be prepared in a inverse pole figure, the direction angle θ and the φ angle of the orientation are calculated, and the θ and the φ are converted into corresponding angles in the Laue method by a formula; after the [001] direction is calibrated by a diffractometer and a three-axis rotating tool, the seed crystal with the specific orientation in the inverse pole figure is cut by using the calculated angles. The method adopts the single crystal plate with preparation conditions, utilizes a tool capable of rotating in three directions, realizes the cutting of the seed crystal with any orientation in the inverse pole figure, and simultaneously corresponds the rotating angles in the single crystal cutting to the angles in the existing general standard, namely, the Laue method for measuring crystal orientation, so that the seed crystal with any orientation in the inverse pole figure can be quickly and conveniently cut.
Owner:SHENZHEN WANZE ZHONGNAN RES INST CO LTD +1

Microcapsule for latent heat storage materials, method for producing same, powder containing microcapsules for latent heat storage materials, and heat storage device comprising said powder

A microcapsule for latent heat storage materials includes a metal core containing Zn and Al and a shell covering the metal core. The shell of the microcapsule includes an oxide film containing Zn and O, and an oxide film containing Al and O adjacent to an inner side of the oxide film containing Zn and O. In the microcapsule, a mass ratio of ZnAl2O4 is 4% or less. The mass ratio is determined by analyzing the microcapsule by an XRD (X-ray diffractometer) device and subjecting results to quantitative analysis using a RIR (Reference Integrity Ratio) method.
Owner:HOKKAIDO UNIVERSITY

A water-soluble fertilizer microelement precise feeding and continuous mixing preparation method for soil improvement

This invention discloses a method for precise feeding and continuous mixing of water-soluble micronutrient fertilizers for soil improvement, belonging to the field of organic fertilizer manufacturing technology. The method includes: classifying the substrate and monitoring the flow rate and controlling the fluctuation rate using a Coriolis mass flow meter; employing a loss-in-weight precision feeding system for multi-channel feeding, combined with an ultrasonic transducer to prevent bridging; premixing the micronutrient powder with liquid to form a slurry, and injecting it into a microfluidic pre-chelation reactor for rapid chelation; achieving microscopic uniform dispersion using a twin-screw continuous mixer combined with a chaotic mixing flow field; and real-time detection using a near-infrared spectroscopy online analyzer and a laser diffractometer, combined with a PID algorithm closed-loop feedback to adjust the feeding speed. This invention solves the problems of low precision in micronutrient addition and uneven mixing in existing technologies, improves feeding accuracy and product uniformity, and is suitable for continuous large-scale production.
Owner:KUQA SHENGTAI TECH DEV CO LTD

New feed additive potassium magnesium sulfate production equipment and method thereof

The invention relates to the technical field of production of an additive potassium magnesium sulfate, and discloses production equipment of a new feed additive potassium magnesium sulfate. A lattice reconstruction furnace; a cold drying device; an internal dedusting fluidized drying machine; a granulator; a screen box; a passivation packaging line is provided with a magnesium stearate spraying bin (the spraying amount is 0.1%-0.5%) and a vacuum packaging machine. According to the new feed additive potassium magnesium sulfate production equipment and the method thereof, by arranging segmented drying-lattice reconstruction integrated equipment (a roller dryer and a lattice reconstruction furnace) and an orthogonal feedback module, picromerite is directly and efficiently converted, the moisture content is accurately controlled to be smaller than or equal to 5% through double-layer hot air circulation (120 DEG C to 150 DEG C), the crystal water removal rate is larger than or equal to 99%, and the production efficiency is greatly improved. A crushing / mixing pretreatment link is omitted, and the process is shortened by 30%; the purity is monitored in real time by an X-ray diffractometer, calcination parameters are dynamically adjusted in combination with a function Y = 0.35 X1 + 0.28 X2 + 0.22 X3 + 0.15 X4, the conversion rate of K2Mg2 (SO4) 3 is stably larger than or equal to 90%, and the problem that lattice conversion is not accurate is solved.
Owner:QINGHAI LANHUSHANCHENG BIO-TECH CO LTD

An aeroengine blade clamping mechanism

The present application relates to a kind of aero-engine blade clamping mechanism, fixed seat is fixedly installed on diffractometer, sliding table is movably installed on fixed seat along first direction, rotating frame is rotatably installed on sliding table along second direction, clamping assembly for clamping blade is rotatably installed on rotating frame along third direction, two clamping jaws of clamping assembly at different heights are respectively installed on two piston rods and open-close action is carried out under the push of piston rod, clamping column is rotatably installed on clamping jaw and cooperates with clamping jaw to embed in the groove of tenon of blade to realize clamping.According to the aero-engine blade clamping mechanism of the present application, the diffractometer is fixed by horizontal fixed seat, the irregular tenon of blade can be clamped by clamping column, different models of blade can be clamped and positioning is reliable by air cylinder, three degrees of freedom motion of blade is realized, three degrees of freedom are used to adjust blade to be compatible with diffractometer, and X-ray nondestructive testing is realized.
Owner:SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI

X-ray diffraction sample holder for crystal form structure analysis of ophthalmic implant

The invention discloses an X-ray diffraction sample holder for crystal form structure analysis of an ophthalmic implant, and belongs to the technical field of X-ray diffraction analysis sample holders, the X-ray diffraction sample holder comprises an X-ray diffractometer, the inner part of the X-ray diffractometer is rotatably connected with a sample holder; the rotating unit is rotationally connected inside the X-ray diffractometer and is connected with the center of the sample holder; a lifting frame is connected into the X-ray diffractometer in a sliding mode, the lifting frame is of a T-shaped structure, and a grinding unit, a trowelling unit and a cleaning unit are installed at the three ends of the lifting frame respectively. When sample powder in a placement groove rotates to a next station, a through hole is completely communicated with the bottom of the placement groove under the magnetic action of an electromagnet and a magnetic part, and at the moment, the ophthalmic implant sample powder in the placement groove is pushed into a sample groove in a sample seat under the action of a conical feeding frame; and the whole-process automation of the sample from grinding, positioning to feeding is realized.
Owner:JIANGSU KEBIAO MEDICAL TECH GRP CO LTD

In-situ characterization system for material surface and interface damage in multi-factor coupled corrosion

The application provides a material surface interface damage in-situ characterization system for multi-factor coupled corrosion, relates to the technical field of in-situ detection equipment, and aims to solve the technical problems that the material surface interface cannot be observed in-situ under a simulated service environment and the corrosion behavior dynamic evolution rule of the same area in a corrosion process cannot be accurately tracked in the prior art. The material surface interface damage in-situ characterization system for multi-factor coupled corrosion is realized by a salt mist generating device, a multi-point heating module and a corrosion-resistant loading table to simulate multi-field coupled corrosion of heat, salt and force, X-ray incidence and X-ray emission windows allow an X-ray diffractometer to perform in-situ diffraction testing, in-situ phase analysis of corrosion products under simulated working conditions is realized, the corrosion-resistant loading table can enter an electron microscope to perform micro-area structure and micro-area component analysis, the multi-point heating module can keep the sample state consistent in the X-ray diffractometer and the electron microscope, and different heating points can perform environmental experiments of heat, salt and force.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACAD OF SCI

Fine-adjustable bicrystal monochromator for X-ray diffractometer

The utility model discloses a fine-adjustable bicrystal monochromator for an X-ray diffractometer, belongs to the technical field of X-rays, and aims to solve the problem that a traditional U-shaped crystal monochromator is high in price due to the fact that the difficulty of a processing mode is high and the yield is low in the prior art. The utility model relates to a fine-adjustable bicrystal monochromator for an X-ray diffractometer. The fine-adjustable bicrystal monochromator comprises a U-shaped bicrystal fixing piece; a first crystal; the crystal adjusting mechanism is arranged below the first crystal, the crystal adjusting mechanism is fixed on one side of the U-shaped double-crystal fixing piece, and the first crystal swings around the X axis, the Y axis and the Z axis through the crystal adjusting mechanism; the crystal face of the second crystal and the crystal face of the first crystal are oppositely arranged; the first crystal and the second crystal are complete crystals of the same kind, and two opposite crystal faces have the same parallelism; the balancing weight is arranged below the second crystal; and the balancing weight is fixed on the other side of the U-shaped double-crystal fixing piece.
Owner:SUZHOU LIYING TECH CO LTD

A method for identifying bauxite adulterated with secondary aluminum dross

The application relates to a method for identifying bauxite doped with secondary aluminum ash, and belongs to the technical field of chemical analysis. The application realizes rapid preliminary screening and accurate quantitative confirmation of the secondary aluminum ash doped in the bauxite, uses ion chromatography equipment popularized in an alumina plant to replace an expensive X-ray diffractometer, solves the technical problems of high detection cost and long period, and improves the reliability of the identification result through double verification of precipitation observation and ion quantification.
Owner:TESTING TECHNOLOGY (ZHENGZHOU) CO LTD OF CHALCO

A test method for coating residual stress testing

The application provides a test method for coating residual stress test, aiming at the particularity of the coating and the problems existing in the actual detection, studies the component composition and phase analysis of the coating, and establishes a test method for testing the residual stress of the coating by using different X-ray diffraction emission sources. Therefore, in the residual stress test of the coating, in addition to the basic preparation work including the component analysis and the phase analysis, the 2theta angle conversion between different ray sources is carried out according to the Bragg law, that is, the diffraction characteristics of different ray sources, and then the X-ray stress constant is further calculated, the residual stress calculation formula is introduced, and the residual stress database is established. The application has the advantages that: aiming at the component composition and phase analysis of the coating, the physical characteristics of different emission ray sources are used to calculate the residual stress value, the test demand of the X-ray diffractometer can be flexibly met, the residual stress test of the coating with different components can be met, and the practical value is great.
Owner:SHENYANG LIMING AERO-ENGINE GROUP CORPORATION

An x-ray diffraction sample holder for ophthalmic implant crystal form analysis

The application discloses an X-ray diffraction sample holder for ophthalmic implant crystal form structure analysis and belongs to the technical field of X-ray diffraction analysis sample holders, which comprises an X-ray diffractometer, a sample holder rotatably connected to the inside of the X-ray diffractometer, a rotating unit rotatably connected to the inside of the X-ray diffractometer and connected to the center of the sample holder, a lifting frame slidably connected to the inside of the X-ray diffractometer, and a grinding unit, a leveling unit and a cleaning unit respectively installed at three ends of the lifting frame in a T-shaped structure. When sample powder in a placing groove is rotated to the next station, the through hole is completely communicated with the bottom of the placing groove under the magnetic action of an electromagnet and a magnetic part, at which time the ophthalmic implant sample powder in the placing groove is pushed into a sample groove in a sample seat under the action of a conical feeding frame, and full automation of the ophthalmic implant sample from grinding, positioning to feeding is realized.
Owner:JIANGSU KEBIAO MEDICAL TECH GRP CO LTD

Preparation and analysis method of hot-dip Zn.Al.Mg series alloy coating

The invention provides a preparation and analysis method of a hot-dip Zn-Al-Mg alloy coating, and belongs to the technical field of metal surface coating. The preparation method comprises the steps of steel strip pretreatment, hot dipping and post-plating treatment, and an alloy plating layer with a uniform structure is obtained by controlling parameters of all working procedures; the invention also provides a matched coating analysis method which comprises the following steps: performing phase analysis by adopting an X-ray diffractometer, and performing quantitative characterization on the microscopic structure of the coating by adopting a scanning electron microscope in combination with image analysis software. The corrosion resistance of the coating is remarkably improved by increasing the content of Al and cooperatively adding Mg and Si, the microstructure characteristics of the coating are revealed through analysis, a theoretical basis is provided for component optimization and process control, and industrial application prospects are achieved.
Owner:JIUGANG GROUP GANSU HONGXING HONGYU NEW MATERIALS CO LTD