The invention provides a sample
pretreatment method for in-situ analysis of impurities in high-purity
quartz sand, which comprises the following steps: crushing, screening, scrubbing, desliming and grading a raw ore sample to obtain a mineral with the particle size of-2mm + 0.5 mm; carrying out
quartz single mineral selection on minerals with the particle size of + 0.5 mm by adopting an
optical microscope; the method comprises the following steps: uniformly dispersing selected
quartz single minerals on a
glass slide, and preparing an oil-immersed sheet; placing the oil immersed sheet under a polarizing
microscope, selecting quartz single
mineral particles with low gas-liquid inclusion content, and cleaning and
drying the quartz single
mineral particles; and embedding the quartz single
mineral particles into
epoxy resin,
polishing and cleaning to obtain the high-purity quartz
sand sample target sheet. According to the method, an
oil immersion observation method is firstly adopted to select quartz single minerals with relatively low gas-liquid inclusion content, so that the sample representativeness of subsequent in-situ analysis test is ensured; then,
epoxy resin is adopted for embedding,
polishing and cleaning, target material preparation is simplified, and secondary
pollution to a to-be-detected surface is avoided.