The present application relates to a kind of hollow small ball
heat resistance visualization evaluation method based on high temperature
microscope technique.First, temperature calibration is carried out to high temperature metallographic
microscope, second, 1-10mg hollow small ball is evenly sprinkled on
glass slide using
medicine spoon, and the
glass slide is vibrated, so that the hollow small ball on it is single layer distribution, not mutually overlapping, shielding, in 600-1000 ℃ temperature interval, at least three grades of temperature increasing rate is used to heat, and the state of hollow small ball under each temperature increasing rate is recorded in real time using
video image.Subsequently, according to the state continuous change spectrum of
microsphere in heating process, the temperature T m1 、 m2 、 m3 of 50±5% proportion of hollow small ball in a certain
field of view is determined, which softens and collapses.Finally, the
softening temperature T m1 、 m2 、 m3 of hollow small ball under at least three grades of temperature increasing rate is linearly fitted, and the
softening temperature T m of hollow small ball at heating speed of 0 ℃ / min, i.e., constant temperature, is obtained, which is the
heat resistance characteristic temperature in equilibrium state.