4491 results about "Centrifugal separation" patented technology

The invention relates to the field of electric heating materials, and provides a graphene-based heating coating and a preparation method thereof. The coating is prepared from functionalized graphene, a surface modified bismuth telluride nanobelt, polyaniline, bisphenol A epoxy acrylate, polyurethane acrylate, a dispersing agent, a flatting agent, a silane coupling agent, a defoaming agent and a propylene glycol methyl ether acetate / N-methyl pyrrolidone mixed solvent. The functionalized graphene is obtained by modifying a hyperbranched polyolefin-acryloyl-POSS copolymer, and carrying out ultrasonic stripping, centrifugal separation, gradient washing and vacuum drying; the surface-modified bismuth telluride nanobelt is modified by an amino silane coupling agent, so that the interfacial compatibility is improved. The preparation method comprises the steps of solvent premixing, nanofiller dispersion, ultrasonic homogenization, coupling agent modification, ultraviolet curing and thermocuring. The heating coating provided by the invention has high conductivity, excellent thermal stability and adhesive force, and can be widely applied to heating electric appliances and intelligent temperature control equipment.

The invention discloses an intelligent control method of a zinc ash-containing tail gas purification system, which relates to the technical field of tail gas purification systems, and comprises the following steps of: firstly, continuously monitoring a condensation process of high-temperature zinc-containing steam in a cooler through a monitoring device, and collecting zinc steam condensation conditions and particle generation data of tail gas under different temperature and pressure states in real time; according to the invention, intelligent monitoring, signal analysis, machine learning identification and dynamic regulation and control are combined to realize accurate control of the zinc-ash-containing tail gas purification system. Key features are extracted through real-time monitoring and data preprocessing, intelligent recognition of particle concentration is achieved based on feature vectors and machine learning, the rotating speed of the centrifugal separator is adjusted in a self-adaptive mode, and efficient separation and system stability are ensured by linkage with pulse back-blowing dust removal. Compared with a traditional fixed rotating speed mode, the tail gas purification efficiency is improved, the maintenance cost is reduced, the service life of equipment is prolonged, the automatic operation capacity is enhanced, and the system is kept in the optimal working state during load fluctuation.

The invention relates to a method for preparing lithium sulfide, which comprises the following steps: respectively dissolving a sulfur source compound and a lithium source compound in alcohol under the protection of inert atmosphere, and then mixing the two alcohol solutions for double decomposition reaction to generate a lithium sulfide suspension; and then carrying out evaporative crystallization, supercritical fluid washing, centrifugal separation and freeze drying treatment to obtain a lithium sulfide product. The purity of the lithium sulfide prepared through the method can reach 99.9% or above, the lithium sulfide can be used as a positive electrode material of a lithium-sulfur battery or a raw material of a sulfide solid electrolyte in an all-solid-state battery, and the method is low in energy consumption, conforms to the concept of green chemistry and is suitable for large-scale industrial production.

The invention relates to a silicon-carbon composite material and a preparation method and application thereof.The preparation method comprises the steps that a porous graphite raw material is subjected to acid pickling and smashing to obtain pretreated porous graphite, then the pretreated porous graphite is soaked in a carbon precursor solution in a vacuum mode, carbonization treatment is conducted after centrifugal separation, pores of the porous graphite are filled with carbides, physical activation is conducted, and the silicon-carbon composite material is obtained; the preparation method comprises the following steps: forming pores in a carbide to form a graded pore structure to obtain a porous graphite composite material, then carrying out silicon deposition in a fluidized bed to obtain a uniform nano silicon layer, and then carrying out carbon coating treatment to obtain a silicon-carbon composite material; the graphite with relatively low cost is adopted as a matrix, high capacity and long cycle performance of the graphite-based silicon-carbon negative electrode material are realized through hierarchical pore structure design, carbonization-activation synergistic pore forming and interface deposition process optimization, and the graphite-based silicon-carbon negative electrode material can be applied to the fields of power batteries and high-energy-density energy storage, especially the field of lithium ion batteries and has wide application prospects. The expansion rate of the battery can be reduced, and the specific capacity, cycling stability and safety of the lithium ion battery can be improved.

The invention discloses a centrifugal separation device for kelp processing and a use method of the centrifugal separation device, and belongs to the technical field of kelp centrifugal separation devices. Comprising a first cavity cylinder, a second cavity cylinder, a second servo motor and a separation disc, a plurality of sets of dynamic adjusting mechanisms are sequentially arranged and installed at the outer edge of the upper surface of the separation disc in a circumferential mode, a dehydration cylinder is formed through the dynamic adjusting mechanisms, and gas is injected in a reciprocating mode in the centrifugal separation process through dynamic adjustment; compared with a passive scheme depending on a flexible lining or rotating speed adjustment in the background technology, the active intervention mechanism can adjust the kelp distribution state in real time, and a moisture discharge channel is prevented from being blocked.

The invention discloses industrial-grade mixed oil produced by utilizing kitchen waste oil and a preparation method of the industrial-grade mixed oil, and belongs to the technical field of recycling of the kitchen waste oil. The invention relates to industrial-grade mixed oil produced by using kitchen waste oil and a preparation method thereof, and the preparation method comprises the following steps: firstly collecting kitchen waste containing the waste oil, and storing the kitchen waste in a container through special equipment; carrying out screen solid-liquid separation, cleaning grease on the surface of the solid waste, and then carrying out precipitation separation; then carrying out centrifugal separation, chemical cleaning, water washing, acid treatment, dehydration, degumming and metal ion removal on the separated grease and oil-containing liquid; carrying out ultrasonic-assisted multistage ester exchange after enzymolysis optimization, carrying out membrane separation on glycerol and fatty acid methyl ester, and carrying out reduced pressure distillation to obtain a high-purity fraction; carrying out adsorption refining, plasma treatment and supercritical fluid extraction; finally, nano particles are added and blended with additives, efficient recycling of the kitchen waste oil is achieved, and then high-purity industrial-grade mixed oil is prepared.

The invention discloses a preparation method and application of an amorphous nickel-cobalt-iron phosphate anode catalyst, and belongs to the technical field of alkaline water electrolysis hydrogen production, the preparation method comprises the following steps: (1) dissolving transition metal salt in a solvent, and stirring to obtain a metal salt solution; (2) dissolving phosphate in a solvent, and stirring to obtain a phosphate solution; and (3) adding the phosphate solution into the metal salt solution for reaction, washing with deionized water and ethanol, centrifugally separating, and drying to obtain the amorphous nickel-cobalt-iron phosphate anode catalyst. According to the preparation method and application of the amorphous nickel-cobalt-iron phosphate anode catalyst, process safety improvement and environmental friendliness optimization are achieved through an all-water-phase green synthesis system, the obtained catalyst shows excellent performance in an AEM electrolytic cell, the cell voltage is only 1.87 V under the current density of 2 A / cm, and the method has remarkable industrial application prospects.

The invention relates to the technical field of blood potassium detection, in particular to a blood potassium detection paper-based sensor and a preparation method and application thereof.The sensor is obtained by integrating a substrate, a sensing electrode and a whole blood microfluid channel, and the sensing electrode is located between the substrate and the whole blood microfluid channel; the whole blood microfluid channel comprises a serum diffusion area, a whole blood separation area positioned above the serum diffusion area and a blood potassium detection area positioned below the serum diffusion area; a blood separation membrane is also arranged in the whole blood separation area; the substrate is qualitative filter paper, and the sensing electrode comprises an all-solid-state PBA working electrode and an Ag / AgCl reference electrode; compared with the prior art, calibration is not needed when potassium ions in whole blood are detected, the whole blood sample can be directly used, centrifugal separation is not needed, the detection speed is increased, the hemolysis problem of the whole blood sample in blood potassium detection can be avoided, and the detection sensitivity, accuracy and stability are further improved.

The invention discloses a multifunctional composite material for mineralizing and storing CO2 based on fly ash and a preparation method of the multifunctional composite material. The material is prepared from high-activity fly ash subjected to plasma activation treatment, a nanoscale metal oxide catalyst, a metal organic framework, a functional organic ligand, an intelligent pH regulator, a solid suspension stabilizer and water. The preparation method comprises the steps of suspension preparation, high-pressure CO2 mineralization reaction in a reaction kettle, centrifugal separation and freeze drying treatment. The method is simple, the raw material cost is low, the prepared multifunctional composite material not only can remarkably improve the storage efficiency of CO2, but also can ensure that a stable carbonate product is generated, and the carbonate product has high specific surface area and excellent chemical stability, can be widely applied to the fields of high-end building materials, energy storage materials and fine chemical engineering, and has wide application prospects. And meanwhile, the high-added-value utilization of the industrial by-product fly ash is realized, and the dual purposes of reducing carbon emission and improving the utilization rate of solid wastes are achieved.

The invention discloses a preparation method of an In2O3-Cu-Cu2O ternary heterojunction catalyst and a preparation method of the In2O3-Cu-Cu2O ternary heterojunction catalyst. The method comprises the following steps: at room temperature and normal pressure, firstly, dissolving indium chloride tetrahydrate in a mixed solvent of ethylenediamine-ethylene glycol (the volume ratio is 1: 20-1: 30) and dihydric alcohol amine to obtain a homogeneous solution; then transferring the solution to a hydrothermal kettle, adding deionized water and Cu2O powder with different volumes, and carrying out hydrothermal crystallization at 160-200 DEG C for 10-14 hours; and centrifuging the obtained precipitate, alternately washing with water and alcohol for 2-3 times, carrying out vacuum drying at 60 DEG C for 5-7 hours, heating to 600 + / -10 DEG C at a speed of 3-5 DEG C / min in an N2 atmosphere, calcining for 3 hours, and cooling along with a furnace to obtain a target product. By adjusting the adding amount of the deionized water, the mass proportion of the three phases of In2O3, Cu and Cu2O can be continuously adjusted and controlled, and controllable preparation from'rich copper 'to'rich cuprous oxide' and'stable ternary 'is achieved.

The invention provides application of a turbellarian worm extract in preparation of a product for promoting wound healing, a biological agent for promoting the proliferation activity and / or migration ability of fibroblast NIH3T3, a biological agent for improving the wound healing rate and the decrustation time and a biological agent for improving the collagen fiber deposition type in the wound healing process. The biological preparation is used for promoting regeneration of skin appendage organs in the wound healing process. Wherein the extraction of the turbellarian worm extract comprises the steps of turbellarian worm cleaning, tissue crushing, alcohol extraction, centrifugal separation and concentration drying. The turbellarian worm extract has good capacity of promoting wound healing, and has the effects of effectively improving skin wound healing efficiency, shortening decrustation time, inhibiting scar formation in the wound healing process, promoting regeneration of skin appendage organs in the wound healing process and the like.

The invention discloses tea juice treatment equipment, and relates to the technical field of tea juice treatment. The device comprises a separation net provided with a through hole, a cutter head and a dial wheel plate crushing assembly which are coaxially arranged up and down, an adjustable magnetic coupling driving part composed of an electromagnet and a planetary gear, a bidirectional flow centrifugal separation chamber, a filter element fine filtration cavity and a non-stop screw deslagging mechanism. Flushing wastewater is actively pre-crushed and then tangentially guided to a centrifugal cavity, and solid and liquid are rapidly separated under the synergistic effect of centrifugal force and suction pressure difference; a liquid phase is subjected to center suction, refined filtration, clarification and discharge, and a solid phase settles along the inner wall and is automatically conveyed to the outside for sealed collection. According to the system, the rotating speed is adjusted in a closed-loop mode through online particle monitoring, load self-adaption and low-energy-consumption operation are achieved, filter screen blockage, shutdown cleaning and peculiar smell diffusion are avoided, and the system is suitable for on-site up-to-standard treatment of tea residue sewage in the peak period of a catering store.

The invention relates to the technical field of biology, in particular to a method for preparing a high-activity small-molecule cartilage extract from animal cartilage tissue, the cartilage extract and application of the cartilage extract, and the method for preparing the high-activity small-molecule cartilage extract from the animal cartilage tissue comprises the following steps: S1, soaking; s2, bone breaking; s3, removing cartilage fat by adopting a skimming and centrifugal separation process; s4, enzymolysis: performing compound shearing on compound protease to obtain enzymatic hydrolysate; s5, filtering; and S6, freeze drying. Through the application of various new technologies, the content of type II collagen in the prepared cartilage extract reaches 65% or above, the content of GAGS reaches 30% or above, the content of hyaluronic acid reaches 17% or above, and the problem that in the prior art, biological activity is damaged due to the processes of degreasing through a chemical degreasing agent, physical high temperature, chemical degradation and high-temperature drying is solved; the biological activity of the natural extract is completely reserved by adopting a physical degreasing and multi-enzyme multi-level directional composite enzymolysis technology and a freeze-drying technology at the temperature of minus 40 DEG C or below.

The invention discloses a rare earth boride nano material as well as a preparation method and application thereof. The phase state of the rare earth boride nano material is REB6 or REB4; the preparation method comprises the following steps: S1, respectively weighing a compound raw material containing an RE element and a compound raw material containing a B element; s2, adding an additive, and fully grinding; s3, reacting under the protection of inert gas; s4, after the reaction is finished, excessive methanol is added, centrifugal separation is performed after no bubbles emerge, and a precipitate A is reserved; s5, adding diluted hydrochloric acid for soaking, and performing centrifugal separation again to reserve a precipitate B; and S6, washing the precipitate B with deionized water, and drying to obtain the rare earth boride nano material. According to the preparation method disclosed by the invention, a normal-pressure and low-temperature preparation method is adopted, the pure-phase rare earth hexaboride nanocrystal can be obtained at normal pressure and the temperature as low as 300 DEG C, and no active metal elementary substance needs to be introduced in the preparation process.

The invention discloses application of polygonatum kingianum polysaccharide in preparation of medicine for treating ulcerative colitis, and relates to the field of biomedicine.The preparation method of the polygonatum kingianum polysaccharide comprises the following steps that S1, polygonatum kingianum roots are taken, smashed and then screened, and polygonatum kingianum powder is prepared; s2, the polygonatum kingianum powder obtained in the step S1 is soaked in an ethanol solution, and polygonatum kingianum powder residues are obtained; s3, performing water extraction on the polygonatum kingianum powder residues obtained in the step S2 to obtain an extracting solution; s4, concentrating the extracting solution obtained in the step S3, adding ethanol into the concentrated solution to precipitate polysaccharide, and centrifugally separating to obtain crude polysaccharide; the polygonatum kingianum polysaccharide disclosed by the invention is high in purity, the effectiveness of the polygonatum kingianum polysaccharide in treatment of ulcerative colitis is verified, and a new solution is provided for relieving the problem of shortage of current colitis treatment medicines.

The invention relates to the technical field of green manufacturing, in particular to a manufactured cutting fluid recovery treatment method based on an oil-scrap separation system, which comprises the following steps: step 1, dynamic viscosity regulation and control pretreatment; 2, gradient centrifugal separation, wherein the pretreated mixed liquid is subjected to three-stage centrifugal separation; 3, interface adsorption fine treatment is conducted, specifically, the oil liquid obtained after centrifugal separation flows through a layered variable-porosity adsorption tower, and regeneration of an adsorption material is triggered according to the pressure drop change; and step 4, optimizing closed-loop parameters, and dynamically correcting the control parameter thresholds in the steps 1-3 by collecting and processing the associated data of the process parameters and the final oil metal residual quantity. According to the method, through precise matching and dynamic adjustment of multiple steps, the separation effect can be improved to the maximum extent in the green manufacturing and cutting fluid recycling process, waste emission and resource waste are reduced, and the purposes of energy conservation and emission reduction are achieved.

The invention relates to the technical field of preparation of lithium battery materials, and discloses a synthesis method of a low-cost battery-grade lithium dihydrogen phosphate raw material lithium phosphate. The synthesis method comprises the following steps: dissolving crude lithium sulfate in alkaline lithium phosphate lithium precipitation mother liquor; carrying out chemical precipitation on the filtered lithium sulfate solution to preliminarily remove calcium, and subsequently, deeply removing calcium and COD (Chemical Oxygen Demand) by sequentially using activated carbon and calcium removal resin to obtain a lithium sulfate finished solution; mixing the lithium sulfate completion liquid and the alkali liquid, freezing to-10 DEG C to-3 DEG C, and performing centrifugal separation to obtain a lithium sulfate freezing liquid; and reacting the refrigerating fluid with a dilute phosphoric acid solution to precipitate lithium phosphate, stirring, washing and centrifuging the filtered crude product lithium phosphate, and drying to obtain the battery-grade lithium dihydrogen phosphate raw material lithium phosphate. The lithium phosphate prepared at low cost is used for replacing battery-grade lithium carbonate, lithium hydroxide and the like as a lithium source for producing the lithium dihydrogen phosphate, so that the production cost of the battery-grade lithium dihydrogen phosphate can be effectively reduced, the lithium phosphate mother liquor is recycled, and the problem of treating a large amount of wastewater caused by other methods is solved.

The invention discloses a high-entropy layered double hydroxide with a strong strain effect and a preparation method of the high-entropy layered double hydroxide. The preparation method comprises the following steps: firstly, preparing ferric salt, cobalt salt, nickel salt, copper salt and zinc salt into a mixed aqueous solution of five metal salts; preparing sodium hydroxide and sodium carbonate into an alkali source aqueous solution; then mixing and stirring the mixed aqueous solution of the five metal salts and the alkali source aqueous solution to gradually form yellowish-brown precipitates, then transferring the yellowish-brown precipitates into a polytetrafluoroethylene reaction kettle, and further reacting in a drying oven; and finally, carrying out centrifugal separation, deionized water and absolute ethyl alcohol washing and freeze drying on the fully reacted precipitate to obtain brown powdery solid, namely the high-entropy layered double hydroxide. The high-entropy layered double hydroxide can be used for advanced oxidation catalytic degradation of tetracycline antibiotic wastewater, the strong strain effect of the high-entropy layered double hydroxide enhances the benefit of activating peroxymonosulfate to generate active free radicals, the efficiency of degrading water pollutants is improved, and the high-entropy layered double hydroxide has good application prospects.

The invention discloses a plant-source nutritional supplement based on glycoside compounds and a preparation method thereof, and relates to the technical field of preparation of plant-source nutritional supplements.The preparation method comprises the steps that raw materials are prepared; the preparation method comprises the following steps: respectively carrying out ultrasonic-assisted extraction on flavonoid glycoside, saponin and geniposide raw materials to obtain an extracting solution; carrying out centrifugal separation on the extracting solution, taking supernate, and then purifying by adopting a macroporous resin adsorption method to obtain a purified glycoside compound solution; mixing the purified glycoside compound solution with lycium barbarum polysaccharide, Chinese yam starch, vitamin E and other auxiliaries in proportion, and uniformly stirring to form a mixed solution; carrying out spray drying on the mixed solution to obtain a powdery nutritional supplement; and screening the powdery nutritional supplement. The high-purity plant source glycoside compound and the functional auxiliary agent are scientifically compounded, and ultrasonic extraction, resin purification and precise process control are combined, so that the integrated improvement of activity synergy, quality stability and personalized scene adaptation of the nutritional supplement is realized.

The invention discloses a method for chemically-assisted pyrolysis recovery of carbon fibers in a thermosetting composite material and full-quantitative reutilization of products, which comprises the following steps: firstly, cutting and sorting a retired wind power blade thermosetting composite material to obtain blade blocks, then treating the blade blocks by using a pretreating agent, and then recovering the pretreating agent to obtain the carbon fibers in the thermosetting composite material. And performing low-temperature pyrolysis on the blade blocks treated by the pretreatment agent by using a swelling agent, recycling the regenerated carbon fibers, and finally recycling the swelling agent and a resin degradation product. According to the method, high-efficiency thermally induced separation of the carbon fibers and the matrix resin is realized, and the used citric acid reagent is efficiently recycled by deeply researching the chemical characteristics of a degradation product and a pretreatment agent. According to the method, centrifugal separation and reduced pressure distillation technologies are combined, the swelling agent is separated out, the resin polymer is degraded, and full-quantitative recovery of solid-phase and liquid-phase products in the process is achieved. And the recovered reagent is directly used for the next round of material degradation treatment, so that the reagent consumption and the treatment cost are greatly reduced, meanwhile, the environmental pollution risk is reduced, and a recovery closed loop is realized.

The invention relates to an iron-based phosphate sodium ion positive electrode material and a preparation method and application thereof, and the preparation method comprises the following steps: respectively dissolving an iron source containing a + 2 valence state and a + 3 valence state and a sodium-containing phosphorus source in deionized water, uniformly mixing, reacting, centrifuging and drying to obtain a powder precursor; the preparation method comprises the following steps: mechanically mixing a precursor, a sodium source, a carbon source, a doping agent and a solvent by adopting ball milling or sand milling, then separating out solid particles by utilizing centrifugation, and carrying out vacuum drying on the obtained solid; and calcining and sintering in an inert atmosphere or a hydrogen-argon mixed atmosphere, and naturally cooling to room temperature to obtain the iron-based phosphate sodium ion positive electrode material. Compared with the prior art, the method has the advantages that the raw material utilization rate is high, the reaction ignition loss rate can be as low as 3.16%, meanwhile, reactants in the method are easy to obtain, the synthesis process is environment-friendly, safe and low in cost, the product impurity content is low and stable, and the obtained material shows excellent electrochemical performance when applied to the sodium ion battery and can be used for industrial production.

The invention discloses a blood component separation system and a control method, and belongs to the field of blood separation.The system comprises a centrifugal device, a blood supply pipeline, an air detector valve and a blood pump, a liquid outlet of the centrifugal device is connected with a separation pipeline, and the separation pipeline is sequentially connected with a first plasma bag and a second plasma bag; a centrifugal pressure sensor, a centrifugal high-speed camera and a red blood cell sensor; and the control center comprises a data acquisition module, a data analysis module and a centrifugal control module. The control method comprises steps S1 to S4. Dynamic intelligent regulation and control and automatic control of the blood component centrifugal separation system are achieved, the centrifugal effect is optimized through the image recognition technology, the image recognition technology is superior to the photoelectric recognition technology in the prior art, excessive centrifugation is avoided, meanwhile, the centrifugal quality is guaranteed, and the quality and activity of separated blood components are effectively guaranteed.

The present disclosure provides processes for removing hydrocarbons, oil coated solids, and suspended solids from a separated water stream produced from a produced water source. In particular, the methods comprise subjecting the separated water stream to a centrifugal separation followed by filtration.

The invention provides a dirty oil sludge treatment method and skid-mounted dirty oil sludge treatment equipment, the method comprises treatment of dirty oil, aged oil, oily sludge and the like, and the main steps are as follows: short-time demulsification is performed through special equipment, and then primary and secondary centrifugal separation is performed to separate water, solid residues and other impurities in the dirty oil sludge, so that the dirty oil sludge is treated. And reduction and recycling of the oil sludge are realized. According to the skid-mounted dirty oil sludge treatment equipment, dirty oil sludge is pumped to a filter to remove large-particle-size impurities, then the dirty oil sludge enters a preheater to be heated, and the heated dirty oil enters a core treatment unit to be subjected to high-energy physical nucleation demulsification; feeding the demulsified sump oil into a horizontal screw centrifuge for solid-liquid separation, and bagging the separated solid residues or feeding the separated solid residues into a sludge drying pry; feeding a separated liquid phase into a three-phase disc centrifuge, carrying out oil-water separation, conveying separated oil out for refining, and conveying separated water out to a sewage treatment plant. And finally, physical and chemical inspection of an oil-phase, water-phase and solid-phase product is inspected, and operation parameters and the technological process are adjusted.

The invention provides a method for catalytically converting waste PET (Polyethylene Terephthalate) plastic into 1, 4-cyclohexanedimethanol by a two-step method, which comprises the following steps of: 1, hydrogenating the waste PET plastic dispersed in methanol under the action of a nickel-based catalyst to obtain dimethyl 1, 4-cyclohexane dicarboxylate; and 2, centrifugally separating the catalyst and the reaction liquid in the step 1, and hydrogenating the reaction liquid under the action of a CuMgAl catalyst to obtain the target product 1, 4-cyclohexanedimethanol. The 1, 4-cyclohexanedimethanol is a key raw material for producing high-end polyester, and has very high market requirements. Under the optimal reaction condition, the molar yield of the 1, 4-cyclohexanedimethanol can reach 83.8%, and the separation purity reaches up to 99.5%. According to the method, upgrading and recycling of the PET waste are achieved so as to cope with the threat of white pollution to the ecological environment and human health.

The present invention discloses an injectable human collagen soft tissue filling material and a preparation method thereof, belonging to the technical field of biomedical materials. The injectable human collagen soft tissue filling material comprises pretreated recombinant human collagen and an osmotic pressure regulator, and the injectable human collagen soft tissue filling material is in an isotonic state; the pretreatment of the recombinant human collagen is processed by isoelectric precipitation and centrifugal separation process; the preparation method thereof comprises filtering and sterilizing the raw materials, pretreatment, and homogenizing the pretreated recombinant human collagen and the osmotic pressure regulator. The injectable human collagen soft tissue filling material of the present invention is mainly human collagen, has a large molecular weight and a triple helix structure, and has a uniform particle size distribution, which can play a filling and supporting effect; the preparation process thereof is simple and convenient, without special processing technology, and will not introduce toxic and harmful residual substances, so that the product performance is stable.

The invention relates to the technical field of zinc glycinate production, and provides a zinc glycinate chelate preparation method, which comprises: (1) pre-mixing glycine and nano zinc oxide, adding into water, and carrying out microwave treatment and ultrasonic-assisted synergistic treatment to prepare a glycine suspension; (2) adding L-ascorbic acid, stirring, maintaining the temperature at 58-62 DEG C for 30-40 minutes, heating to 74-80 DEG C, and maintaining the temperature at 74-80 DEG C for 2-3 hours; and (3) cooling to room temperature, standing, centrifugally separating, and drying to obtain the zinc glycinate chelate. According to the preparation method of the glycine zinc chelate, the production cost is effectively reduced and the production efficiency is improved under the condition that the purity and the stability of the product are ensured.

To provide an improved system and method for balancing a centrifuge rotor.SOLUTION: A hub assembly 10 for a centrifuge rotor 12 includes a rotor hub 14 including a head portion 20, an elongated shaft portion 22 extending axially away from the head portion 20, and a central bore 102 extending through the head and shaft portions 20, 22. A system and method for balancing a centrifuge rotor 12 in which a head 20 includes a plurality of balance holes 52 each configured to selectively receive at least one balance weight 16 for balancing the centrifuge rotor 12.SELECTED DRAWING: Figure 4

The invention provides an immunodetection method of a multi-index immune checkpoint detection kit, which belongs to the technical field of immunodetection and comprises three main stages of sample preparation, immune reaction and data analysis. The method comprises the following steps: firstly, carrying out centrifugal separation to obtain a plasma sample, and preparing a fluorescent microsphere coupled capture antibody and biotin labeled detection antibody compound; then carrying out immune reaction, forming a sandwich type immune complex through specific binding, and adding streptavidin marked by phycoerythrin for signal amplification. Detecting a fluorescence signal by adopting a flow cytometer to obtain an original data matrix; a contribution feature vector, a utility feature vector and an expression feature matrix are extracted through a feature decomposition algorithm, and a deep learning model of a total-score-total structure is established for data analysis. Finally, a detection report containing a quantitative result, an importance score and reliability evaluation is generated, and the technical problem that in the prior art, the analysis accuracy of a multi-index immune checkpoint detection result is insufficient is solved.

The invention discloses a metal particle Ni supported catalyst based on fly ash. The preparation method comprises the following steps: firstly, carrying out alkali fusion on fly ash to prepare powder; dissolving the powder and Ni (NO3) 2.6 H2O in a mixed solution of distilled water and absolute ethyl alcohol, adding polyethylene glycol, and performing ultrasonic stirring to obtain uniform dispersion liquid; and finally, continuously performing ultrasonic stirring on the dispersion liquid, performing hydrothermal reaction, cooling, performing centrifugal separation, drying, calcining, cooling and grinding to obtain the catalyst. The coal ash derivative zeolite is adopted as a carrier of the catalyst, Ni is loaded on the carrier to improve the specific surface and effective active sites of the carrier, the effective catalytic specific surface area of the catalyst is effectively improved, and the catalytic activity is improved, so that a stable and safe catalyst material for preparing methane through CO2 hydrogenation with high activity and selectivity is obtained; the space time yield of methane is high.