1244 results about "Phytic acid" patented technology

The invention discloses a composite electrode material for removing uranium through photoelectrocatalysis and a preparation method and application of the composite electrode material, and belongs to the technical field of catalytic materials and wastewater treatment.The preparation method of the composite electrode material comprises the following steps that a ZIF-8 material, copper salt and ferric salt are mixed, and a first metal composite material is prepared; reacting the first metal composite material with a KOH solution to prepare a second metal composite material; carrying out carbonization treatment on the second metal composite material, and then carrying out acid treatment by using acid to obtain a bimetallic atom catalytic material; the preparation method comprises the following steps: dispersing a bimetallic atom catalytic material and a g-C3N4 material in a mixed solution containing phytic acid and a Nafion solution to obtain catalyst ink; and coating the catalyst ink on a substrate, and carrying out illumination drying to obtain the composite electrode material. According to the composite electrode material, under the synergistic effect of the bimetallic single atomic cluster catalyst and g-C3N4, respective advantages are fully exerted, and efficient deposition removal of uranium is achieved.

The invention provides a green and efficient petroleum passivator and a preparation method thereof, and belongs to the technical field of passivators. Carboxymethyl chitosan, phytic acid and beta-cyclodextrin are coupled to prepare a chitosan-phytic acid-cyclodextrin compound, bismuth, lanthanum, cerium and aluminum are compounded, and the green and efficient petroleum passivator is prepared through tannic acid polymerization modification. The prepared green and efficient petroleum passivator is green, safe, non-toxic and efficient, has good capturing and passivating capacity on ions such as iron, nickel and vanadium, greatly improves the activity of a catalyst, prolongs the service life of the catalyst, and has wide application prospects.

The invention discloses a glass fiber reinforced epoxy resin composite material and a preparation method thereof, and relates to the technical field of composite materials, and the preparation method comprises the following steps: carrying out organic solvent immersion treatment, cleaning and drying on glass fibers to obtain pretreated glass fibers; respectively carrying out phytic acid modification treatment on the pretreated glass fibers and hollow alumina microspheres; performing plasma surface treatment on the glass fibers and the hollow aluminum oxide microspheres subjected to the phytic acid modification treatment; mixing and dispersing epoxy resin, a curing agent, the glass fibers subjected to plasma surface treatment and the hollow aluminum oxide microspheres according to a preset mass ratio; carrying out vacuum degassing on the mixture; and injecting the degassed mixture into a mold for step-by-step curing. The preparation method has the beneficial effects that active groups are introduced to the surfaces of the glass fibers through phytic acid treatment, the number of the active groups is further increased by combining plasma surface treatment, and the interface bonding capacity of the glass fibers and an epoxy resin matrix is remarkably improved.

The invention provides a polyurethane material for leaking stoppage of coal mine spraying and a preparation method thereof, and belongs to the technical field of polyurethane. The preparation method comprises the following steps: pretreating a multi-walled carbon nanotube, coupling phytic acid and a silane coupling agent, reacting with UiO-66-NH2, coating the surface with a graphene oxide layer, mixing with polyether polyol, a catalyst and an antistatic agent, adding into water, adding a foaming agent and silicone oil, heating, stirring and mixing, transferring into a mold, adding diisocyanate, and after foaming is completed and the temperature of the material is reduced to room temperature, carrying out extrusion molding to obtain the composite material. And drying, heating and curing to obtain the polyurethane material for coal mine spraying air leakage stoppage. By adding the prepared wrinkled graphene oxide coated UiO-66-NH2 / modified multi-walled carbon nanotubes, the mechanical property and strength of the prepared polyurethane material for coal mine spraying air leakage stoppage can be obviously improved, the flame retardant property such as the oxygen index of the material is also obviously improved, the foam expansion is improved to a certain extent, the preparation method is simple, and the preparation method is suitable for industrial production. The flame-retardant and mechanical properties can be obviously improved, and the application prospect is wide.

The invention belongs to the field of flame-retardant finishing of textiles, and discloses a phytic acid-based flame retardant and a preparation method of a flame-retardant cotton fabric. Natural phytic acid, polyethylene glycol, melamine and metal salt are used as main raw materials, the environment-friendly characteristic of a biomass material is combined, an efficient and environment-friendly flame retardant is prepared, the prepared flame retardant is arranged on a cotton fabric through a traditional impregnation method, and the flame retardance and smoke suppression performance of the arranged cotton fabric are greatly improved. The method not only has a good flame retardant effect, but also avoids potential hazards of a traditional flame retardant to the environment and human health, and has a wide application prospect. The flame-retardant cotton fabric can be widely applied to the fields of household textiles, protective clothing, fire-fighting equipment and the like, and has remarkable economic benefits and social benefits. The invention not only provides an efficient and environment-friendly flame retardant preparation method, but also opens up a new way for application of biomass materials in the field of flame retardance, and has important scientific significance and practical value.

The invention belongs to the technical field of insulating flame-retardant adhesive tapes, and particularly relates to an insulating flame-retardant adhesive tape and a preparation method thereof. According to the invention, phytic acid reacts with 3-amino-5-methylpyrazole, triaminopyrimidine and polyether amine-2000 to prepare a flame-retardant auxiliary agent, and the flame-retardant auxiliary agent is compounded with magnesium hydroxide, zinc borate and melamine to prepare a modified flame retardant which can generate an expansive carbon layer during combustion to block heat and isolate oxygen so as to achieve a flame-retardant effect; an aluminum oxide layer generated on the artificial diamond micro-powder is used as an insulating heat-conducting aid, so that the insulativity, wear resistance and corrosion resistance of the insulating flame-retardant adhesive tape are improved, the adhesive tape can be assisted in uniform heat conduction, and combustion caused by over-high local temperature is prevented; epoxy resin is used for wrapping the uniformly dispersed insulating heat-conducting auxiliary agent, and anisyl and boron nitride ceramic powder are cured to prepare an insulating material, so that the dielectric breakdown performance of the adhesive tape is enhanced. The insulating flame-retardant adhesive tape prepared by the invention is excellent in insulativity and flame retardance and free of halogen flame retardants, and the production process is environment-friendly.

The invention relates to the field of packaging materials, and discloses low-temperature heat-sealing water-based coated paper and a preparation method and application thereof.The water-based coated paper comprises a base paper layer and a water-based coating, and the water-based coating comprises water-based ethylene-acrylic acid copolymer emulsion, modified nano-silica, a coalescing agent and water; a cardanol derivative is introduced into the water-based ethylene-acrylic acid copolymer emulsion as a functional component; the cardanol derivative is prepared by reacting epoxidized cardanol with 9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide and then grafting with acryloyl chloride. The preparation method comprises the following steps: reacting epoxidized cardanol with 9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide; the modified nano silicon dioxide is prepared by mixing aminated nano silicon dioxide and chitosan and adding a cross-linking agent prepared by grafting phytic acid and ethylene glycol diglycidyl ether. The water-based coating paper prepared by the invention overcomes the defects that the existing BOPP film is not environment-friendly, and the conventional coating paper is high in heat sealing temperature and easy to stick; meanwhile, good mechanical properties, water resistance and flame retardance are achieved.

The invention belongs to the technical field of flame-retardant polyether polyol, and particularly relates to a preparation method and application of multi-element synergistic reaction type anti-dripping flame-retardant polyether polyol. The preparation method of the multi-element synergistic reaction type anti-dripping flame-retardant polyether polyol comprises the following steps: taking phosphorus-containing polyether polyol and a nitrogen-containing compound as composite initiators, and carrying out polymerization reaction on the phosphorus-containing polyether polyol and the nitrogen-containing compound and an epoxy compound under the self-catalysis action to obtain the reaction type anti-dripping flame-retardant polyether polyol. According to the preparation method of the multi-element synergistic reaction type anti-dripping flame-retardant polyether polyol provided by the invention, phosphorus, nitrogen and chlorine elements are embedded into the polyether polyol by constructing a ternary synergistic system, so that the problems of poor compatibility, migration and precipitation of an externally added flame-retardant system are solved; in the preparation process, low-cost bio-based phytic acid is adopted as a raw material, no catalyst needs to be introduced, the operation is simple, the prepared polyether polyol is used for preparing a waterborne polyurethane film, the flame-retardant characteristic of the material is improved, and meanwhile, the good anti-dripping characteristic is achieved.

The invention relates to the field of cosmetics, in particular to sea rice fermentation filtrate, a preparation method thereof and a whitening cosmetic. Inoculating the first fermentation seed solution and the second fermentation seed solution into a fermentation culture medium, fermenting at 25-30 DEG C to obtain a fermentation product, and removing thalli in the fermentation product; the fermentation culture medium is prepared from the following components in percentage by mass: 5 to 10 percent of sea rice powder, 1 to 5 percent of saccharides and the balance of water; the pH value of the fermentation culture medium is 4-5; the first fermentation seed solution is a saccharomyces cerevisiae strain fermentation seed solution; the second fermentation seed solution is a lactobacillus plantarum strain fermentation seed solution. The method can promote the growth of saccharomyces cerevisiae and lactobacillus plantarum while promoting the release of an active component phytic acid in the sea rice, and has a remarkable effect of removing excessive free radicals and inhibiting the activity of related enzymes for synthesizing melanin; therefore, the whitening effect of the cosmetic can be effectively improved.

The invention discloses a preparation method and application of phytic acid modified zero-valent iron. The method comprises the following steps: (1) mixing phytate and liquid phytic acid according to a molar ratio of (5: 5)-(8: 2), and preparing a buffer solution with the concentration of 0.05-0.5 mol / L; (2) adding micron or nano zero-valent iron into a buffer solution according to a solid-to-liquid ratio of 1: 10 to 1: 50 (g / mL), and transferring to a polytetrafluoroethylene reaction kettle; (3) under the protection of nitrogen, reacting for 6-48 hours under the conditions that the temperature is 20-80 DEG C and the oscillation rate is 100-1000 rpm, and controlling the pH value to be 3.5-5.5; and (4) after the reaction, carrying out suction filtration, ethanol-water alternate washing and vacuum drying to prepare the modified zero-valent iron with the surface coated with the phytic acid iron complex. A stable chelation layer is formed on the surface of phytic acid molecules and zero-valent iron, the oxidation resistance, dispersity and heavy metal adsorption capacity of the material are remarkably improved, and the material is suitable for efficient repair of industrial wastewater.

The invention discloses a woven suede fabric and a preparation process thereof, and relates to the technical field of fabrics. According to the preparation method, the base cloth is subjected to dipping treatment by using the dipping liquid, so that the woven suede fabric with excellent flame retardance is prepared. A modified metal organic framework material is added into an impregnation liquid, the metal organic framework material has excellent thermal stability, 2-methylimidazole and zinc nitrate are used as raw materials, hexachlorocyclotriphosphazene with a good flame-retardant effect is packaged into the metal organic framework material, and the flame-retardant performance of the material is improved. The flame-retardant effect of the metal organic framework material is further enhanced, so that the flame-retardant property of the woven suede fabric is improved. The metal organic framework material is treated by using phytic acid, then copper sulfate pentahydrate is added, more metal ions can be chelated through the chelating performance of phytic acid on the metal ions, the catalytic carbonization effect is achieved, and therefore the flame retardant property of the woven suede fabric is improved.

The invention relates to the technical field of collagen peptide extraction, and particularly discloses aquatic collagen tripeptide and a processing technology thereof, and the processing technology comprises the following steps: step S1, fish skin pretreatment; step S2, performing enzymolysis; step S3, fermentation; step S4, separation and purification; starting from three aspects, firstly, a modified degreasing agent is added in the degreasing treatment process, the modified degreasing agent takes 1-ethyl-3-methylimidazole acetate, zinc phytate and calcium citrate as main components according to a specific mass ratio, and secondly, gel emulsion is added in the enzymolysis process, so that the modified degreasing agent is prepared. The gel emulsion has an oil gel structure, grape seed oil and sodium lignin sulfonate, and 3, a composite strain is added in the fermentation process, the composite strain is prepared by mixing bacillus natto and lactobacillus plantarum according to a specific proportion, and the purity and the extraction rate of the aquatic collagen tripeptide are improved through the synergistic effect of all the procedures.

The invention discloses weather-resistant water-based two-component epoxy paint and a preparation method thereof, and belongs to the technical field of paint. The weather-resistant water-based two-component epoxy paint comprises a component A and a component B, the component A comprises 50-70 parts by mass of a modified waterborne epoxy emulsion, 3-6 parts by mass of a pigment, 7-13 parts by mass of a modified filler, 0.3-1.5 parts by mass of a wetting dispersant, 2-4 parts by mass of a coalescing agent, 0.1-0.5 part by mass of a defoaming agent, 0.5-5 parts by mass of water and 0.5-1 part by mass of a leveling agent; the component B comprises 35-65 parts by mass of a modified curing agent, 10-20 parts by mass of ethanol and 30-40 parts by mass of water; the component A and the component B are mixed according to the mass ratio of 100: (20-30); the modified curing agent is obtained by reacting polyethylene glycol diglycidyl ether, epoxy resin, triethylene tetramine, functional organic silicon and phenyl glycidyl ether; the modified filler is obtained by modifying nano silicon dioxide with poly (m-xylylenediamine) and a silane coupling agent KH560; the modified water-based epoxy emulsion is a phytic acid modified water-based epoxy emulsion.

The invention relates to a natural antioxidant for prefabricated vegetables and a preparation method of the natural antioxidant, and belongs to the technical field of food additives. The antioxidant is prepared from rosmarinic acid, carnosic acid, drug-loaded cellulose and double-phase chelating microspheres; the drug-loaded cellulose is prepared by modifying cellulose with quercetin, loading anthocyanin and then wrapping with a trehalose-gamma-polyglutamic acid composite film; the biphase chelating microspheres are phytic acid-citric acid biphase sustained-release microspheres formed by wrapping phytic acid and citric acid with a chitosan and sodium alginate composite film. Through multi-component functional complementation, multi-stage slow release design and physical-chemical synergistic barrier, comprehensive inhibition of the oxidation problem of the prefabricated vegetable is realized, a'free radical scavenging-metal chelating-phase interface stabilization 'triple protection system is constructed, accurate oxidation resistance in different stages of processing, storage and transportation is realized, and the prepared vegetable has good market prospects. The bottlenecks of short action period and single protection dimension of a natural antioxidant are broken through.

The invention relates to the technical field of aerogel, in particular to flexible flame-retardant aerogel and a preparation method thereof.The flexible flame-retardant aerogel is prepared from modified graphene, modified polyvinyl alcohol, silver nanowires, phytic acid and epoxy resin E-51; the furan group is introduced into the aerogel through the modified graphene, the furan group and the maleimide group are subjected to a D-A reaction, an adhesive is prevented from being used when the aerogel is bonded with a screen backboard, the D-A reaction is reversible, and lossless reworking can be realized. PVA and epoxy resin E-51 are added together, so that the heat resistance and mechanical strength of the material are improved. PVA is grafted with a large-steric-hindrance amine group, weak interaction with a furan group is generated, side reaction with an epoxy group of epoxy resin E-51 is avoided, and when aerogel is bonded to an OLED screen backboard, the protective layer is reversibly released, so that D-A reaction can be smoothly carried out. The hydrophobic treatment of the modified graphene and the modified grafting of the polyethylene to the mPEG can effectively improve the agglomeration of the modified graphene and ensure the uniform dispersion of the modified graphene.

The invention provides tartary buckwheat herbal baijiu and a preparation method thereof.The method aims at solving the problems that existing tartary buckwheat baijiu is lost in active ingredient, single in flavor and unstable in baijiu body, firstly, tartary buckwheat submicron powder, radix puerariae submicron powder and rhizoma polygonati submicron powder are put into Maotai-flavor base liquor together, and two-section type closed extraction is conducted at the normal temperature and then at the low temperature, adding a part of citric acid solution to adjust the pH at the initial stage of extraction; squeezing and filtering extract liquor, immediately adding bamboo leaf extract and phytic acid to carry out synergistic anti-oxidation treatment, and carrying out short-term aging; and finally, blending with the residual base wine. According to the preparation method disclosed by the invention, the retention rate of active ingredients such as tartary buckwheat flavone and the stability of the wine body are remarkably improved through staged extraction and dual antioxidant protection, the wine body is successfully endowed with coordinated baking fragrance, sauce fragrance and herbal flavor, and the taste is mellow and mild.

The invention relates to the field of coatings, and discloses a biomass-based oil-resistant coating and a preparation method thereof, the coating comprises an additive solution, a paraffin solution and gallic acid; the paraffin solution is obtained by dissolving paraffin in absolute ethyl alcohol; a preparation method of the additive solution comprises the following steps: mixing chitosan powder and an acetic acid aqueous solution to prepare a chitosan solution, ultrasonically dispersing functionalized montmorillonite in deionized water to prepare a suspension, then uniformly mixing the chitosan solution and the suspension, adding modified phytic acid prepared by grafting phytic acid and ethylene glycol diglycidyl ether, and stirring to react; the functional montmorillonite is prepared by modifying modified montmorillonite with titanium dioxide and zinc oxide, then activating the modified montmorillonite with 3-aminopropyltriethoxysilane and succinic anhydride, and then carrying out a ring-opening reaction with glycidyl neodecanoate. The coating prepared by the invention has high water resistance, the Kit oil-proof grade is kept at grade 12, and the oil-proof performance of the coating is greatly improved. Meanwhile, the antibacterial performance, the tensile index and the ultraviolet aging resistance are relatively high.

The invention relates to the technical field of waterproof coiled materials, and discloses a flame-retardant waterproof coiled material and a preparation method thereof.The flame-retardant waterproof coiled material is prepared from, by weight, 100 parts of thermoplastic polyolefin elastomer, 20-40 parts of modified flame retardant, 5-18 parts of fiber filler, 0-3 parts of lubricant, 0-3 parts of antioxidant, 0-3 parts of stabilizer and 0-15 parts of pigment; the modified flame retardant takes MOF, hexagonal boron nitride and phytic acid as an inner core, and polysiloxane is cross-linked and polymerized on the surface of the inner core. According to the flame-retardant waterproof coiled material provided by the invention, if the MOF or the modified MOF material is independently added into the resin material, the problem of poor compatibility of the MOF or the modified MOF material and the resin system cannot be avoided. According to the invention, a microcapsule technology is creatively utilized to polymerize polysiloxane on the surface of the MOF material, so that not only can the problem of dispersion of the MOF material be effectively solved, but also the compatibility of polysiloxane and the flame-retardant characteristic of organic silicon are utilized to promote formation of carbon at high temperature by utilizing phosphorus, and the thermal stability of a carbon layer is improved by utilizing silicon; therefore, the purpose of synergistic flame retardance is achieved.

The invention discloses a preparation method of flame-retardant fire early-warning bacterial cellulose aerogel fibers, and belongs to the technical field of materials. According to the preparation method, bacterial cellulose is taken as a core raw material, then a phytic acid-polypyrrole conductive network is constructed in the fiber through a solvent replacement effect, and a ZnO-MXene sensing material with high flame sensitivity is further covered on the surface, so that the flame-retardant bacterial cellulose aerogel fiber with excellent flame retardance and high flame sensitivity is prepared. The preparation method is simple, convenient and efficient, resource recycling is effectively promoted, and the prepared flame-retardant fire early-warning bacterial cellulose aerogel fiber has wide application prospects in the fields of vehicle interiors, clothes and furniture.

The invention discloses a flame-retardant thermoplastic polyurethane elastomer material and a preparation method thereof, and belongs to the technical field of modified nano materials. The preparation method comprises the following steps: dissolving melamine, phytic acid and boron nitride in deionized water, carrying out oil bath, adding a coupling agent, stirring, carrying out vacuum filtration, washing with water, and drying to obtain a layered nano flame retardant; the preparation method comprises the following steps: dispersing a flame retardant in deionized water containing a nonionic dispersant, and carrying out ultrasonic treatment; the preparation method comprises the following steps: reacting polyether polyol with diisocyanate to obtain a primary prepolymer; adding other auxiliary agents, stirring, and carrying out gradient heating polymerization; and injecting into a mold, curing for 6-12 hours at 105-125 DEG C, and drying for 12-24 hours at 80-90 DEG C. A phosphorus-nitrogen-silicon ternary synergistic flame-retardant system is introduced, the boron nitride nanosheet surface grafting and dynamic pre-polymerization-gradient heating process is optimized, the dispersity is improved, and smoke suppression and thermal stability are achieved. Compared with the prior art, the flame retardant efficiency is high, the mechanical property is excellent, and environmental friendliness is achieved.

The invention relates to the field of fabrics, in particular to a metallic yarn fabric based on a discontinuous aluminum layer and a processing technology thereof.The metallic yarn and polyester fibers are blended to serve as warps, the polyester fibers serve as wefts, the warps and the wefts are interwoven to obtain base cloth, the base cloth is subjected to discontinuous etching in the warp direction through etching liquid, and the pretreated base cloth is obtained; transferring the fabric into antibacterial finishing liquid for padding treatment to prepare the fabric. Modified waterborne polyurethane emulsion containing silicon and nitrogen elements is introduced into finishing liquid, polytetrahydrofuran glycol, hydroxyl-terminated polydimethylsiloxane and isophorone diisocyanate are used as raw materials, 2, 2-bis (hydroxymethyl) propionic acid is used as a hydrophilic chain extender, and cyanuric chloride derivative glycol based on menthol is used as a chain extender; the preparation method comprises the following steps: introducing nano zinc oxide as a finishing agent into a finishing liquid, firstly aminating the nano zinc oxide by using 3-aminopropyltriethoxysilane, then obtaining phytic acid modified nano zinc oxide by using electrostatic and hydrogen-bond interaction, and further grafting cyanuric chloride derivative diol based on menthol.

The invention relates to the field of flame retardants, in particular to a flame retardant synergist and a preparation method thereof. The flame-retardant synergist is prepared from the following raw materials in parts by mass: 20 to 30 parts of hydrotalcite, 5 to 15 parts of sepiolite and 0.5 to 1 part of phytic acid. The preparation method comprises the following steps: 1, mixing phytic acid with water to prepare a phytic acid solution for later use; step 2, hydrotalcite and a phytic acid solution are mixed under the condition of 200-300 r / min; 3, carrying out solid-liquid separation, wherein the solid part is a first product; step 4, mixing the first product, sepiolite and water under the condition of 2500 to 3000r / min; and step 5, carrying out solid-liquid separation, wherein the solid part is the flame-retardant synergist. The environment-friendly flame-retardant synergist provided by the invention is applied to plastics, can effectively improve the mechanical properties of plastic products, and shows excellent flame-retardant and smoke-suppressing effects.

The invention discloses high-toughness low-swelling ionic conductive hydrogel and a preparation method and application thereof, and belongs to the technical field of polymer hydrogel, and the preparation method comprises the following steps: dissolving acrylic acid, acrylamide, phytic acid and sodium carboxymethyl cellulose in deionized water, and uniformly mixing to obtain a precursor solution; removing bubbles in the precursor solution to prepare a bubble-removed precursor solution; adding an initiator and a cross-linking agent into the bubble-removed precursor solution, and stirring until the initiator and the cross-linking agent are completely dissolved to obtain a pre-polymerized solution; and carrying out free radical polymerization on the pre-polymerized solution under a preset condition to obtain the high-toughness and low-swelling ionic conductive hydrogel. Through the synergistic enhancement effect of phytic acid and carboxymethyl cellulose, the multifunctional ionic conductive hydrogel is developed, and the hydrogel has excellent mechanical properties, can realize low swelling in water and artificial seawater, and also has good conductivity. The preparation method is simple, controllable in operation and easy for industrial production.

The invention discloses a multi-network anti-freezing hydrogel electrolyte, a preparation method thereof and application of the multi-network anti-freezing hydrogel electrolyte in an electrochemical device. The hydrogel is prepared by using polyvinyl alcohol (PVA) and polyacrylamide (PAM) to form a basic network skeleton, introducing phytic acid, ethylene glycol and lithium / zinc bimetal salt (Li2SO4 / ZnSO4), and carrying out thermal initiation polymerization and freeze thawing. The hydrogel prepared by the invention has a multiple physical cross-linked network formed by polymer molecular chain entanglement, hydrogen-bond interaction among functional groups and metal coordinate bonds constructed between phosphate groups and divalent metal ions, so that the hydrogel electrolyte has excellent mechanical properties. Due to introduction of ethylene glycol, formation of ice crystals is effectively inhibited, and the hydrogel is endowed with excellent anti-freezing performance; the high-concentration Li < + > and Zn < 2 + > ensure the high ionic conductivity. The supercapacitor assembled by using the hydrogel electrolyte shows relatively high specific capacitance and good capacitance retention rate under bending and freezing conditions, and has good electrochemical properties and safety performance.

The invention relates to the technical field of bacterium enrichment nutrient solutions, in particular to a bacterium enrichment nutrient solution for fermentation and a preparation method of the bacterium enrichment nutrient solution. The culture medium is prepared from the following raw materials in parts by weight: maltodextrin, crystalline glucose, low-pigment yeast extract powder, refined soy peptone, dipotassium phosphate, monopotassium phosphate, magnesium sulfate heptahydrate, sodium chloride, phytic acid, L-ascorbic acid, manganese sulfate monohydrate, biotin, thiamine hydrochloride and choline chloride. Through a double-carbon-source structure, maltodextrin and crystalline glucose cooperate, metabolic oscillation is avoided, and the energy utilization rate is increased; the low-pigment yeast extract powder and the refined soy peptone are complementary, so that the rapid growth requirement of thalli is met; phytic acid is chelated with metal ions to prevent precipitation, L-ascorbic acid is used for resisting oxidation, and biotin and thiamine activate a coenzyme pathway to realize accurate regulation and control of a metabolic network.

The invention discloses a preparation process of crocodile penis peptide wine for improving kidney deficiency, and relates to the technical field of biology, the process comprises the steps of raw material pretreatment, collaborative graded enzymolysis, starter propagation, sand feeding, sand roughening, starter addition and stacking fermentation, distillation for wine taking and fine adjustment. Wherein the synergistic graded enzymolysis adopts a mixed enzymolysis technology, lecithin and phytic acid are added, and natural pH gradient is combined, so that the problems of wine precipitation and taste layering are effectively solved, and the product stability and the polypeptide retention rate are improved. Meanwhile, a traditional Chinese medicinal material compound formula is fused in the process, and the health-care effect is enhanced through the synergistic effect of enzymolysis and fermentation. The wine can significantly increase the content of testosterone in serum and the physical endurance, and improve the symptom of kidney deficiency. The method is mature in process, high in product quality and suitable for large-scale production.

The invention discloses an environment-friendly flame-retardant polyvinyl alcohol film and a preparation method thereof, and relates to the technical field of polyvinyl alcohol films. The polyvinyl alcohol film is prepared from the following components in parts by weight: 90 to 110 parts of polyvinyl alcohol, 0.4 to 1.2 parts of polydopamine modified cellulose nanocrystals, 8 to 15 parts of chitosan / phytic acid / boron nitride composite flame retardant and 0.6 to 0.9 part of plasticizer. The preparation method comprises the following steps: adding polyvinyl alcohol into deionized water, dissolving and mixing to obtain a polyvinyl alcohol aqueous solution, adding glycerol, continuously stirring for 1-2 hours, sequentially adding a chitosan / phytic acid / boron nitride composite flame retardant and polydopamine modified cellulose nanocrystals, and uniformly stirring and mixing at 50-70 DEG C to obtain a blended solution; and carrying out film casting on the blended solution. The limit oxygen index of the film is greater than or equal to 30%, the vertical combustion grade is V-0, the tensile strength is greater than or equal to 40%, the elongation at break is greater than or equal to 140%, and the light transmittance is greater than or equal to 85%.

The embodiment of the invention discloses a Yarrowia guilliermondii as well as a separation and screening method, an identification method and application of the Yarrowia guilliermondii. The preservation number of the Yarrowia guilliermondii is CGMCC (China General Microbiological Culture Collection Center) No.27603, and the preservation number of the Yarrowia guilliermondii is CGMCC No.27603. The Yarrowia guilliermondii disclosed by the embodiment of the invention has a very good prevention and control effect on postharvest diseases of fruits, and the prevention and control effect of the Yarrowia guilliermondii on the diseases can be enhanced by respectively adding auxiliary factors, namely calcium chloride, alginate oligosaccharide (AOS), phytic acid (PA) and metschhia yeast. Through identification, the antagonistic bacterium is a Yeyrozyma guilliermondii, and the antagonistic bacterium is a Yeyrozyma guilliermondii. The M.guilliermonii has a good control effect on gray mold, penicilliosis, black spot and aspergillus niger of strawberry, apple, pear and tomato fruits, can be rapidly colonized on fruit wounds, and can enhance the resistance-related enzyme activity of the fruits, occupy the wound space and induce the fruit resistance to reduce the morbidity of diseases.

The invention discloses a green construction of a porous separation membrane and an efficient uranium separation / enrichment method thereof.The method comprises the steps that firstly, mixed-dimension attapulgite clay acid etching powder is modified through phytic acid and then added into a saponin plant extracting solution, and then the mixture is mixed with a sodium alginate-chitosan double-network matrix; a film-forming solution with a high-mechanical-stability gas-liquid interface is obtained through a Pickering foam template method, and then the porous separation film is controllably constructed through cooperative strategies such as film casting, calcium cross-linking and carboxylation. Based on the advantages of a rod / sheet mixed dimension structure of minerals, synergistic interaction of plant derivatives and a spatial orientation regulation and control synergistic mechanism of functional groups, a porous separation membrane with a specific porous structure, excellent mechanical properties and uranium separation efficiency is constructed in a green manner, and the uranium separation efficiency is improved by combining optimization of membrane layer stacking and elution strategies. A high-efficiency uranium separation / enrichment method is developed, and a new normal form is provided for solving uranium pollution prevention and control and resource recovery and enrichment by a membrane separation technology.

Ammonium dihydrogen phosphate (ADP), phytic acid (PA) and guanazole (GZ) are taken as main raw materials, gamma-aminopropyltriethoxysilane KH550 is taken as a coupling aid, and the KH550 has the effects of improving the interaction force between ADP, PA and GZ and the surface of wood and providing a silicon element to form Si-O with a high-stability structure. The preparation method comprises the following steps: 1, preparing a phytic acid-guanidazole polyelectrolyte solution PG; and 2, preparation of the smoke suppression and flame retardation liquid ADP / KH550 / PG. When being used as a wood flame-retardant liquid, the flame-retardant liquid has flame-retardant property, and passes a UL-94V-0 grade test in a UL-94 grade test; a carbon residue layer formed after combustion is in a large-area continuous compact state; the limit oxygen index is 38.4 + / -1%; the maximum heat release rate is 41.31 + / -2.51 kW / m < 2 >, the total heat release amount is 6.15 + / -0.94 MJ / m < 2 >, the total smoke release amount is 0.26 + / -0.01 m < 2 >, and the fire increase index is 0.31 + / -0.02 kW / m < 2 > / s. And the carbon residue amount at 800 DEG C is 40.96 + / -1 wt.%.