2785results about "Fibre types" patented technology

The invention belongs to the technical field of gel materials, and particularly relates to aerogel powder for polyolefin modification and a preparation method and application thereof. The preparation method of the aerogel powder comprises the following steps: (1) preparing aramid nanofiber dispersion liquid; (2) preparing a polypyrrole coated aramid nanofiber dispersion liquid; (3) mixing polyamide acid and the polypyrrole coated aramid nanofiber dispersion liquid, and then carrying out partial imidization and solvent exchange to prepare hydrogel; and (4) carrying out freeze drying, thermal imidization and crushing to obtain the aerogel powder for polyolefin modification. The aerogel powder is a porous solid material formed by forming one-dimensional composite fibers from aramid nanofibers and polypyrrole and combining the one-dimensional composite fibers with polyimide resin. The aerogel powder and polyolefin resin are compounded to obtain the polyolefin resin composite material with high strength and antistatic property, and the polyolefin resin composite material can be widely applied to the fields of pipes, plates, grouting equipment parts, grouting bags and the like.

The invention belongs to the technical field of fiber materials, and particularly relates to a modified aramid nanofiber as well as a preparation method and application thereof. The preparation method comprises the following steps: (1) preparing an aramid nanofiber dispersion liquid; (2) modifying the aramid nanofiber by using POSS; and (3) carrying out in-situ polymerization on polypyrrole on the surface of the aramid nanofiber. POSS (polyhedral oligomeric silsesquioxane) has a relatively large volume exclusion effect, the template effect of long-chain alkyl quaternary ammonium salt can be influenced by scattered adhesion of POSS on the surface of aramid nanofiber, uneven polymerization of pyrrole monomers is caused, and formation of a rough structure on the surface of the fiber is facilitated. According to the invention, the polypyrrole-coated aramid nanofiber with a coarse structure is used as a polyolefin modified material, so that the problem of low interfacial force existing in a common filler is solved, and the polyolefin resin composite material with high strength and antistatic property is obtained and can be widely applied to the fields of pipes, plates, grouting equipment parts, grouting bags and the like.

The invention relates to a flame-retardant and heat-insulating aerogel composite material as well as a preparation method and application thereof, and belongs to the technical field of novel building materials. The fiber aerogel is prepared through coaxial electrostatic spinning, an injector containing a polymer spinning solution is connected to a skin layer needle tube connecting port, an injector containing air is connected to a core layer needle tube connecting port, coaxial electrostatic spinning is carried out to prepare micron fibers with skin-core structures, the micron fibers fall on a receiving base material, and the micron fibers with the skin-core structures fall on the receiving base material. A hollow fiber aerogel material with a three-dimensional fluffy structure is obtained, in-situ growth of hydrated nano silicate particles is carried out after thermal crosslinking treatment, the nano silicate particles grow along the fiber surface and cover the micron fiber surface of the hollow fiber aerogel material, and the aerogel composite material is obtained. The hydrated nano silicate particle growth solution comprises polyvinyl alcohol, calcium salt, silicate and aluminum salt. The prepared aerogel composite material has excellent flame retardance and heat insulation performance and is suitable for being used as a building material.

The invention discloses a flame-retardant high-temperature-resistant fiber and a preparation method thereof, and relates to the technical field of fibers. When the flame-retardant high-temperature-resistant fiber is prepared, 1, 6-hexamethylenediamine, 1, 6-adipic acid, tetrahydrodifuran [3, 4-B: 3 ', 4'-D] furantetraone and a phosphorus-sulfur composite flame retardant are copolymerized to generate a polyamide-polyamide acid solution; 4-aminopyridine and the polyamide-polyamide acid solution are subjected to a reaction, and modified polyamide is prepared; the modified polyamide is subjected to melt spinning, and polyamide fibers are prepared; the preparation method comprises the following steps: pretreating nano titanium dioxide by using 4-bromobutyl trimethoxy silane to prepare modified nano titanium dioxide; mixing the modified nano titanium dioxide and ethanol to prepare a light-resistant antibacterial finishing agent; and carrying out post-treatment on the polyamide fiber by using an anti-light antibacterial finishing agent to prepare the flame-retardant and high-temperature-resistant fiber. The prepared fiber is excellent in comprehensive performance, particularly outstanding in flame retardance and high temperature resistance, and suitable for the fields of special protective clothing, high-temperature filtering materials and the like.

The invention relates to a preparation method of modified aramid fibers and an aramid fiber insulation pull rod, and belongs to the technical field of high-voltage equipment materials. The preparation method of the modified aramid fiber comprises the following steps: soaking the aramid fiber in a dopamine self-polymerization reaction solution for modification treatment to obtain the modified aramid fiber, the dopamine self-polymerization reaction solution is prepared from acetate, periodate, dopamine salt and water. According to the invention, the dopamine self-polymerization reaction liquid is utilized to carry out rapid surface modification treatment on the aramid fiber, and polydopamine is deposited on the aramid fiber, so that the roughness of the fiber surface is improved on one hand, the activity of the fiber surface is improved on the other hand, and the combination strength between the fiber and the epoxy resin is increased through the synergistic effect of the two components; and the mechanical performance of the insulating pull rod is improved.

The invention relates to the technical field of antibacterial and antifouling fabrics, provides a preparation method of an antibacterial and antifouling fabric, and solves the problem of poor fabric durability caused by single functional component and lack of physical protection in the prior art. The preparation method comprises the following steps: S1, preparing MOFs loaded antibacterial fibers: blending a metal organic framework antibacterial composite nanomaterial and a polymer matrix material, and carrying out melt spinning to prepare the MOFs loaded antibacterial fibers; s2, constructing a self-cleaning functional coating: dispersing the fluorinated nanoparticles and a polymer adhesive in a solvent to prepare a self-cleaning coating solution; s2, performing surface activation treatment on the MOFs-loaded antibacterial fiber obtained in the step S1, soaking the MOFs-loaded antibacterial fiber in the self-cleaning coating liquid, and performing pulling and curing to form a bionic micro-nano structure coating on the surface of the MOFs-loaded antibacterial fiber so as to obtain a functional composite fiber; s3, spinning forming: taking the functional composite fibers obtained in the step S2 as warp yarns and / or weft yarns, and weaving to obtain the antibacterial and antifouling fabric.

The invention belongs to the technical field of sole materials, and particularly discloses an anti-skid sole material and a preparation method thereof. The anti-skid sole material comprises a sole body, the sole body comprises an anti-skid layer and a rubber layer, and the anti-skid layer comprises the following raw material components in parts by weight; comprising 50-55 parts of polyurethane, 16-20 parts of a silicon carbide composite material, 10-14 parts of polyethylene composite fibers, 4-8 parts of a maleic anhydride grafted polyethylene octylene co-elastomer, 3-5 parts of a silane coupling agent, 1-2 parts of an antioxidant and 0.5-0.8 part of a lubricant. The anti-skid sole material prepared in the invention has excellent mechanical strength, skid resistance and wear resistance, and can provide protection for feet and prolong the service life of soles.

The invention provides a modified polyimide fiber and a preparation method and application thereof, and the preparation method comprises the following steps: S1, adding a polyimide fiber into an alkali solution for reaction, cleaning a reactant with acid and alkaline alcohol, and drying to obtain an activated polyimide fiber; s2, adding the activated polyimide fiber into an alkaline alcohol solution, adding into a first silane coupling agent, carrying out modification reaction, adding modified epoxy resin, and mixing to obtain a bottom layer component; s3, adding the activated polyimide fiber into an alkaline alcohol solution, adding a second silane coupling agent and a hyperbranched polymer, and carrying out a modification reaction to obtain a surface layer component; and S4, covering the bottom layer component with the surface layer component, drying to obtain the modified polyimide fiber, and optimizing the coating to obtain the modified polyimide fiber with high mechanical property, excellent atomic oxygen resistance and ultraviolet resistance and environmental adaptability.

The invention provides a polylactic acid fiber with a controllable degradation period. The polylactic acid fiber comprises a core layer and a skin layer wrapping the core layer, the core layer is first polylactic acid; the skin layer is second polylactic acid; the weight-average molecular weight of the first polylactic acid is 20000 to 50000; and the weight-average molecular weight of the second polylactic acid is 100000 to 200000. Compared with the prior art, the polylactic acid fiber provided by the invention has the skin-core structure, the skin layer is high-molecular-weight polylactic acid, and the core layer is low-molecular-weight polylactic acid, so that the main component of the polylactic acid fiber takes polylactic acid as a main component, other organic molecules are not introduced, and the biocompatibility and biosafety of the polylactic acid fiber are ensured; meanwhile, the degradation period can be adjusted through the molecular weight change of the skin layer and the core layer and the mass ratio.

The invention relates to the technical field of polyester fabrics, in particular to an icy, cool and smooth fabric and a preparation method thereof.Antibacterial modified polyester fibers are prepared through a composite modification technology of nano-zinc oxide and a silane coupling agent KH-560, antibacterial components can form a chemical bonding type load structure on the surfaces of the fibers, and the antibacterial components can form a chemical bonding type load structure on the surfaces of the fibers; meanwhile, the slow-release mechanism of the nano-zinc oxide can avoid direct contact with the skin, so that the antibacterial fiber has both safety and durability; secondly, the cool-feeling modified polyester fiber realizes a dual cooling mechanism through a mint essential oil microencapsulation technology and high-thermal-conductivity mineral compounding, a microcapsule slowly releases mint essential oil to provide a contact cool feeling, aluminum nitride powder and jade powder construct a rapid heat conduction channel, and the cool feeling effect can last for a long time; and finally, a softening agent prepared by compounding hydroxyl-terminated silicone oil and amino silicone oil is adopted, a low-surface-energy lubricating layer is formed on the surface of the fiber through a molecular chain directional arrangement technology, and the fabric is endowed with a silky smooth touch feeling.

The invention discloses a method for preparing flame-retardant and wear-resistant fibers for fireproof clothing by using regenerated polyester fibers, and belongs to the technical field of fiber processing, and the method specifically comprises the following steps: mixing polyester alcoholysate, a siloxane-based modifier, a catalyst and an additive, and carrying out condensation polymerization for 3-5 hours, namely modifying the polyester alcoholysate by using the siloxane-based modifier, and adding the additive into the polyester alcoholysate to obtain the flame-retardant and wear-resistant fibers for fireproof clothing. Regenerated polyester fibers with rigid frameworks and flexible networks are prepared through melt spinning and hot drafting, and then surface enhancement protection is performed through polypyrrole, so that the mechanical strength of the wear-resistant and flame-retardant fibers is effectively improved, and the wear resistance and flame retardance of the wear-resistant and flame-retardant fibers are also improved; and the composite material can be more easily applied to special fields such as fireproof suits.

The invention relates to the technical field of knitted fabrics, in particular to a high-strength wear-resistant anti-snagging functional dry knitted fabric for exercise training and a production process thereof, and the production process comprises the following steps: weighing the following raw materials in parts by weight: 30-40 parts of polyester fibers, 20-30 parts of aramid fibers, 5-10 parts of jade fibers and 5-10 parts of polyamide fibers; polyester fibers, aramid fibers, jade fibers and polyamide fibers are subjected to relaxation treatment and then subjected to a drawing procedure, and the mixed roving is obtained. According to the knitted fabric for exercise training, polyester fibers, aramid fibers, jade fibers and polyamide fibers are blended and blended to prepare mixed roving, meanwhile, the mixed roving is infiltrated and improved through infiltrating liquid, finally, the mixed roving is matched with modified polyester filaments to be subjected to circular knitting improvement, and the obtained knitted fabric has the advantages of being excellent in wear resistance, mechanical strength performance and snagging performance, good in elasticity and good in elasticity. And the knitted fabric has remarkable moisture absorption, dryness and dryness and washing resistance, and the comprehensive coordination of the product is excellent.

The invention relates to the technical field of microfiber material preparation, in particular to a preparation method of an insulating flame-retardant automotive interior microfiber material, which comprises the following steps: spinning sea-island fibers by taking PA6 as an island component and LDPE as a sea component and matching with master batches; performing opening, carding, lapping, pre-needling by a pre-needling machine and needling by a needling machine on the sea-island fibers to prepare non-woven fabric; carrying out heat setting on the non-woven fabric; preparing insulating flame-retardant polyurethane slurry, infiltrating the heat-set non-woven fabric to enable the non-woven fabric to be fully impregnated, and then feeding the non-woven fabric into an aqueous solution of dimethylformamide to be subjected to water bath curing, so as to prepare a semi-finished synthetic leather product; extracting sea components in the sea-island fibers from the synthetic leather semi-finished product by adopting a stripping process; and drying the reduced superfine fiber synthetic leather base cloth, immersing the base cloth into a softening agent aqueous solution, and then carrying out drying and leather rubbing treatment to obtain the insulating flame-retardant superfine fiber leather. The product provided by the invention is used for external protection of an intelligent auxiliary driving steering wheel sensing layer, and the resistance of the microfiber material reaches 1.2 megohm or above.

The invention relates to the technical field of fabrics, in particular to a moisture absorption and sweat releasing fabric and a preparation process thereof.The preparation process includes the following steps that raw materials including, by weight, 35-40 parts of modified polyester silk, 20-25 parts of functional yarn and 8-12 parts of polyester fiber are weighed; a preparation method of the modified polyester yarn comprises the following steps: melting, blending and extruding polyester resin and a modifier according to a weight ratio of 100: 5; weaving the modified polyester yarns, the functional yarns and the polyester fibers into a knitted fabric body by using a circular knitting machine; setting the knitted fabric body at a high temperature of 115 DEG C for 50 seconds, and obtaining the moisture-absorbing and sweat-releasing fabric after setting is finished. According to the moisture absorption and sweat releasing fabric, the modified polyester yarn, the functional yarn and the polyester fiber are woven into the knitted fabric through the circular knitting machine, the modified polyester yarn is improved and optimized by matching polyester resin with the modifier, and the moisture absorption and sweat releasing performance, the elasticity and the wear resistance of the polyester yarn are enhanced through mutual matching and mutual assistance of the raw materials.

The invention relates to the technical field of reverse osmosis membrane supports, in particular to a polyester non-woven fabric and a preparation method and application thereof.The preparation method comprises the steps that S1, polyester main body fibers and polyester adhesive fibers are used as raw materials to prepare high-quantitation original cloth M0 and low-quantitation original cloth H0; carrying out hot pressing pretreatment on the H0 to obtain a product H0 '; s2, overlapping and hot-pressing M0 and H0 'to obtain a composite non-woven fabric M1H1; s3, the M1H1 is impregnated with a functional solution, and the functional solution contains para-aramid nanofibers and nano calcium carbonate modified by hexadecyl trimethyl ammonium bromide; and then carrying out cold pressing on the composite non-woven fabric impregnated with the functional solution to obtain the nano-material modified composite non-woven fabric. And S4, carrying out secondary hot pressing treatment to obtain the polyester non-woven fabric. The polyester non-woven fabric can effectively avoid the problems of excessive curling, excessive permeation of a polysulfone solution and the like during curing after being coated with polysulfone, and is more beneficial to application in a reverse osmosis membrane.

To provide a fiber structure suitable for a wear for healthcare and nursing care workers in which inferior light resistance and heat resistance which are intrinsic to cationic dyeable polyester fiber dyed with a cationic dye are simultaneously overcome, and a method for manufacturing the fiber structure.SOLUTION: A fiber structure containing cationic dyeable polyester fiber dyed with a cationic dye contains a benzotriazole-based compound by 0.50 mass% to 3.50 mass% based on the mass of the fiber structure, and contains a zinc pyrithione-based compound by 0.05 mass% to 0.20 mass% based on the mass of the fiber structure.SELECTED DRAWING: None

The invention relates to the technical field of layered composite fabrics, and discloses a light-absorbing and heat-emitting chinlon fabric, a preparation method and application of the light-absorbing and heat-emitting chinlon fabric to thermal fabrics. According to the invention, the fluorine-free and waterproof light-absorbing and heating finishing agent with excellent light-absorbing and heating performance is prepared, then the sulfydryl silane modified chinlon single-layer fabric is subjected to surface finishing by adopting the light-absorbing and heating finishing agent through sulfydryl-alkene click reaction, and the prepared light-absorbing and heating chinlon single-layer fabric is used as the surface layer fabric; the light-absorbing and heating chinlon fabric obtained by compounding the light-absorbing and heating chinlon fabric with the inner layer made of the acrylic fiber / special-shaped section chinlon blended yarn not only has excellent light-absorbing and heating performance, but also has good waterproof performance of the surface layer, good warm-keeping performance of the inner layer and good wearing comfort, and can be applied to warm-keeping fabrics.

A material for producing macromolecule air fibers, a preparation method, and an application thereof are provided. The material for producing macromolecule air fiber is prepared by preparation of doped antibacterial TiO2 / ZnO / ZrO2 ceramic powder, deposition of magnetic iron oxide, surface modification with tannic acid, addition of water-soluble chitosan solution, immersion in a spined TPEE air fiber membrane, uniform addition of Genipin solution, heating and reacting, membrane removal, washing, and drying. The TPEE air fiber membrane produced by the present disclosure has good mechanical properties, and modified ceramic powder is uniformly dispersed in the TPEE air fiber membrane, which plays a good role in antibacterial, environmental protection, immune regulation, magnetic therapy, far-infrared heating and other effects, rendering the material for producing macromolecule air fibers have better comprehensive performance and a good mattress support material with broad application prospects.

The invention discloses a conductive yarn and a preparation method thereof, relates to the technical field of functional textile materials and composite conductive fiber preparation, and can solve the problems that an existing conductive yarn is poor in flexibility, insufficient in durability, prone to oxidation failure and difficult to integrate multiple functional performances. The preparation method comprises the following steps that S1, PBO yarn is soaked in a dopamine solution, a PDA modification layer is formed on the surface of the PBO yarn through a polydopamine self-polymerization reaction, and the PDA modification layer provides a chelation site and a bonding interface for metal deposition; s2, the PDA modified PBO yarn obtained in the step S1 is subjected to chemical silver plating, silver is deposited on a PDA modified layer to form a continuous conductive layer, and conductive PBO core yarn is prepared; s3, carrying out melt blending and granulation on the low-dielectric-constant flame-retardant filler and thermoplastic polymer resin to prepare flame-retardant composite particles; and S4, spinning by taking the conductive PBO core yarn prepared in the step S2 as a core layer and a melt formed by melting the flame-retardant composite particles prepared in the step S3 as a skin layer to prepare the conductive yarn.

The invention discloses a sixteen-hole multifunctional polyester staple fiber and a preparation method thereof, and relates to the technical field of functional fibers. Sodium alginate is used as a skin layer, polyethylene glycol terephthalate is used as a core layer, functional layering is achieved through skin-core compounding, and the interface bonding force between sodium alginate and polyethylene glycol terephthalate is enhanced through glutaraldehyde; in the melting processing process of polyethylene glycol terephthalate, a chain extender is used for reducing the melting point of the polyethylene glycol terephthalate so as to reduce the pyrolysis risk of sodium alginate, meanwhile, a low-polarity lubricant is used for grafting zirconium carbide so as to balance the lubrication and enhancement functions and realize far infrared and antistatic properties, and then an aniline monomer is initiated to polymerize on the surface of zirconium carbide so as to prepare the far infrared anti-static polyethylene glycol terephthalate composite material. Seaweed-carbon can generate far infrared radiation and negative ions, and zirconium carbide can be used as an electron acceptor to enhance the carrier mobility, so that the far infrared and antistatic properties of the fiber are enhanced.

The invention discloses a medical washable high-temperature-resistant modified polyester fiber fabric and a preparation method thereof, and relates to the technical field of fabrics. The medical washable high-temperature-resistant modified polyester fiber fabric prepared by the invention is obtained by blending, spinning and weaving modified polyester and modified mica and activating with sodium hypochlorite; the modified polyester is obtained by grafting organic silicon modified polyester with n-dodecanethiol and then reacting with bromooctylhydantoin; the modified mica is prepared by polymerizing diethyl phosphite and bisphenol S on the surface of the pretreated mica, grafting a vinyl monomer and then reducing; the vinyl monomer is obtained by carrying out a reaction on 1-allyl-3-cyano-6-hydroxy-4-methyl-2-pyridone and an azo salt, and the vinyl monomer is obtained by carrying out a reaction on 1-allyl-3-cyano-6-hydroxy-4-methyl-2-pyridone and an azo salt; the medical washable high-temperature-resistant modified polyester fiber fabric prepared by the invention has good antibacterial, anti-aging and flame-retardant properties.

The invention relates to the technical field of high-performance polyester fibers, and discloses a dry skin-friendly fiber fabric, a preparation method thereof and application of the dry skin-friendly fiber fabric in underwear. The preparation method of the dry and comfortable skin-friendly fiber fabric comprises the following steps: carrying out reaction on terephthalic acid, ethylene glycol and an antibacterial modified diamide diol monomer to obtain modified polyester; the modified polyester and the polyester master batch are mixed and spun, and the modified profiled polyester fiber is obtained; dipping the modified profiled polyester fiber in a finishing liquid containing a biopolymer finishing agent to obtain the high-performance polyester fiber, blending and knitting high-performance polyester fibers, cotton fibers and mulberry silk fibers to obtain a dry skin-friendly fiber fabric; the dry and comfortable skin-friendly fiber fabric has excellent antibacterial performance, moisture absorption performance and skin-friendly performance, the skin can be kept dry and comfortable, safe and comfortable wearing experience is provided for a wearer, and the dry and comfortable skin-friendly fiber fabric can be used for underwear and other underwear materials.

The invention discloses a drilling fluid plugging agent based on modified resin and fibers, and relates to the technical field of oilfield chemistry. The plugging agent comprises modified phenolic resin, modified epoxy resin, modified urea resin, modified polyester fiber and modified glass fiber. The modified phenolic resin is prepared by modifying phenolic resin with ethyl silicate, the modified epoxy resin is prepared by reacting a carbon nanotube grafted with a silane coupling agent with epoxy resin, and the modified urea-formaldehyde resin is prepared by reacting diisocyanate with urea-formaldehyde resin. The modified polyester fiber is prepared by reaction of a silane coupling agent and polyester fiber, and the modified glass fiber is prepared by reaction of boric acid ester and glass fiber etched by hydrofluoric acid. The plugging agent disclosed by the invention has excellent temperature resistance and pressure-bearing strength, and meanwhile, the influence on the rheological property of the drilling fluid is relatively small.

The present invention discloses an antistatic and quick-drying multi-layer composite nylon fabric and a preparation method thereof. The antistatic and quick-drying multi-layer composite nylon fabric sequentially includes, from the outside to the inside: a modified layer, a carbon bead layer, and a moisture absorption layer; the modified layer is prepared by mixing bio-based nylon and modified graphene to obtain a modified graphene nylon fabric, and then blending it into yarn and weaving it; the carbon bead layer is prepared from carbon powder, phenolic resin, nano silver, and a surfactant; the moisture absorption layer is prepared by soaking bio-based nylon in a moisture absorbent, blending it into yarn, and weaving it; when polypropylene / modified graphene fiber modifies the existing bio-based nylon, it not only improves the antistatic resistance but also maintains a relatively high mechanical strength as much as possible. The prepared composite fabric has better antistatic, antibacterial, and moisture absorption properties, effectively solving the problem of the decrease in breaking strength and service performance caused by the improvement of antistatic properties.

The invention provides a preparation method of a hydrophilic antibacterial modified polylactic acid wire, which comprises the following steps: S1) plying and twisting polylactic acid filaments to obtain polylactic acid plied yarns; s2) weaving the polylactic acid plied yarn to obtain a polylactic acid wire; s3) performing low-temperature plasma treatment on the polylactic acid fiber to obtain a surface-activated polylactic acid wire; and S4) transferring the treatment solution to the surface of the surface-activated polylactic acid wire rod to obtain the hydrophilic antibacterial modified polylactic acid wire rod. Compared with the prior art, the preparation method disclosed by the invention has the advantages that a low-temperature plasma technology and a carboxyl-terminated hyperbranched polymer / polydopamine blended solution coating technology are utilized to achieve a synergistic effect, hydrophilic and antibacterial functions are simultaneously given to the modified polylactic acid wire rod, and the modification effect is ensured to have very high stability and durability; in addition, according to the method, the main component of the polylactic acid in the suture fibers is reserved, and the biocompatibility and the biological safety of the polylactic acid material are ensured.

A preparation method of an emulsion type aramid fiber sizing agent belongs to the technical field of fiber surface treatment, and the specific scheme is as follows: preparing aromatic polyamide from corresponding diamine and acyl chloride, then reacting with epoxy resin to prepare modified epoxy resin, and preparing the emulsion type aramid fiber sizing agent under the action of a compound emulsifier. The preparation method disclosed by the invention is simple and relatively low in cost, better interface bonding can be formed between the aramid fiber and the epoxy resin after sizing by the sizing agent, and particularly, the interlayer shear strength of the aramid fiber / epoxy resin composite material is relatively well improved; the preparation method has important significance in improving the use performance and stability of the aramid fiber composite material and expanding the application of the aramid fiber.

The invention discloses a phosphorus-sulfur synergistic flame retardant with high gas phase activity, a durable flame-retardant nylon fabric and a preparation method of the flame-retardant nylon fabric, and relates to the technical field of flame-retardant nylon fabric preparation.The preparation method of the phosphorus-sulfur synergistic flame retardant comprises the steps that 9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide and polyepoxide are mixed and heated to be molten for a reaction, and the phosphorus-sulfur synergistic flame retardant is obtained; obtaining an intermediate after the reaction is finished; the intermediate and a thiophenethiol derivative are subjected to a click chemical reaction, and a 9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide derivative containing phosphorus and sulfur is obtained; the preparation method comprises the following steps: dissolving a 9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide derivative containing phosphorus and sulfur into a mixed solvent of ethanol and water, so as to obtain the phosphorus-sulfur synergistic flame retardant with high gas phase activity. The raw materials are safe and environmentally friendly, the preparation method is simple, and the prepared flame-retardant nylon fabric is excellent in flame retardance and washing resistance and free of pollution in the using process.

The invention relates to the technical field of sewage treatment, in particular to an electrostatic spinning PVDF nanofiber membrane for sewage treatment and a preparation method and application of the electrostatic spinning PVDF nanofiber membrane. The preparation method comprises the following steps: dissolving PVDF (Polyvinylidene Fluoride) particles in a mixed solvent of DMF (Dimethyl Formamide) and acetone, adding nano TiO2 particles subjected to APTES (Aminopropyltriethoxysilane) surface modification, and adding PVP (Polyvinyl Pyrrolidone) into the solution to obtain a uniform spinning solution; spinning by adopting electrostatic spinning equipment to obtain a PVDF / TiO2 / PVP nanofiber membrane; the nanofiber membrane is soaked in a sodium hydroxide solution, then the membrane is soaked in a Tris-HCl buffer solution containing dopamine, and the final electrostatic spinning PVDF nanofiber membrane is obtained. The average diameter of nanofibers of the nanofiber membrane is 200-300nm, the porosity of the membrane is 70-80%, and the water contact angle is less than 60 degrees; when the nanofiber membrane is used for treating sewage containing organic pollutants and heavy metal ions, the removal rate of the nanofiber membrane on methyl orange can reach 95% or above; the rejection rate of copper ions can reach 90% or above; the removal efficiency of organic pollutants and heavy metal ions is obviously improved.

The invention discloses special cloth for a single-sided terry bath foaming towel and a weaving method of the special cloth. The terry cloth comprises a three-layer structure integrally woven by a warp knitting machine, wherein the three-layer structure comprises a base layer and 100D / 36F polyester filament yarn warp knitting chain weave; the binding layer is a 100D / 96F polyester filament chain stitch and penetrates through the substrate layer; the looped pile layer is of a vertical looped pile structure formed by 300D / 10F polyester filaments, the height of looped piles is 7-8 mm, and the density of the looped piles is 25-30 / cm; the thickness ratio of the base layer to the binding layer to the looped pile layer of the three-layer structure is 0.6: 1: 7. The three kinds of yarns with different thicknesses are combined to form a three-layer structure, the three-layer structure is directly formed through warp knitting, a traditional fuzzing roller is not needed for fuzzing, the upright performance of a looped pile is guaranteed, it is guaranteed that the looped pile does not generate monofilament breakage and is stable in structure, and the foaming performance and the weaving feasibility are balanced.

The invention provides an optical transparency-optical confinement composite nanofiber membrane as well as a preparation method and application thereof. The optical transparency-optical confinement composite nanofiber membrane comprises a PDMS (Polydimethylsiloxane) / PS (Polystyrene) / TPU (Thermoplastic Polyurethane) nanofiber membrane and a photothermal conversion material layer loaded on the PDMS / PS / TPU nanofiber membrane, the PDMS / PS / TPU nanofiber membrane is prepared by taking PDMS, PS and TPU as raw materials and adopting an electrostatic spinning technology; the photothermal conversion material layer comprises honeycomb porous carbon nanofibers and PDA (Personal Digital Assistant). The optical transparency-optical confinement composite nanofiber membrane and the PDMS / PS / TPU nanofiber membrane have excellent light transmittance and hydrophobicity, the photo-thermal conversion material layer has excellent light absorptivity and high photo-thermal conversion capacity, and the optical transparency-optical confinement composite nanofiber membrane has high membrane flux when being used for photo-thermal membrane distillation desalination. And the photo-thermal film is excellent in distillation performance stability.