80793results about How to "Simple preparation process" patented technology

A reflective element assembly for a variable reflectance vehicular mirror includes a front substrate having a transparent conductive coating disposed on a second surface, and a rear substrate having a third surface conductive coating disposed on its third surface and preferably, a fourth surface conductive coating disposed on its fourth surface. At least a portion of the third surface conductive coating may wrap around an edge portion of the rear substrate and at least a portion of the fourth surface conductive coating may wrap around at least a second portion of the perimeter edge so as to establish electrical continuity between the fourth surface conductive coating on the fourth surface and the third surface conductive coating on the third surface. The rear substrate may have a smaller dimension than the front substrate so as to provide an overhang region, preferably at the wraparound region.

A reflective element assembly for a variable reflectance vehicular mirror includes a front substrate having a transparent conductive coating disposed on a second surface, and a rear substrate having a third surface conductive coating disposed on its third surface and preferably, a fourth surface conductive coating disposed on its fourth surface. At least a portion of the third surface conductive coating may wrap around an edge portion of the rear substrate and at least a portion of the fourth surface conductive coating may wrap around at least a second portion of the perimeter edge so as to establish electrical continuity between the fourth surface conductive coating on the fourth surface and the third surface conductive coating on the third surface. The rear substrate may have a smaller dimension than the front substrate so as to provide an overhang region, preferably at the wraparound region.

The invention discloses a microcapsule of an organic phase change energy storage material and a preparation method thereof. The microcapsule of an organic phase change energy storage material comprises a core and a nucleocapsid, wherein the material of the core comprises the organic phase change energy storage material; the nucleocapsid at least comprises an inner layer and an outer layer, the inner layer is packaged by any one of an in situ polymerization method, an interface polymerization method, a reaction phase separating method, a double agglomeration method and a sol-gal process, and the outer layer is packaged by any one of an in situ polymerization method, a reaction phase separating method, a sol-gal process and a double agglomeration method. The microcapsule has adjustable size, nucleocapsid composition and shell thickness, favorable flexibility, mechanical strength, penetrability resistance and dispersibility and can be widely applied to the fields of energy sources, materials, aero-space, textile, electric power, medical apparatus, architecture, and the like, such as solar utilization, industrial afterheat and waste heat recovery, architecture energy storage, dress with constant temperature, air conditioners for cool and heat accumulation, constant temperature of electric appliances, and the like.

The invention relates to a preparation method of a polymer / graphene composite material through in situ reduction, which is characterized by comprising the following steps: adopting ultrasonic wave or grinding to evenly disperse the graphite oxide prepared by a Hummers method into polymer dispersion; introducing reducing agent into the polymer dispersion for in situ reduction, enabling the graphite oxide to be reduced into the grapheme so as to obtain stable polymer / graphene composite emulsion; carrying out demulsification, agglomeration and drying to obtain the composite polymer / grapheme composite master batch; adding the dried polymer / grapheme composite master batch and various assistants into the polymeric matrix according to a certain ratio; and carrying out double-roller mixing, vulcanization, melt extrusion or injection molding to obtain the polymer / graphene composite material with excellent physical and mechanical properties.

The invention discloses a full-carbon coaxial line and a manufacturing method of the full-carbon coaxial line, and belongs to the technical field of integrated circuits. Graphene serves as a monatomic layer thickness, is coiled into a cylinder and form an inner conductor of the coaxial line with a small radius (can be as small as the nm level), and the inner conductor of the coaxial line transfers currents. Meanwhile, a signal layer or multiple layers of graphene serve(s) as an outer conductor of the coaxial line to form a boundary of electromagnetic waves in a space, and graphite oxide serves as medium materials between the inner conductor and the outer conductor to limit and guide oriented transmission of electromagnetic wave energy. The coaxial line is quite small in size and applicable to radio-frequency and microwave integrated circuits.

Improved, adaptable tissue-type heart valves and methods for their manufacture are disclosed wherein a dimensionally stable, pre-aligned tissue leaflet subassembly is formed and its peripheral edge clamped between and attached to an upper shaped wireform and a lower support stent. A variety of adaptable structural interfaces including suture rings, flanges, and conduits may be attached to the support stent with or without an outlet conduit disposed about the wireform to provide a tissue-type heart valve adaptable for use in either a natural heart or in mechanical pumping devices. The methods include forming individual leaflets with a template and using the template to attach the leaflets together to form a tissue leaflet subassembly. The template and leaflets include a straight edge terminating in oppositely directed tabs, and a curvilinear cusp edge extending opposite the straight edge. The template may include a guide slot in its straight edge and the assembly includes aligning two leaflet tabs with the template and passing sutures through the guide slot and through the leaflet tabs. The leaflet subassembly is mated to a wireform with the tabs extending through commissure posts of the wireform. A support stent having an upper surface matching the lower surface of the wireform sandwiches the edges of the leaflet subassembly therebetween. Separated tabs on the leaflet subassembly are passed through the wireform commissures and attached to adjacent stent commissures so as to induce clamping of the leaflet tabs between the stent commissures and wireform commissures upon a radially inward force being applied to the leaflets.

The invention relates to a method for the isolation of hepatitis C virus. The method comprises the separation of particles termed exosomes from the blood plasma of an individual infected with hepatitis C virus (HCV) and the extraction or RNA from these exosome particles.

The invention relates to a catalyst for dehydrogenating propane to prepare propone, which uses thermal-resistant oxide as carrier, uses palladium-group metal as main catalyst, uses IV A group metal and rare-earth metal as agents, uses halogen as modifier, and uses inorganic oxide with high temperature resistance as adhesive. The inventive catalyst under high temperature and low pressure has higher propane transfer rate, propone selectivity and reaction stability. And the preparation comprises that at 60-100Deg. C, immerging thermal-resistant oxide with rare-earth metal water solution for 2-10h, at 60-180Deg. C baking for 2-10h, at 400-600Deg. C baking for 3-10h, immerging said carrier and the water solution which contains palladium metal and IVA metal at 60-100Deg. C for 2-10h, and baking for 2-10h at 60-180Deg. C, adding adhesive, protruding agent and acid gel solvent, protruding and shaping, baking for 2-10h at 60-180Deg. C, activating for 3-10h at 400-600Deg. C, and reducing for 2-10h in hydrogen flow at 400-600Deg. C.

A method to promote the activity of a catalyst for dehydrogenation of propane to propylene is as follows: (1) an inorganic oxide bonding agent, a promoter and an acid solvent are added into a heat-resistant oxide; then after the oxide bonding agent, the promoter, the acid solvent and the oxide are kneaded evenly, the oxide is molded by rolling or band-extruding; (2) the catalyst carrier prepared is dried for 2 to 10 hours under the temperature of 60 centigrade degrees, and calcined under the temperature of 400 to 800 degrees; (3) the calcined carrier is immersed in a rare earth metal water solution under the temperature of 60 to 100 centigrade degrees for 2 to 10 hours; (4) the catalyst carrier modified by the rare earth is immersed in a water solution comprising platinum metal elementsand the fourteenth metal elements under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours, and then the carrier is filtered, washed with distilled water, dried under the temperature of 60 to 180 centigrade degrees for 2 to 10 hours, and calcined under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours; (5) the catalyst prepared is activated in the air under the temperature of 400 to 600 centigrade degrees for 3 to 10 hours, and reduced in a hydrogen flow under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours; the reduced catalyst is used for catalytic reaction for dehydrogenation of propane to propylene.

Targeted therapeutics that localize to a specific subcellular compartment such as the lysosome are provided. The targeted therapeutics include a therapeutic agent and a targeting moiety that binds a receptor on an exterior surface of the cell, permitting proper subcellular localization of the targeted therapeutic upon internalization of the receptor. Nucleic acids, cells, and methods relating to the practice of the invention are also provided.

The present invention belongs to the field of hollow material preparing technology, and is especially the preparation process of hollow ball of inorganic matter, metal, organic matter and composite structure with hollow polymer ball as template. The present invention prepares composite hollow ball through combining hollow polymer ball template with sol-gel, deposition reaction, oxidation-reduction process and through forced interface process or surface deposition process; and obtain hollow ball of inorganic matter, metal and organic matter through high temperature sintering or selective solvent extraction to eliminate template polymer. The control of hollow ball structure and size and the compounding of several kinds of matters may be realized through controlling reactant activity, material feeding mode, reactant concentration and circulating reaction process. The hollow ball has excellent dispersivity, high strength and size stability. The present invention also relates to the application of these hollow structure materials.

A preparation method of completely peeled oxidation graphene / rubber nanometer composite material adopts combination of emulsion compounding and flocculation processes or combination of emulsion compounding and spraying drying processes. The preparation method retains the phase state structure of the oxidation grapheme / rubber composite emulation in the liquid state and obtains the phase-state structure which is highly dispersed, highly peeled and dispersed in nanometer scale dispersion. Simultaneously, substances capable of acting with generating ionic bond effect or chemical bond effect with an oxidation graphene surface functional group are added into the oxidation graphene / hydrosol to serve as an interface agent, thereby improving interface combination effect of oxidation graphene and rubber. Vulcanized rubber prepared by the composite material of the preparation method through follow-up mixing and vulcanizing has mechanical property such as high tensile strength, stretching stress and tearing strength and is capable of greatly improving abrasion resistance and gas separation performance of the vulcanized rubber. The preparation method is simple, easy, low in cost, apt to industrialization and wide in suitable aspect, saves energy and has better economical and social benefits.

The present invention provides for compositions and methods for the preservation of tissues and organs ex vivo and in situ. In addition, the present invention provides for kits that may be used in the preparation of the solutions of the present invention.

The invention relates to a lithium ion battery silicon-based composite anode material, a preparation method of the lithium ion battery silicon-based composite anode material, and a battery. The lithium ion battery silicon-based composite anode material adopts an embedded composite core-shell structure, a core has a structure formed by embedding nano silicon particles into a gap of an inner layer of hollowed graphite, and a shell is made from a non-graphite carbon material. According to the silicon-based composite anode material, mechanical grinding, mechanical fusing, isotropic compression processing and carbon coating technologies are combined, so that the nano silicon particles can be successfully embedded into the inner layer of the graphite and the surfaces of graphite particles are uniformly coated; the high-performance silicon-based composite anode material is obtained and is excellent in cycle performance (the 300-times cycle capacity retention ratio is more than 90%) and high in first efficiency (more than 90%); in addition, the silicon-based composite anode material is high in specific energy and compaction density, and can meet the requirements of a high-power density lithium ion battery; the preparation process is simple, the raw material cost is low, and the environment is protected.

The invention relates to an electromagnetic shielding optical window with a two-double pane metal grating structure and belongs to the optical transparent piece electromagnetic shielding technical field; the electromagnetic shielding optical window is formed by placing two layers of pane metal gratings or metal silk screens with the same structure parameters on two sides of the optical window or a transparent underlay in parallel; a side length of a pane of the two-double pane metal grating is greater than two times of a side length of a pane of the prior monolayer pane metal grating; the space between two layers of pane metal gratings is two to four times of the side length of the pane; compared with the prior monolayer pane metal grating, the optical window adopting the two-double pane metal grating structure does not reduce light transmittance, substantially improves the shielding efficiency of microwaves and millimeter waves, solves the problems that the high light transmittance and strong electromagnetic shielding efficiency can not simultaneously considered in the prior optical window electromagnetic shielding technology and is suitable for electromagnetic shielding in aerospace equipment, security facilities, medical diagnostic instruments and other military and civil optical transparent pieces.

The invention relates to a self-greasing paint which can prevent screw thread from sticking and wearing and a preparation method thereof. The self-greasing paint which can prevent screw thread from sticking and wearing is a two-component self-greasing paint that consists of a component A and a component B. Component A consists of raw materials with weight proportion of 40-90 percent of film-forming material, 5-60 percent of solid greasing material, 0-10 percent of additive, 0-50 percent of solvent, 0-10 percent of color paint and 0-10 percent of filling while component B consists of raw materials with weight proportion of 50-100 percent of curing agent and 0-50 percent of solvent. The weight ratio of component A and component B is 1 to 0.1-5. The friction coefficient of the coat formed by the paint is low and the paint has self greasing function, anti-sticking and wearing resistant performances; the invention reduces and even avoids the use of grease and solves pollution problem caused by grease. The self-greasing paint is applicable to various mechanical parts such as bolt, screw, etc., in particular to screw threads of oil pipe, cashing and drill rod, etc. that are special for oil industry.

A negative electrode material comprises a conductive powder of particles of a lithium ion-occluding and releasing material coated on their surface with a graphite coating. The graphite coating, on Raman spectroscopy analysis, develops broad peaks having an intensity I1330 and I1580 at 1330 cm−1 and 1580 cm−1 Raman shift, an intensity ratio I1330 / I1580 being 1.5<I1330 / I1580<3.0. Using the negative electrode material, a lithium ion secondary battery having a high capacity and improved cycle performance can be manufactured.

The invention relates to a high-temperature-insulating material and a preparation method therefor and particularly relates to the high-temperature-insulating material, which has a nano porous structure, prepared through forming an aqueous-phase uniform three-dimensional-network nano porous structure by taking thixotropic colloid as a template agent and adding a binding agent, aggregates, powder materials, an opacifier and admixtures. The preparation method for the high-temperature-insulating material, disclosed by the invention, is simple and easy in operation, low in production cost and environment-friendly and safe in process, does not need high-pressure special equipment, is free of combustible and explosive or other harmful substances and is beneficial to mass production. The high-temperature-insulating material disclosed by the invention has the characteristics of light weight, high strength and low coefficient of thermal conductivity, can be used for preparing high-temperature-insulating bricks, heat-insulating plates, special-shaped pieces and coating materials and can be applied to the heat insulating protection of equipment such as high-temperature furnace hearths, pipelines and valves in the fields of aerospace and military industries, metallurgical forging, petroleum refining, electric power and the like, so that the safety of use and the level of energy saving and consumption lowering are improved.

The invention relates to the technical field of soil heavy metal remediation, and specifically discloses a method for preparing an iron-based bio-char material, a prepared iron-based bio-char material, and a method for applying the iron-based bio-char material in treating soil heavy metal pollution. According to the material, biomass is adopted as a raw material; a high-temperature carbonization method is adopted; during the bio-char preparation process, an iron-containing compound is added, such that iron is doped according to a certain ratio, and the iron-based bio-char material with special structure and function is formed. The material has the advantages of simple preparation process, low production cost, and short production period. The obtained iron-based bio-char material has a unique effect in repairing arsenic-cadmium composite polluted soil. With the material, bio-availability of arsenic and cadmium in soil can be effectively reduced, arsenic and cadmium contents in agricultural products planted in the arsenic-cadmium composite polluted soil can be greatly reduced, and no toxic or side effect is caused on crops. The material is safe to apply, and can be used in a large scale in treatment of arsenic-cadmium composite polluted soil.

Targeted therapeutics that localize to a specific subcellular compartment such as the lysosome are provided. The targeted therapeutics include a therapeutic agent and a targeting moiety that binds a receptor on an exterior surface of the cell, permitting proper subcellular localization of the targeted therapeutic upon internalization of the receptor. Nucleic acids, cells, and methods relating to the practice of the invention are also provided.

A non-aqueous electrolyte secondary battery negative electrode material is provided wherein a negative electrode active material containing a lithium ion-occluding and releasing material which has been treated with an organosilicon base surface treating agent is surface coated with a conductive coating. Using the negative electrode material, a lithium ion secondary battery having a high capacity and improved cycle performance is obtainable.

The present invention provides a method for reducing the amount of water produced from a subterranean formation as a result of stimulation of the subterranean formation. The method comprises the introduction of a first and second reactive polymer which leak-off into the formation and which are capable of subsequently reacting together to form a reaction product which selectively reduces the permeability of the formation to water flow through the formation. The reactive polymers react in situ to form a reaction product that binds to the formation in such a manner that the flow of water is selectively retarded through the matrix while the flow of oil is substantially unaffected.

The invention discloses a grapheme / silicon composite material for a lithium ion battery cathode material and a preparation method thereof, belonging to the fields of electrochemistry and new energy materials. The method comprises the following steps of: using graphite as a raw material; oxidizing the graphite into oxidized graphite by adopting oxidants of concentrated sulfuric acid and potassium permanganate; then, ultrasonically stripping the oxidized graphite to prepare oxidized graphene; mixing oxidized graphene in different proportions with nano silicon powder; ultrasonically dispersing, filtering or directly drying into a cake / film; and roasting under a reduction atmosphere to prepare self-support graphene / silicon composite film materials in different proportions. Proved by electrochemistry tests, the graphene / silicon composite film material prepared by the method has higher specific capacity and cycle stability, simple preparation method and easy mass production and consequently is an ideal high-energy lithium ion battery cathode material.

The invention discloses a mesoporous Y-type zeolite molecular sieve and a preparation method thereof. The preparation method comprises the following steps of: firstly preparing a Y-type zeolite guiding agent; and then guiding synthesis of the mesoporous Y-type zeolite molecular sieve by using amphiphilic organosilane N,N-dimethyl-N-[3-(trimethoxysilane)propyl]octadecyl ammonium chloride (TPOAC) as a mesoporous template, wherein siloxane group at the organosilane terminal is firstly hydrolyzed into silicon hydroxyl; then the silicon hydroxyl is linked to a skeleton on the zeolite surface through chemical bonds; and other alkyl terminals are polymerized and then participate in pore expansion. According to the method disclosed by the invention, mesoporous zeolites can be synthesized by using a one-step hydrothermal process; the method is simple in preparation process, easy to operate and low in cost and good in connectivity between mesopores and micropores, and facilitates macromolecular diffusion. As the prepared mesoporous zeolite molecular sieve has the mesopores and the micropores, the defect of a single pore structure is avoided; and the mesoporous Y-type zeolite molecular sieve has broad application prospect in the catalytic field, in particular in macromolecular diffusion-limited reaction.

The present invention provides a process for preparing carbon quantum dots having uniform size by using emulsion, and a process for doping the inside of the carbon structure with other element or replacing the surface with a surface stabilizer having a specific chemical functional group different from existing stabilizers in order to control the properties of the carbon quantum dots. The process for preparing the carbon quantum dots according to the present invention makes a mass production possible and the process thereof is simple. Furthermore, the process is easy to control the size of the quantum dots and the reaction yield rate of the method is excellent. In addition, according to the present invention, it is possible to synthesize carbon quantum dots having uniform size and superior quantum yield rate and it makes it possible to embody the color as equivalent to existing molecular chromophores or heavy metal quantum dots by changing the structure of the chromophore.

The invention relates to high-temperature-resistant modified polyfunctional epoxy matrix resin for an advanced composite material. The resin comprises tetramaleimide resin, carboxy terminated nitrile rubber, polyfunctional epoxy resin, a curing agent and an organic solvent. A preparation method comprises the following steps of: adding the tetramaleimide resin, the carboxy terminated nitrile rubber and the polyfunctional epoxy resin into a reaction kettle and reacting at the temperature of 110 DEG C for one hour; adding the organic solvent and dissolving under stirring to obtain a component A;mixing the curing agent and the organic solvent and dissolving under stirring to obtain a component B; and mixing the component A and the component B and uniformly stirring during use. The high-temperature-resistant modified polyfunctional epoxy matrix resin provided by the invention has the advantages of high room temperature tensile shear strength, high heat resistance, wide application prospect in the fields such as electronics, micro-electronics, printed circuit boards (PCB), motors, aerospace and the like, simple preparation process, low cost and contribution to realizing industrial production.

The entire process of reverse transcription-polymerase chain reaction (RT-PCR) is simplified by using oligonucleotide-immobilized microplates made of, e.g., polypropylene, to which oligonucleotides are securely immobilized and which can be subjected to thermal cycles of PCR. RT-PCR is preferably conducted in solid-phase. Capturing of mRNA and RT-PCR can be conducted in the same plates. The cDNA synthesized from the mRNA captured on the microplates can be used more than once. Further, in combination with the microplates, a filter plate is used for the preparation of cell lysates wherein target cells are placed on the filter plate, and a lysis buffer is passed through the cell layer on the filter to transfer cell lysate directly to the microplate via well-to-well communication.

The invention discloses a preparation method of a graphene / polymer nano composite material, which is characterized by comprising the following steps: adding 0.1-30 parts by weight of graphite oxide into 10-3000 parts by weight of water, and dispersing and exfoliating by carrying out ultrasonic dispersion (the power is 50-500W, and the frequency is 10-100000Hz) at 10-100 DEG C for 15 minutes-5 hours or mechanical lapping for 15 minutes-5 hours or mechanical stirring for 1-48 hours to obtain a graphene oxide water solution; adding the graphene oxide water solution into 100 parts by weight of polymer emulsion of which the solid content is 10-70%; continuing the ultrasonic or mechanical stirring to carry out uniform mixing; demulsifying by adding 1-100 parts by weight of 5-100% demulsifier toobtain a graphene oxide / polymer granular suspension; adding 0.1-100 parts by weight of reducer into the graphene oxide / polymer granular suspension, reducing at 20-100 DEG C for 1-72 hours, filtering,and drying in a drying oven at 20-100 DEG C for 2-72 hours or drying in a vacuum drying oven at 20-120 DEG C under a vacuum degree of 0.1-0.01 MPa for 2-48 hours, thereby obtaining the graphene / polymer nano composite material.

The invention discloses a super-hydrophilic and underwater-super-oleophobic oil-water separation mesh membrane, and a preparation method and an application thereof. According to the method, fabric mesh with a specification of 100-300 meshes is subjected to ultrasonic cleaning, and is air-dried under normal temperature; a hydrophilic polymer water-sensitive agent and a cross-linking agent are dissolved in water according to a ratio of 1:9-9:1; the mixture is well mixed by magnetic stirring, such that a solution with a concentration of 1-99% is prepared; nano-sol is prepared with a sol-gel method; the solution and the nano-sol are prepared into a mixed solution with a concentration of 1-99%, and the solution is well dispersed through ultrasonic dispersion; the mesh is soaked in the mixed solution and is vertically lifted, or the mesh is directly sprayed by using a high-pressure spraying gun; and the mesh is bake-dried, such that the super-hydrophilic and underwater-super-oleophobic oil-water separation mesh membrane is obtained. Contact angles of the super-hydrophilic and underwater-super-oleophobic oil-water separation mesh membrane with water and oil in air are both 0 DEG, and the membrane is super-hydrophilic. Under water, the contact angle of the membrane with oil drops is larger than 150 DEG, and the membrane has an oil drop low adhesion characteristic. The mesh membrane provided by the invention can be used in oil-water mixture separation and oil-containing sewage processing.

A preparation method of a high power capacity lithium ion battery cathode material uses natural spherical graphite to serve as raw materials, uses concentrated sulfuric acid to serve as an inserting layer agent, uses potassium permanganate to serve as an oxidizing agent, conducts expansion treatment at high temperature to obtain micro-expanded graphite, then enables the micro-expanded graphite in different proportions to be mixed with nanometer ganister sand, conducts ultrasonic dispersion, suction filtration and dying to obtain the micro-expanded graphite with the nanometer ganister sand inserted in layers, enables the micro-expanded graphite to be mixed and coated with carbon source carbon source according to certain proportion, and finally conducts carburizing sintering under inert gas shielding to prepare completely coated silicon carbon composite cathode material with sufficient obligated obligate inside. Electrochemistry shows that the silicon carbon composite material prepared by the preparation method has high specific capacity and cycling stability and is the ideal high power capacity lithium ion battery cathode material.