2123 results about "Melt extrusion" patented technology

The invention relates to the technical field of current collectors, in particular to a flame-retardant composite current collector and a preparation method thereof.The flame-retardant composite current collector is composed of a base film layer, metal film layers deposited on the two faces of the base film layer and flame-retardant layers formed by curing flame-retardant coatings and coated on the surfaces of the metal film layers; the preparation method comprises the following steps: S1, mixing the modified polypropylene resin, the reinforcing component, the antioxidant, the lubricant, the coupling agent and the compatilizer to obtain a mixture; s2, carrying out melt extrusion and tape casting on the mixture, and stretching through a two-way stretching process to form a base film layer; s3, metal film layers are deposited on the two faces of the base film layer, and hot press molding is conducted; s4, coating a flame-retardant coating, drying and curing to obtain the flame-retardant composite current collector, the prepared flame-retardant composite current collector has excellent flame retardance, excellent mechanical property and thermal aging resistance and high peel strength, the binding force of the metal film layer and the base film layer is firm, and the quality and safety of the composite current collector are effectively improved.

The invention relates to the technical field of capacitor films, in particular to a high-temperature-resistant polypropylene capacitor film and a preparation method thereof.The high-temperature-resistant polypropylene capacitor film is prepared from, by weight, 94-98 parts of polypropylene resin, 1-3 parts of filler-doped modified balance adjusting agent, 0.5-2 parts of boron nitride-glass fiber combined agent, 0.05-0.4 part of nucleating agent, 0.2-0.4 part of antioxidant and 0.1-0.4 part of silane coupling agent; the high-temperature-resistant polypropylene capacitor film is obtained through the processes of melting extrusion molding, cooling shaping, preheating, two-way stretching, heat shaping, rolling and the like of the raw material composition. The polypropylene resin, the nucleating agent, the antioxidant and the silane coupling agent are blended, the filler-doped modified balance adjusting agent and the boron nitride-glass fiber coupling agent are added, and the raw materials are blended and coordinated, so that high feasibility of a two-way stretching process is guaranteed, breakdown resistance, mechanical strength and dielectric loss performance of the product are optimized, and the product has good mechanical properties. And meanwhile, the high-temperature-resistant and corrosion-resistant stability effects are remarkable.

The invention relates to the field of functional master batch materials, in particular to a phase-change energy temperature-adjusting fiber master batch and a fat-burning fabric thereof. The phase-change energy temperature-regulating fiber master batch is prepared from a composite phase-change material and polyethylene glycol terephthalate slices through melt extrusion and granulation, the fat-burning fabric is prepared from the phase-change energy temperature-adjusting fiber master batch and polyethylene glycol terephthalate slices through melt spinning, network compounding and weaving processing. By introducing the microencapsulated phase-change material and the high-thermal-conductivity filler, in the melt extrusion process, the microencapsulated phase-change material and the high-thermal-conductivity filler can be uniformly dispersed in the matrix material to form stable fiber master batches, form an efficient thermal-conductivity structure and provide excellent thermal regulation performance; meanwhile, microencapsulation can improve the stability and dispersity of the phase-change material, and the fat-burning fabric is prepared through melt spinning and weaving of fiber master batches, so that the heat-conducting property of the product is improved, and the continuous fat-burning effect is achieved.

The invention relates to the technical field of plastic cups, in particular to a transparent polypropylene medical plastic cup and a preparation method thereof. The plastic cup comprises the following components in parts by weight: 60-80 parts of polypropylene, 3-8 parts of polyformaldehyde, 5-15 parts of modified nano calcium carbonate, 3-5 parts of kaolin, 2-4 parts of talcum powder, 0.2-0.4 part of a nucleating agent, 0.5-1.5 parts of a lubricant, 1-3 parts of an antioxidant and 0.5-1.0 part of a stabilizer. The preparation method comprises the following steps: uniformly stirring polypropylene, polyformaldehyde, modified nano calcium carbonate, kaolin, talcum powder, a nucleating agent, a lubricant, an antioxidant and a stabilizer to obtain a mixture; the mixture is subjected to melt extrusion, granulation and injection molding to obtain the plastic cup, and the plastic cup not only has excellent mechanical properties, but also has excellent antibacterial properties, and can effectively prevent growth of bacteria.

The invention relates to the technical field of high polymer material preparation, and discloses a bamboo fiber graft modified full-biodegradable composite membrane material preparation process which comprises the following steps: firstly, performing hot mixing and cooling on dried bamboo fiber powder, anhydrous citric acid, choline chloride, activated zinc oxide and pentaerythritol to prepare a bamboo fiber modified premix; then mixing the biodegradable polyester resin with the premix; adding the mixture into an extruder, injecting epoxidized soybean oil into a barrel through a liquid metering device, and performing melt extrusion granulation under a vacuum exhaust condition; and finally carrying out blow molding to form the film. Through in-situ reaction extrusion of multi-component synergism, surface grafting of bamboo fibers, chain extension of a polyester matrix and interface chemical bonding of the bamboo fibers and the polyester matrix are achieved, interface compatibility is effectively improved, degradation of the material in the processing process is inhibited, and the mechanical property and thermal stability of the composite film material are remarkably improved; the process is efficient and environment-friendly, and the cost is controllable.

The invention is suitable for the field of film manufacturing, and provides a PO film tape casting process which comprises the following steps: S1, raw material pretreatment; s2, mixing the materials; s3, melt extrusion; s4, carrying out tape casting; s5, cooling and shaping; s6, thickness detection and adjustment; s7, carrying out post-treatment; and S8, rolling is conducted. According to the invention, the three-stage gradient cooling process significantly reduces the internal stress of the film, improves the dimensional stability, and reduces the warping shrinkage of subsequent processing; the thickness deviation of the thin film is controlled within + / -0.01 mm through an online thickness detection and automatic adjustment system, so that the product precision is improved; the surface tension of the film is stably improved by the corona post-treatment process, and the application scene is widened; through strict raw material pretreatment, the bubble defect of the film is effectively avoided, and the appearance quality of the product is improved; and a combined process of high-speed mixing and double-screw extrusion is adopted, so that uniform dispersion and full plasticization of the materials are ensured, and the problems of crystal points, stripes and the like are reduced.

The invention relates to the technical field of polyurethane films, in particular to a long-acting, stable, flexible, impact-resistant and resistance-reducing protective film and a preparation process thereof. According to the invention, the raw materials such as polyethylene glycol, a modified fluorosilicone monomer, isophorone diisocyanate, hydroxyethyl acrylate, an acrylic antifouling monomer, dodecafluoroheptyl methacrylate and the like are added to prepare the anti-drag coating. Mixing a polyurethane thermoplastic elastomer, aminopropyl polydimethylsiloxane, an antioxidant and an ultraviolet light absorber, and carrying out melt extrusion and blow molding to form a film, so as to obtain a flexible impact-resistant base film; and uniformly coating the surface of the flexible anti-impact base film with the anti-drag coating, and carrying out ultraviolet curing to obtain a finished product. The finished product prepared by the invention has good impact resistance, and can effectively reduce frictional resistance, so that the finished product has wide application prospects in the technical field of polyurethane films.

The invention relates to an antistatic MLCC release film base film and a preparation method thereof. The antistatic MLCC release film base film is prepared by melt blending and biaxial stretching of PET master batch, an antistatic composition and a nano filler, wherein the antistatic composition is prepared by compounding modified PET-PEG and thiophene modified aromatic polyamide; the nano filler is prepared by carrying out melt extrusion on KH550 modified talcum powder and MAH-g-PET (maleic anhydride-grafted polyethylene terephthalate). The antistatic composition disclosed by the invention has the beneficial effects that the antistatic composition is formed by interweaving two polymers, and a stable three-dimensional conductive network is constructed in the PET film, so that the antistatic performance is more efficient, lasting and stable. In addition, through chemically bonded modified talcum powder, the smoothness and low roughness are provided, and meanwhile reinforcing and toughening are achieved; and the single-layer extrusion process can realize ultrathin thin film, the production process is simplified, and the production cost is greatly reduced.

The invention relates to the technical field of coatings, and discloses a modified hexagonal boron nitride and organic silicon double-component doped high-flame-retardant epoxy resin powder coating as well as a preparation method and application thereof. Comprising the following raw materials in parts by weight: 25-50 parts of modified hexagonal boron nitride, 90-110 parts of organic silicon resin, 120-150 parts of epoxy resin, 5-8 parts of dicyandiamide, 100-120 parts of silica powder, 8-12 parts of other auxiliaries and 80-100 parts of filler. The flame-retardant epoxy resin powder coating is prepared by uniformly mixing the components, melting, extruding a sheet material, grinding and sieving. The flame-retardant and fireproof performance of the epoxy resin powder coating is greatly improved in a modified hexagonal boron nitride and organic silicon double-component doping mode.

The invention discloses CPVC (Chlorinated Polyvinyl Chloride) modification-based high-wear-resistance antistatic plastic and a preparation method thereof, belongs to the technical field of composite CPVC preparation, and aims to solve the technical problem that the wear resistance and the antistatic property of CPVC-based plastic in the prior art need to be further improved. The high-wear-resistant antistatic plastic based on CPVC modification comprises the following raw materials in parts by weight: 80-100 parts of modified CPVC, 6-8 parts of a modified heat stabilizer and 8-16 parts of an auxiliary material, the amino group on the surface of the prepared antistatic filler participates in the ammoniation process of the prepared CPVC, a large number of amino groups hybridize the chain segment structure of the CPVC and introduce tertiary amino groups, and an ion structure is introduced into the hybridized CPVC through quaternary ammonium salinization to obtain the modified CPVC. The CPVC-based plastic is obtained by mixing, melting and extruding the CPVC-based plastic, the prepared polyamide acid-based modified heat stabilizer and auxiliary materials.

The invention relates to a preparation method of high-heat-resistance low-warpage glass fiber reinforced flame-retardant PBT (Polybutylene Terephthalate) engineering plastic, which comprises the following steps: firstly, adding a premix into a double-screw extruder for melting, then respectively feeding a flame retardant and glass fiber into the double-screw extruder from a lateral feeding port, mixing with the molten premix, and extruding to obtain the high-heat-resistance low-warpage glass fiber reinforced flame-retardant PBT engineering plastic. After mixing, extruding a strip-shaped object from a machine head mouth mold of the double-screw extruder, finally cooling the strip-shaped object in a cooling water tank, and granulating by a granulator to obtain the high-heat-resistance low-warpage glass fiber reinforced flame-retardant PBT engineering plastic. The premix is obtained by uniformly mixing PBT resin II, low-warpage PBT master batch, a compatilizer, a crystallization inhibiting polymer, a flame-retardant synergist, an inorganic filler, a nucleating agent and other auxiliaries; the low-warpage PBT master batch is prepared by uniformly mixing PBT resin I, a transesterification inhibitor, a transesterification inhibition synergist and other auxiliaries and then carrying out melt extrusion granulation. The warping problem of the glass fiber reinforced flame-retardant PBT engineering plastic is solved, and the glass fiber reinforced flame-retardant PBT engineering plastic has relatively high thermal deformation temperature.

The invention relates to a preparation method of a high-antibacterial hydrophobic polyamide fiber. The preparation method comprises the following steps: carrying out melt extrusion grafting on polyamide, a quaternary ammonium salt monomer, an initiator and an auxiliary agent to prepare quaternary ammonium salt grafted polyamide; and carrying out melt blending on the prepared quaternary ammonium salt grafted polyamide, polyamide, cuprous oxide and polydimethylsiloxane to obtain the high-antibacterial hydrophobic nylon composite material. And spinning the high-antibacterial hydrophobic nylon composite material to obtain the high-antibacterial hydrophobic polyamide fiber. The high-antibacterial hydrophobic nylon composite material prepared by the method disclosed by the invention can realize efficient antibacterial performance, and the high antibacterial hydrophobic performance of the prepared polyamide fiber is improved.

This case relates to a self-healing optical film and its preparation method. The optical film is made by adding a nanoparticle suspension to PET masterbatch as the main material during its melt extrusion process, resulting in a cast sheet. After biaxial stretching, a self-healing coating liquid is coated online, followed by shaping and cooling. The nanoparticle suspension includes nano-titanium oxide, MAH-PET polymer, ATO nanoparticles, and titanate coupling agent. The self-healing coating liquid is produced by core-shell emulsion polymerization, forming a nano-silica hard core and an acrylate functional monomer polymer soft shell. This invention adds the nanoparticle suspension by in-situ feeding in the middle of the extruder, reducing steps, improving dispersion uniformity, and making the film surface smoother. Then, the self-healing coating liquid is applied online after longitudinal stretching and before transverse stretching, forming a film on the film surface, improving the hardness and scratch resistance of the film material, enabling rapid self-healing at room temperature, strong stability, and avoiding the occurrence of rainbow patterns.

The invention belongs to the technical field of high polymer materials, and particularly relates to a PVB (Polyvinyl Butyral) film and a preparation method thereof. The PVB film provided by the invention is prepared from the following components in parts by mass: 100 parts of PVB resin, 33 to 36 parts of triethylene glycol di-2-ethylhexoate, 7 to 9 parts of integrated anti-radiation toughening filler, 1 to 2 parts of organic montmorillonite, 0.8 to 1.2 parts of composite coupling agent, 0.5 to 1 part of ultraviolet light absorber, 0.6 to 0.8 part of antioxidant and 0.8 to 1 part of heat stabilizer. The integrated anti-radiation toughening filler adopts a core-shell structure, the anti-radiation core is composed of bismuth oxide and tungsten oxide according to the mass ratio of 3: 1, and the elastic coating layer is maleic anhydride grafted modified POE. The preparation method comprises the steps of pre-dispersion treatment, component mixing, melt extrusion, film casting, graded cooling, two-way stretching and the like. Through the core-shell structure design of the integrated anti-radiation toughening filler and the optimized processing technology, the anti-radiation performance and the toughening performance are synergistically improved, and the prepared film has the advantages of excellent anti-radiation effect, high toughness and good transparency.

The invention relates to the field of regenerated fiber production equipment manufacturing and process integration, and discloses a modular intelligent continuous regenerated fiber production line which comprises a sorting and cleaning module, a melt extrusion module, an impurity filtering module, a granulation module, a decoloration module, a solid phase polycondensation tackifying module and a melt spinning module. The self-adaptive material distribution device is used for realizing material connection among the modules; the automatic control system is used for realizing collaborative operation of all the modules; wherein the solid phase polycondensation tackifying module is provided with an intelligent control unit for dynamically optimizing the operation of the solid phase polycondensation tackifying module. Compared with the prior art that each process is relatively independent and depends on manual scheduling or simple linkage, the scheme effectively overcomes the common problems of unsmooth material conveying, unbalanced matching between modules and insufficient automation degree in the traditional regeneration process, and remarkably improves the production continuity and the resource utilization rate.

The invention relates to the technical field of materials, and discloses an antibacterial composite pp material and a preparation process thereof.The antibacterial composite pp material is prepared from polypropylene as a main raw material and a compatilizer, a functional fiber modified additive, a rubber additive and the like as auxiliary materials through mixing and extrusion granulation processes. Wherein the functional fiber modified additive is medical stone fiber of which the surface is modified with a reactive macromolecular antibacterial agent, and the reactive macromolecular antibacterial agent can interact with a maleic anhydride group in a compatilizer structure in a subsequent melt extrusion process, so that the interface bonding performance between the medical stone fiber and polypropylene is greatly improved; further, the reinforcing effect of the medical stone fiber is fully exerted, so that the mechanical strength of the polypropylene material is effectively improved. In addition, triclosan in the structure of the macromolecular antibacterial agent has a broad-spectrum antibacterial effect, so that the polypropylene material can be endowed with excellent broad-spectrum antibacterial performance.

The invention relates to a production process of a high-elasticity heat-resistant polyester yarn, which comprises the following steps: firstly, selecting high-molecular-weight polyethylene glycol terephthalate, adding 1-3% of nano filler and 5-10% of functional copolymer, and drying at 150 DEG C for 4-6 hours to improve the stability and processability of the material; secondly, melt extrusion is conducted at 280-290 DEG C, spinning is conducted through a multi-section temperature control spinning head, and the fiber cooling uniformity is effectively controlled. Then, two times of drafting and a heat setting process are adopted, the orientation degree of a molecular chain is improved in one time of drafting, and low-temperature plasma treatment is combined to optimize the surface activity and the setting effect of the fibers. In the secondary drafting, the fiber deformation is finely adjusted at low temperature, the thermal damage is reduced, the elasticity is improved, and finally, xylanase treatment and ultraviolet curing are combined, so that the softness, the skin-friendly property and the weather resistance of the fiber are remarkably improved.

The present invention belongs to the technical field of polymer films, and specifically relates to a polypropylene film for lithium battery current collector and a preparation method thereof. The polypropylene film comprises an upper layer, an intermediate layer and a lower layer; by weight, the components of the upper layer and the lower layer each comprise 70-80 parts of isotactic polypropylene and 20-25 parts of modified polystyrene; the components of the intermediate layer comprise 80-85 parts of isotactic polypropylene and 15-20 parts of cycloolefin copolymer; firstly, the components of the upper layer, the intermediate layer and the lower layer are uniformly mixed, and then the main machine and the auxiliary machine of a three-layer co-extrusion casting machine are added for melt extrusion to obtain a polypropylene film; then, the polypropylene film is subjected to biaxial stretching to obtain a polypropylene film; the obtained composite polypropylene film has good mechanical properties and dielectric properties, high thermal stability, and is more suitable for lithium battery current collectors.

The preparation method of the antibacterial polyester fiber comprises the following steps: firstly, reacting a cationic antibacterial agent with a terminal carboxyl group with 4-sulfobenzoic acid monopotassium salt to obtain a high-temperature-resistant polymerizable cationic antibacterial agent; then taking purified terephthalic acid, a high-temperature-resistant polymerizable cationic antibacterial agent and ethylene glycol as raw materials, adding an auxiliary agent trimethyl phosphate and a catalyst to prepare uniform slurry, and adding the uniform slurry into an esterification reaction kettle; entering a polycondensation stage after esterification is finished, filling nitrogen after reaction is finished, pressurizing, discharging, and performing underwater granulation to obtain antibacterial polyester chips; then, the antibacterial polyester chips are dried until the water content is lower than 30 ppm, and the antibacterial polyester fibers are obtained through the melt extrusion spinning step; the fiber strength of the prepared antibacterial polyester fiber is larger than or equal to 2.8 cN / dtex, the antibacterial rate meets the AAA grade standard, and the antibacterial polyester fiber has good strength and is wide in application range.

The invention discloses a high-toughness regenerated ABS (Acrylonitrile Butadiene Styrene) composite material and a preparation method thereof, belongs to the technical field of material regeneration, and is used for solving the technical problem that the tensile resistance and flame retardance of a regenerated ABS material in the prior art need to be further improved. The regenerated ABS composite material comprises the following raw materials in parts by weight: 70-80 parts of regenerated ABS, 10-12 parts of a modified toughening agent, 15-18 parts of composite whiskers and 3-6 parts of auxiliary materials, in the process of recycling waste ABS, active groups in ABS chain segments are protected by using a protective agent and a temperature agent, regenerated ABS is obtained by using a solvent purification method, a modified toughening agent and composite whiskers are prepared, and after the regenerated ABS, the modified toughening agent and the composite whiskers are subjected to melt extrusion with auxiliary materials, through the promotion effect of a titanium dioxide component on electron irradiation and through irradiation crosslinking, the modified toughening agent, the composite whiskers and the auxiliary materials are subjected to melt extrusion. Finally, the high-toughness composite ABS is prepared.

The invention discloses a high-stability endotoxin-free PHA nano-emulsion and a preparation method thereof, and belongs to the technical field of biodegradable high polymer material compositions and processing thereof. The nano-emulsion is characterized in that the endotoxin content is not higher than 0.10 EU / g, the median particle size d50 is 100-200 nm, and the PDI is not higher than 0.15, and the nano-emulsion is stable in long-term storage. The preparation method is a continuous solvent-free process and comprises the steps of melt extrusion, high-pressure thermal emulsification and deep endotoxin removal. By adopting the specific pH-insensitive cationic polymer emulsifier and the crystallization inhibitor, the chemical contradiction that an efficient alkaline purification process is incompatible with a nano-emulsion stable system is solved, physical aging is inhibited, and an unexpected technical effect is obtained. The invention also discloses an O / W type cream containing the nano emulsion.

The invention discloses a degradable environment-friendly modified plastic master batch and a preparation method thereof, and belongs to the technical field of plastic master batches, the plastic master batch comprises the following raw materials by weight: 100 parts of polypropylene, 40-50 parts of polylactic acid, 10-20 parts of MOFs modified carbon fiber, 5-10 parts of a compatibilizer, and 1-3 parts of an antioxidant; and the compatibilizer is 2-methacryloyloxyethyl phosphorylcholine grafted polypropylene. The preparation method comprises the following steps: uniformly mixing the raw materials, and carrying out melt extrusion. Polypropylene and polylactic acid are used as basic resin, 2-methacryloyloxyethyl phosphorylcholine grafted polypropylene is used as a compatibilizer, and MOFs modified carbon fiber is used as a reinforcing material to prepare the modified plastic master batch which has good biodegradability and mechanical properties; the method has obvious performance advantages and technical competitiveness in practical application.

The invention relates to the technical field of composite materials, in particular to fiber sizing liquid, a polyether-ether-ketone composite material and a preparation method of the polyether-ether-ketone composite material, and the fiber sizing liquid comprises low-molecular-weight polyaryletherketone containing imide side groups, carbon nanotubes and the like; the composite material is obtained by carrying out heat treatment on fibers, re-sizing the fibers by adopting the sizing liquid, and then carrying out melt extrusion on the fibers and polyether-ether-ketone. The sizing liquid provided by the invention can effectively improve the compatibility between fibers and PEEK, so that the mechanical properties of the composite material are obviously improved.

The invention provides a manufacturing process of high-heat-insulation ray-proof antibacterial glass. The high-heat-insulation ray-proof antibacterial glass comprises outer-layer glass, a middle functional layer, inner-layer glass and an extensible layer, the manufacturing process comprises a PVB adhesive film preparation process and a laminated glass whole process, wherein the PVB adhesive film preparation process specifically comprises the steps of raw material mixing, melt extrusion, tape casting and coiling; the whole process of the laminated glass comprises the steps of glass pretreatment, interlayer assembly, high-temperature and high-pressure forming and post-treatment and quality inspection. According to the design scheme of the multi-film composite laminated glass, based on the structural characteristics of the laminated glass, a layered ray-blocking customized glass scheme is provided in combination with the combination of heat-insulating PVB films and other films with different functions, and the scheme is suitable for scenes such as sunlight rooms, agricultural planting or market curtain walls and the like.

The invention provides a special rare earth antibacterial master batch for a PVC antibacterial air conditioner condensate pipe and a preparation method of the special rare earth antibacterial master batch. The problems that an existing PVC condensate pipe is poor in antibacterial performance, and a rare earth antibacterial agent and PVC resin are poor in compatibility and dispersity are solved. The master batch comprises PVC carrier resin, a rare earth antibacterial agent, a dispersing agent, a plasticizer, a heat stabilizer, a lubricant and a bulking agent, and the rare earth antibacterial agent is prepared by mixing rare earth oxide and inorganic oxide according to a specific proportion and carrying out mechanical dispersion, high-energy dispersion, secondary mechanical dispersion, drying, tunnel kiln firing and grinding treatment. The preparation method of the special rare-earth antibacterial master batch for the PVC antibacterial air conditioner condensate pipe comprises the steps of raw material pretreatment, raw material premixing, coupling treatment, mixing and plasticizing, melt extrusion, granulation molding and the like, and through a refining process and a supercritical carbon dioxide technology, it is ensured that a rare-earth antibacterial agent is uniformly dispersed and stably combined in a PVC matrix; the master batch with excellent antibacterial property, thermal stability and mechanical property is prepared.

The invention relates to the technical field of composite current collectors, and discloses a composite current collector. Comprising the following operation steps: S1, uniformly mixing thermal expansion microspheres and a polymer material, and performing melt extrusion and two-way stretching to obtain a current collector base film; s2, depositing a transition layer on each of the two surfaces of the current collector base film to obtain a composite collector film A; s3, depositing a metal layer on each of the two surfaces of the transition layer of the composite film A to obtain a composite film B; and S4, depositing a protective layer on each of the two surfaces of the metal layer of the composite film B to obtain the composite current collector.

The invention provides a slow-release antibacterial enhanced composite film for fruit and vegetable preservation and a preparation method thereof, and the preparation method comprises the following steps: performing sulfonation modification treatment on nano cellulose powder to obtain sulfonated nano cellulose; carrying out quaternization modification treatment on the sulfonated nano-crystalline cellulose to obtain quaternary ammonium sulfonated nano-crystalline cellulose; adding gelatin and sodium carboxymethyl cellulose into deionized water to obtain a wall material solution, and adding curcumin into the wall material solution to obtain a prepolymer solution; stirring and emulsifying the prepolymer solution at a high speed to obtain a prepolymer suspension; adding a chitosan solution into the prepolymer suspension to obtain a microcapsule solution, adding tannic acid into the microcapsule solution to obtain a microcapsule suspension, and performing spray drying to obtain double-layer microcapsule powder; the preparation method comprises the following steps: uniformly mixing polylactic acid, quaternary ammonium sulfonated nanocellulose, the double-layer microcapsule powder, a plasticizer, a lubricant and an antioxidant to obtain a mixed material, and sequentially carrying out melt extrusion, cooling, pelletizing and film blowing.

The invention provides a neurosteroid derivative solid dispersion, a preparation method and application thereof, and a medicine containing a hot-melt extrusion solid dispersion, and belongs to the technical field of pharmacy. The preparation method comprises the following steps: carrying out melt extrusion on a raw material mixture at 125-160 DEG C to obtain the neurosteroid derivative solid dispersion, the mixed material comprises an active component, a plasticizer and a carrier material in a mass ratio of 10: (1-15): (10-90); the active component comprises at least one of a neurosteroid derivative (with a structure as shown in a formula 1), an isomer, a solvate and a pharmaceutically acceptable salt thereof; the plasticizer is selected from one or more of polyethylene glycol, poloxamer and Tween, and the average molecular weight of the polyethylene glycol is 1t; 6000, 6000; active components in the neurosteroid derivative solid dispersion exist in an amorphous state. The neurosteroid derivative in the neurosteroid derivative solid dispersion disclosed by the invention has relatively high oral bioavailability. # imgabs0 #

The invention provides a medical packaging material and a preparation method thereof.The preparation method comprises the steps that S100, polypropylene, maleic anhydride grafted co-polypropylene, peroxide and filler are mixed, then melt extrusion and two-way stretching are conducted, and a printing layer is obtained; s200, respectively preparing a barrier layer and a heat sealing layer; and S300, the heat sealing layer, the blocking layer and the printing layer are sequentially stacked from inside to outside, and the packaging material is obtained. Through the preparation method of the packaging material, the prepared packaging material has excellent barrier property and antibacterial property while resisting high temperature, and can meet the requirements of the medical field.

The invention discloses a graphene antistatic PC composite material and a preparation method thereof, and belongs to the technical field of composite materials. 150-160 parts of polycarbonate resin, 10-20 parts of modified graphene, 2-5 parts of light stabilizer, 2-5 parts of ultraviolet absorber, and 2-5 parts of lubricant are weighed by weight and added to a high-speed mixer, and sent into a twin-screw extruder after mixing evenly, and after melt extrusion, cooled and pelletized to obtain a graphene antistatic PC composite material. The modified graphene contains graphene, quaternary ammonium salt structure and hindered phenol structure, and the modified graphene contains lipophilic benzene ring and long carbon chain, so the modified graphene has good compatibility with the polycarbonate resin containing benzene ring and other raw materials, and the modified graphene can be evenly dispersed in the composite material, and is not easy to agglomerate, so that the modified graphene can fully play a role, giving the composite material excellent antistatic, antibacterial and anti-aging properties.